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    Process for preparing a polymer using lithium initiator prepared by in situ preparation
    4.
    发明授权
    Process for preparing a polymer using lithium initiator prepared by in situ preparation 失效
    通过原位制备制备使用锂引发剂的聚合物的方法

    公开(公告)号：US5717043A

    公开(公告)日：1998-02-10

    申请号：US731530

    申请日：1996-10-16

    申请人： Atushi Nakayama ,  Koichi Morita ,  Masaaki Izuchi

    发明人： Atushi Nakayama ,  Koichi Morita ,  Masaaki Izuchi

    IPC分类号： C08F8/42 ,  C08C19/30 ,  C08F4/48 ,  C08F8/44 ,  C08F36/04 ,  C08F212/00 ,  C08F212/02 ,  C08F236/10 ,  C08F12/04

    CPC分类号： C08C19/30 ,  C08F36/04

    摘要： In a polymerization process of at least one of monomers selected from the group consisting of conjugated diene compounds such as butadiene and vinylaromatic compounds such as styrene, an organolithium compound such as butyllithium is added to the polymerization system first in the presence of the monomer, and thereafter a secondary amine compound such as saturated cyclic imine is added thereto to produce a soluble initiator by bringing the both compound into contact with each other. Polymerization is carried out with the soluble initiator formed. The obtained high molecular weight polymer is modified with a coupling agent such as tin tetrachloride. The polymer obtained has a high molecular weight, a narrow molecular weight distribution, and controlled molecular weight, and exhibits remarkable coupling property, low hysteresis loss. The process provides a polymer having a consistent characteristic, regardless of production scale and procedures of adding materials.

    摘要翻译： 在选自共轭二烯化合物如丁二烯和乙烯基芳族化合物如苯乙烯的单体中的至少一种的聚合方法中，首先在单体存在下向聚合体系中加入有机锂化合物如丁基锂，并且 此后，通过使两种化合物相互接触，向其中加入饱和环状亚胺等仲胺化合物，生成可溶性引发剂。 用形成的可溶性引发剂进行聚合。 得到的高分子量聚合物用四氯化锡等偶联剂改性。 所得聚合物具有高分子量，窄分子量分布和受控分子量，显示出显着的偶联性能，低滞后损失。 该方法提供具有一致特性的聚合物，而不管添加材料的生产规模和程序如何。

    Polymers containing thiuram disulfide groups and their preparation
    5.
    发明授权
    Polymers containing thiuram disulfide groups and their preparation 失效
    含有秋兰姆二硫化物基团的聚合物及其制备方法

    公开(公告)号：US5658986A

    公开(公告)日：1997-08-19

    申请号：US574143

    申请日：1995-12-18

    申请人： Gilbert Clouet

    发明人： Gilbert Clouet

    IPC分类号： C08G65/32 ,  C08C19/30 ,  C08F2/38 ,  C08F4/00 ,  C08F8/34 ,  C08F293/00 ,  C08F297/00 ,  C08G63/685 ,  C08G63/688 ,  C08G63/91 ,  C08G65/329 ,  C08G65/334 ,  C08G69/48 ,  C08G75/00 ,  C08L59/04

    CPC分类号： C08G65/3348 ,  C08F2/38 ,  C08F8/34 ,  C08G65/329 ,  C08G75/00

    摘要： These copolymers are denoted by the formulae: ##STR1## P.sub.1, P.sub.2 =vinyl or dienic (p with a value of 1), or polyoxyalkylene, polyester or polyamide (p with a value of 0) polymer block;A=(1) ##STR2## with R.sub.1 denoting, among others, alkyl; (2) ##STR3## where E, G, J have various meanings; (3) ##STR4## M, joined to D, having the value ##STR5## h, i, Q and R having various meanings; D=a single bond or (cyclo)alkylene or arylene group;n=1 to 20.These polymers are iniferters in radical polymerization of vinyl monomers. The macroiniferters (I) and the polyiniferters (II) result, respectively, in triblock copolymers PA--PB--PA and diblock copolymers .paren open-st.PA--PB.paren close-st..sub.z a, z having a value from 2 to 25.

    摘要翻译： 这些共聚物由下式表示：其中P1，P2 =乙烯基或二烯（p值为1），或聚氧化烯，聚酯或聚酰胺（p值为0） ）聚合物嵌段; A =（1），其中R1表示烷基; （2）其中E，G，J具有各种含义; （3） M，连接到D，具有值 h，i，Q和R具有各种含义; D =单键或（环）亚烷基或亚芳基; n = 1〜20。这些聚合物是乙烯基单体的自由基聚合中的引发剂。 分别在三嵌段共聚物PA-PB-PA和二嵌段共聚物+545PA-PB + 546za，z中的大分子引发剂（I）和多异构体（II）的值为2至25。

    Method of encapsulating organic material
    9.
    发明授权
    Method of encapsulating organic material 失效
    封装有机材料的方法

    公开(公告)号：US4812242A

    公开(公告)日：1989-03-14

    申请号：US88990

    申请日：1987-08-21

    申请人： Keith James ,  Graham M. Pring

    发明人： Keith James ,  Graham M. Pring

    IPC分类号： B01D17/05 ,  C02F1/68 ,  C08C19/30 ,  C08F8/32 ,  C08J3/12 ,  C08J3/24 ,  C02F1/40

    CPC分类号： C08C19/30 ,  C02F1/681 ,  Y10S210/925

    摘要： Organic material, particularly organic material floating on a water surface, can be encapsulated by reacting, in the presence of the organic material, (A) a functionalized liquid polymer containing anhydride functional groups which groups are derived from an alpha, beta-ethylenically unsaturated dicarboxylic acid anhydride and (B) an alkoxylated fatty monoamine or polyamine having from 1.5 to 15 moles of alkoxylate per mole of fatty amine. The functionalized polymer (A) may be, for example, maleinized polybutadiene and the alkoxylated fatty amine may be, for example, N,N.sup.1, N.sup.1 -tris (2-hydroxypropyl)-N-oleyl-1,3-diaminopropane. Preferably, the alkoxylated fatty amine is derived from a fatty amine having an iodine value of at least 65. The method may also be used to encapsulate a solid contaminated with organic material e.g. oil drilling cuttings.

    摘要翻译： 有机材料，特别是漂浮在水表面上的有机材料可以通过在有机材料存在下使（A）含有酸酐官能团的官能化液体聚合物反应来包封，该基团衍生自α，β-烯键式不饱和二羧酸 酸酐和（B）每摩尔脂肪胺具有1.5至15摩尔烷氧基化物的烷氧基化脂肪单胺或多胺。 官能化聚合物（A）可以是例如马来化聚丁二烯，烷氧基化脂肪胺可以是例如N，N 1，N 3 - 三（2-羟丙基）-N-油基-1,3-二氨基丙烷。 优选地，烷氧基化脂肪胺衍生自碘值至少为65的脂肪胺。该方法还可用于包封被有机材料污染的固体，例如， 石油钻采。