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    PREPARATION OF THIOALKYLAMINES USING CHLOROSULFONIC ACID
    33.
    发明申请
    PREPARATION OF THIOALKYLAMINES USING CHLOROSULFONIC ACID 审中-公开
    使用氯代酸制备三乙胺

    公开(公告)号：WO2007022901A1

    公开(公告)日：2007-03-01

    申请号：PCT/EP2006/008061

    申请日：2006-08-16

    Applicant: BAYER CROPSCIENCE AG ,  BLASCHKE, Harry ,  PAZENOK, Sergiy

    Inventor： BLASCHKE, Harry ,  PAZENOK, Sergiy

    IPC: C07C303/24 ,  C07C305/06 ,  C07C319/14 ,  C07C323/25

    CPC classification number: C07C303/24 ,  C07C319/14 ,  C07C305/06 ,  C07C323/25

    Abstract: The present invention relates to a novel process for the preparation of compounds of the formula (I) by reacting in a first step amino alcohols of the formula (II) with chlorosulfonic acid to give sulfuric acid esters of the general formula (III) and by reacting these sulfuric acid esters in a second step with mercaptans or salts thereof of the general formula (IV): RSM in each formula, where applicable, R 1 , R 2 , R 3 , R 4 , R 5 , R 6 , R, n and M have the meanings given in the description, in the presence of a diluent and in the presence of a base.

    Abstract translation: 本发明涉及一种通过在式（II）的第一步氨基醇与氯磺酸反应得到通式（III）的硫酸酯和通式 在第二步中将这些硫酸酯与通式（IV）的硫醇或其盐反应：各式中的RSM，如适用的话，R 1，R 2， R 3，R 4，R 5，R 6，R，n和M具有以下含义： 描述，在存在稀释剂的情况下和在碱的存在下。

    METHOD FOR FULLERENE DERIVATIVE AND THE FULLERENE DERIVATIVE, PROTON CONDUCTOR AND ELECTROCHEMICAL DEVICE
    36.
    发明申请
    METHOD FOR FULLERENE DERIVATIVE AND THE FULLERENE DERIVATIVE, PROTON CONDUCTOR AND ELECTROCHEMICAL DEVICE 审中-公开
    富勒烯衍生物和富勒烯衍生物，原子导体和电化学装置的方法

    公开(公告)号：WO02051782A1

    公开(公告)日：2002-07-04

    申请号：PCT/JP2001/011352

    申请日：2001-12-25

    IPC: C01B3/00 ,  C07B61/00 ,  C07C35/44 ,  C07C303/02 ,  C07C303/24 ,  C07C305/20 ,  C07C309/25 ,  H01M8/02 ,  H01M8/10

    CPC classification number: C07C305/20 ,  C07C35/44 ,  C07C309/25 ,  C07C2604/00 ,  H01M8/1016 ,  H01M8/1023 ,  Y02E60/324 ,  Y02P70/56 ,  Y10S977/734 ,  Y10S977/735 ,  Y10S977/74

    Abstract: A method for preparing a fullerene derivative, wherein a fullerene derivative having a group capable of liberating a proton introduced to a carbon atom constituting the fullerene molecule is formed by using a halogenated fullerene formed by halogenating a fullerene molecule as a precursor; a method for preparing a polymerized fullerene derivative, wherein a plurality of fullerene molecules are reacted with an aromatic compound molecule to form a polymer comprising a plurality of fullerene molecules which are bound to one another via the aromatic group of the aromatic compound; a novel and useful proton conductor obtained by using the method; and an electrochemical device, such as a fuel cell, using the proton conductor. The above methods allow the efficient preparation of a fullerene having OH groups or SO3H groups such as fullerenol suitable as a proton conductor. A fullerene derivative prepared by these production methods acts as a proton conductor. The electrochemical device is free from the restriction of atmosphere and thus can be miniaturized and simplified.

    Abstract translation: 一种制备富勒烯衍生物的方法，其中通过使用将富勒烯分子卤化形成的卤代富勒烯作为前体，形成具有能够释放引入构成富勒烯分子的碳原子的质子的基团的富勒烯衍生物; 一种制备聚合富勒烯衍生物的方法，其中多个富勒烯分子与芳族化合物分子反应形成包含多个富勒烯分子的聚合物，所述富勒烯分子通过芳香族化合物的芳香族基团彼此结合; 通过使用该方法获得的新颖有用的质子导体; 以及使用质子导体的电化学装置，例如燃料电池。 上述方法允许有效制备具有OH基团或SO 3 H基团的富勒烯，例如适合作为质子导体的富勒烯醇。 通过这些制备方法制备的富勒烯衍生物作为质子导体。 电化学装置没有大气限制，因此可以小型化和简化。

    SULFATION PROCESS
    37.
    发明申请
    SULFATION PROCESS 审中-公开
    硫化过程

    公开(公告)号：WO2002012179A1

    公开(公告)日：2002-02-14

    申请号：PCT/US2001023751

    申请日：2001-07-27

    Applicant: THE PROCTER & GAMBLE COMPANY

    Inventor： THE PROCTER & GAMBLE COMPANY ,  DUPONT, Jeffrey, Scott ,  GOSSELINK, Eugene, Paul

    IPC: C07C303/24

    CPC classification number: C07C303/24 ,  C07C305/06

    Abstract: The present invention relates to a sulfation process comprising the steps of: a) reacting a tertiary amine with a sulfation precursor having the formula: wherein R1is C1-C22 alkyl, C6-C22 aryl, C7-C22alkylenearyl, and mixtures thereof; to form an admixture comprising a quaternized amine and a sulfating species; and b) reacting a hydroxyl species with said admixture to form a sulfated hydroxyl species. The process of the present invention is adaptable to sulfating a wide range of alcohols including the hydroxyl unit which terminates a polyalkoxylate moiety which are prevalent in the area of surfactants, inter alia, alkyl ethoxy sulfates.

    Abstract translation: 本发明涉及硫酸化方法，其包括以下步骤：a）使叔胺与具有下式的硫酸化前体反应：其中R 1是C 1 -C 22烷基，C 6 -C 22芳基，C 7 -C 22亚烷基硬脂基和混合物 物; 以形成包含季铵化胺和硫酸盐物质的混合物; 和b）使羟基与所述混合物反应以形成硫酸化的羟基。 本发明的方法适用于硫酸化宽范围的醇，包括终止在表面活性剂，尤其是烷基乙氧基硫酸盐区域中普遍存在的聚烷氧基化物部分的羟基单元。

    SYNTHESIS OF SULFATED POLYHYDROXY FATTY ACID AMIDE SURFACTANTS
    39.
    发明申请
    SYNTHESIS OF SULFATED POLYHYDROXY FATTY ACID AMIDE SURFACTANTS 审中-公开
    磺化多羟基脂肪酸酰胺表面活性剂的合成

    公开(公告)号：WO1994012472A1

    公开(公告)日：1994-06-09

    申请号：PCT/US1993011452

    申请日：1993-11-24

    Applicant: THE PROCTER & GAMBLE COMPANY

    Inventor： THE PROCTER & GAMBLE COMPANY ,  LETTON, James, Carey

    IPC: C07C303/24

    CPC classification number: C11D1/28 ,  C07C305/10

    Abstract: Polyhydroxy fatty acid amide nonionic surfactants are converted in high yields to their sulfated analog surfactants using an SO3/pyridine complex as a sulfating agent. Thus, C12-C18N-methyl glucamide is sulfated in methylene chloride or pyridine solvent to form the corresponding sulfated glucamide in yields of 80 % or higher.

    Abstract translation: 使用SO 3 /吡啶络合物作为硫酸化剂，将多羟基脂肪酸酰胺非离子表面活性剂以高产率转化为其硫酸化类似物表面活性剂。 因此，C12-C18N-甲基葡糖酰胺在二氯甲烷或吡啶溶剂中硫酸化，形成相应的硫酸化葡糖酰胺，收率为80％以上。

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