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39 条记录 (耗时 0.012 秒)

    Method for preparing 1,3,5-triaminobenzene and hydrolyzing it into high-purity phloroglucinal
    1.
    发明授权
    Method for preparing 1,3,5-triaminobenzene and hydrolyzing it into high-purity phloroglucinal 有权
    制备1,3,5-三氨基苯并将其水解成高纯度离体液体的方法

    公开(公告)号：US07217840B2

    公开(公告)日：2007-05-15

    申请号：US10517716

    申请日：2003-06-06

    申请人： Lhassane Ismaili ,  Bernard Refouvelet ,  Alain Xicluna

    发明人： Lhassane Ismaili ,  Bernard Refouvelet ,  Alain Xicluna

    IPC分类号： C07C209/10 ,  C07C37/05

    CPC分类号： C07C209/10 ,  C07C37/05 ,  C07C39/10

    摘要： The invention concerns a method for method for preparing 1,3,5-triaminobenzene, characterized in that it comprises a step which consists in amination of a compound of formula (I), wherein: A represents a halogen atom or a NH2 group; X1 and X2, identical or different, represent each a halogen atom, the amination step being carried out in the presence of ammonia and a catalyst selected from the group consisting of copper salts, cupric and cuprous oxides or mixtures thereof at a temperature ranging between 150° C. and 250° C. and at a pressure higher that 35 bars

    摘要翻译： 本发明涉及一种制备1,3,5-三氨基苯的方法，其特征在于它包括一个步骤，该步骤由式（I）化合物胺化而成，其中：A代表卤原子或NH 2 组; X 1和X 2相同或不同，表示各自的卤素原子，胺化步骤在氨存在下进行，并且催化剂选自： 铜盐，铜和氧化亚铜或其混合物，温度范围为150℃至250℃，压力高于35巴

    Process for producing polyhalogenated phenols
    2.
    发明授权
    Process for producing polyhalogenated phenols 失效
    生产多卤代酚的方法

    公开(公告)号：US4005151A

    公开(公告)日：1977-01-25

    申请号：US555627

    申请日：1975-03-05

    申请人： Masataka Wataya ,  Nobuo Onodera ,  Shosuke Imamura

    发明人： Masataka Wataya ,  Nobuo Onodera ,  Shosuke Imamura

    IPC分类号： C07C27/00 ,  C07C37/045 ,  C07C37/05 ,  C07C39/27 ,  C07C67/00 ,  C07C39/30 ,  C07C39/32

    CPC分类号： C07C37/045 ,  C07C245/20

    摘要： A process for producing polyhalogenated phenol by mixing a polyhalogenated aniline with an aqueous sulfuric acid solution to obtain a suspension of fine particles of polyhalogenated aniline sulfate having the particle size of 50 .mu. or less, diazotizing the polyhalogenated aniline sulfate to obtain polyhalogenate benzenediazonium sulfate, hydrolyzing the resulting benzenediazonium sulfate by heating it as such, recycling to the diazotization step the aqueous sulfuric acid solution from which the desired polyhalogenated phenol has been separated.

    摘要翻译： 通过将多卤代苯胺与硫酸水溶液混合，得到粒径为50μm以下的多卤代苯胺硫酸盐微粒的悬浮液，重氮化多卤代苯胺硫酸盐，得到多卤代苯二氮硫酸盐，水解 通过将其加热得到的重氮化硫酸盐，将所需的多卤代酚分离出来的硫酸水溶液再循环至重氮化步骤。

    4-Phenoxy-phenoxy-alkane-carboxylic acid derivatives and process for their manufacture
    6.
    发明授权
    4-Phenoxy-phenoxy-alkane-carboxylic acid derivatives and process for their manufacture 失效
    4-苯氧基 - 苯氧基 - 烷烃 - 羧酸衍生物及其制备方法

    公开(公告)号：US4391995A

    公开(公告)日：1983-07-05

    申请号：US265902

    申请日：1981-05-21

    申请人： Helmut Nahm ,  Ernold Granzer

    发明人： Helmut Nahm ,  Ernold Granzer

    IPC分类号： A61K31/19 ,  C07C37/05 ,  C07C43/263 ,  C07C43/29 ,  C07C51/09 ,  C07C59/68 ,  C07C59/70 ,  C07C69/712 ,  C07C2/88

    CPC分类号： C07C323/00 ,  C07C51/09 ,  C07C59/68

    摘要： Novel 4-phenoxy-phenoxy-alkane-carboxylic acid derivatives of the formula I ##STR1## in which R.sub.1 stands for hydrogen, methylithio, cyclopentyl, cyclohexyl, phenyl, methylcycylohexyl, ethylcyclohexyl, or R.sub.1 and R.sub.3 together stand for a --CH.dbd.CH--CH.dbd.CH-- bridge or--unless at least one of the substituents R.sub.2 to R.sub.8 stands for hydrogen, or if R.sub.9 stands for a radical having at least 2 carbon atoms--for chlorine,R.sub.2 and R.sub.3, independent of one another, each stands for hydrogen, chlorine or alkyl of 1 to 4 carbon atoms,R.sub.4 stands for hydrogen, chlorine, alkyl of 1 to 4 carbon atoms, cyclopentyl, cyclohexyl, methylcyclohexyl or R.sub.3 and R.sub.4 together stand for a --CH.dbd.CH--CH.dbd.CH-- bridge,R.sub.5, R.sub.6 and R.sub.7, independent of one another, each stands for hydrogen or alkyl of 1 to 4 carbon atoms,R.sub.8 stands for hydrogen, alkyl of 1 to 4 carbon atoms or allyl,R.sub.9 stands for alkyl of 1 to 10 carbon atoms or phenyl andX stands for hydrogen, the cation of a physiologically acceptable inorganic or organic base of a hydrocarbon radical of 1 to 10 carbon atoms, having a strong action on the lipide and cholesterine metabolism and a process for this manufacture.

    摘要翻译： 式I的新型4-苯氧基 - 苯氧基 - 烷 - 羧酸衍生物，其中R1代表氢，甲硫基，环戊基，环己基，苯基，甲基氰基己基，乙基环己基或R1和R3一起代表-CH = CH -CH = CH-桥或 - 除非取代基R2至R8中的至少一个代表氢，或者如果R9表示具有至少2个碳原子的基团，则对于氯，R 2和R 3彼此独立地，各自独立地 对于氢，氯或1至4个碳原子的烷基，R4代表氢，氯，1至4个碳原子的烷基，环戊基，环己基，甲基环己基或R3和R4一起代表-CH = CH-CH = CH- 桥，R5，R6和R7彼此独立，各代表氢或1-4个碳原子的烷基，R8代表氢，1-4个碳原子的烷基或烯丙基，R9代表1-10个碳原子的烷基 原子或苯基，X代表氢，生物学上可接受的无机或有机碱基的阳离子 具有1至10个碳原子的自由基，对脂质和胆固醇代谢具有强烈的作用和用于该制造的方法。

    Phenol process
    8.
    发明授权
    Phenol process 失效
    苯酚工艺

    公开(公告)号：US3919332A

    公开(公告)日：1975-11-11

    申请号：US37327373

    申请日：1973-06-25

    申请人： ETHYL CORP

    发明人： WOLLENSAK JOHN C

    IPC分类号： C07C37/05 ,  C07C37/07 ,  C07C39/06

    CPC分类号： C07C37/07 ,  C07C37/05 ,  C07C39/06

    摘要： Aminobenzenes (e.g., aniline) are converted to the corresponding hydroxybenzene by reaction with water in the presence of a hydrogen transfer catalyst (e.g., palladium) and a reaction propagating agent selected from cyclohexanones and cyclohexylimines. The cyclohexylimine may be formed by initially adding a reducing agent (e.g., hydrogen) to the aminobenzene.

    摘要翻译： 在氢转移催化剂（例如钯）和选自环己酮和环己基亚胺的反应传播剂的存在下，通过与水反应将氨基苯（例如苯胺）转化为相应的羟基苯。 环己基亚胺可以通过首先向氨基苯中加入还原剂（例如氢）形成。

    Hydrolysis of meta-phenylenediamine
    9.
    发明授权
    Hydrolysis of meta-phenylenediamine 失效
    金属 - 苯乙烯胺的水解

    公开(公告)号：US3862246A

    公开(公告)日：1975-01-21

    申请号：US26752572

    申请日：1972-06-29

    申请人： KOPPERS CO INC

    发明人： GRECO NICHOLAS P

    IPC分类号： C01C1/24 ,  C07C37/05 ,  C07C39/08 ,  C07C37/10

    CPC分类号： C01C1/24 ,  C07C37/05 ,  C07C39/08

    摘要： Resorcinol is produced by the hydrolysis of metaphenylenediamine in an aqueous excess of ammonium bisulfate. The reactants are contacted at an elevated temperature for a period of time sufficient to hydrolyze the meta-phenylenediamine to resorcinol. The resorcinol so produced is separated from the reaction mixture. The ammonium sulfate is regenerated to ammonium bisulfate by removing the water and thermally decomposing the byproduct ammonium sulfate at an elevated temperature.

    摘要翻译： 间苯二酚通过在过量的硫酸氢铵水溶液中产生。 将反应物在升高的温度下接触足以将间苯二胺水解成间苯二酚的时间。 如此制备的间苯二酚与反应混合物分离。 通过除去水并在升高的温度下热分解副产物硫酸铵，将硫酸铵再生成硫酸氢铵。