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    IRON- AND COPPER-CONTAINING ZEOLITE BETA FROM ORGANOTEMPLATE-FREE SYNTHESIS AND USE THEREOF IN THE SELECTIVE CATALYTIC REDUCTION OF NOX
    2.
    发明申请
    IRON- AND COPPER-CONTAINING ZEOLITE BETA FROM ORGANOTEMPLATE-FREE SYNTHESIS AND USE THEREOF IN THE SELECTIVE CATALYTIC REDUCTION OF NOX 审中-公开
    含钴和铜含量的沸石合成及其在选择性催化还原NOX中的应用

    公开(公告)号：WO2013118063A1

    公开(公告)日：2013-08-15

    申请号：PCT/IB2013/050984

    申请日：2013-02-06

    申请人： BASF SE ,  BASF (CHINA) COMPANY LIMITED ,  BASF SCHWEIZ AG

    发明人： MAURER, Stefan ,  WYCISK, Michael ,  PETRY, Julia ,  DEUERLEIN, Stephan ,  ZHANG, Weiping ,  SHI, Chuan ,  TAKASHI, Hihara

    IPC分类号： C01B39/00 ,  B01J29/00 ,  B01J29/70 ,  B01J29/72 ,  B01J29/78

    CPC分类号： B01J29/7215 ,  B01D53/8628 ,  B01D53/9418 ,  B01D2255/20738 ,  B01D2255/20761 ,  B01D2255/502 ,  B01D2257/404 ,  B01J29/7615 ,  B01J35/002 ,  B01J2229/186 ,  B01J2229/42 ,  C01B39/065 ,  C01B39/46

    摘要： The present invention relates to a process for the production of a zeolitic material having a BEA-type framework structure comprising YO 2 and X 2 O 3 , wherein said process comprises the steps of (1) preparing a mixture comprising one or more sources for YO 2 , one or more sources for X 2 O 3 , and seed crystals comprising one or more zeolitic materials having a BEA-type framework structure; (2) crystallizing the mixture obtained in step (1); and (3) subjecting the zeolitic material having a BEA-type framework structure obtained in step (2) to an ion-exchange procedure with Cu and/or Fe; wherein Y is a tetravalent element, and X is a trivaient element, wherein the mixture provided in step (1) and crystallized in step (2) does not contain an organotemplate as structure-directing agent, and wherein the total amount of Cu and/or Fe in the ion-exchanged material obtained in step (3) ranges from 0.1 to 25 wt.-% calculated as Fe 2 O 3 and CuO, as well as to a zeolitic material having a BEA-type framework structure which may be obtained according to said process, and to a method for the treatment of NO x by selective catalytic reduction (SCR) using said zeolitic material.

    摘要翻译： 本发明涉及一种生产具有包含YO 2和X 2 O 3的BEA型骨架结构的沸石材料的方法，其中所述方法包括以下步骤：（1）制备包含一种或多种Y 2 O 2源，一种或多种 X2O3的来源，以及包含一种或多种具有BEA型骨架结构的沸石材料的晶种; （2）使步骤（1）中获得的混合物结晶; 和（3）使具有步骤（2）中获得的BEA型骨架结构的沸石材料与Cu和/或Fe进行离子交换程序; 其中Y是四价元素，X是三元素，其中在步骤（1）中提供并在步骤（2）中结晶的混合物不含作为结构导向剂的有机模板，并且其中Cu和/ 在步骤（3）中获得的离子交换材料中的Fe或Fe按照Fe 2 O 3和CuO计算为0.1至25重量％，以及具有BEA型骨架结构的沸石材料，其可以根据所述 方法以及使用所述沸石材料通过选择性催化还原（SCR）处理NOx的方法。

    BIMETAL-EXCHANGED ZEOLITE BETA FROM ORGANOTEMPLATE-FREE SYNTHESIS AND USE THEREOF IN THE SELECTIVE CATALYTIC REDUCTION OF NOX
    4.
    发明申请
    BIMETAL-EXCHANGED ZEOLITE BETA FROM ORGANOTEMPLATE-FREE SYNTHESIS AND USE THEREOF IN THE SELECTIVE CATALYTIC REDUCTION OF NOX 审中-公开
    无机合成的双官能交换沸石和在选择性催化还原NOX中的用途

    公开(公告)号：WO2015101930A1

    公开(公告)日：2015-07-09

    申请号：PCT/IB2014/067413

    申请日：2014-12-30

    申请人： BASF SE ,  TOKYO INSTITUTE OF TECHNOLOGY ,  BASF (CHINA) COMPANY LIMITED

    发明人： FEYEN, Mathias ,  MAURER, Stefan ,  MÜLLER, Ulrich ,  BAO, Xinhe ,  ZHANG, Weiping ,  DE VOS, Dirk ,  GIES, Hermann ,  XIAO, Feng-Shou ,  TOSHIYUKI, Yokoi ,  YILMAZ, Bilge

    IPC分类号： C01B39/00 ,  B01J29/00

    CPC分类号： B01D53/9418 ,  B01D2255/20738 ,  B01D2255/20761 ,  B01D2255/502 ,  B01J29/7615 ,  B01J37/0203 ,  B01J37/04 ,  B01J37/30 ,  B01J2229/183 ,  B01J2229/186 ,  B01J2229/34 ,  C01B39/026 ,  C01B39/46

    摘要： The present invention relates to a process for the production of a zeolitic material having a BEA-type framework structure comprising YO 2 and X2O 3 , wherein said process comprises the steps of (1)preparing a mixture comprising one or more sources for YO 2 and one or more sources for X 2 O 3 ; (2)crystallizing the mixture obtained in step (1); (3)subjecting the zeolitic material having a BEA-type framework structure obtained in step (2) to an ion-exchange procedure with Cu; and (4) subjecting the Cu ion-exchanged zeolitic material obtained in step (3) to an ion-exchange procedure with Fe; wherein Y is a tetravalent element, and X is a trivalent element, wherein the mixture provided in step (1) and crystallized in step (2) further comprises seed crystals comprising one or more zeolitic materials having a BEA-type framework structure, and wherein the mixture provided in step (1) and crystallized in step (2) does not contain an organotemplate as a structure-directing agent, as well as to the zeolitic material having a BEA framework structure per se, and to its use, in particular in a method for the treatment of NO x by selective catalytic reduction (SCR).

    摘要翻译： 本发明涉及生产具有包含YO 2和X 2 O 3的BEA型骨架结构的沸石材料的方法，其中所述方法包括以下步骤：（1）制备包含一种或多种YO 2和一种或多种源的混合物 X2O3的来源; （2）使步骤（1）中获得的混合物结晶; （3）将具有步骤（2）中获得的BEA型骨架结构的沸石材料与Cu进行离子交换程序; 和（4）使步骤（3）中获得的Cu离子交换的沸石材料与Fe的离子交换程序; 其中Y是四价元素，X是三价元素，其中在步骤（1）中提供并在步骤（2）中结晶的混合物还包含包含一种或多种具有BEA型骨架结构的沸石材料的晶种，其中 步骤（1）中提供并在步骤（2）中结晶的混合物不含作为结构导向剂的有机模板，以及本身具有BEA骨架结构的沸石材料，特别是其用途 通过选择性催化还原（SCR）处理NOx的方法。

    METHOD AND USE FOR THE TERTIARY MINERAL OIL PRODUCTION BY MEANS OF METAL-ORGANIC FRAMEWORK MATERIALS
    6.
    发明申请
    METHOD AND USE FOR THE TERTIARY MINERAL OIL PRODUCTION BY MEANS OF METAL-ORGANIC FRAMEWORK MATERIALS 审中-公开
    方法和使用金属有机框架材料的初步矿物油生产

    公开(公告)号：WO2015083113A1

    公开(公告)日：2015-06-11

    申请号：PCT/IB2014/066586

    申请日：2014-12-04

    申请人： BASF SE ,  BASF CHINA COMPANY LIMITED

    发明人： MAURER, Stefan ,  KIMURA, Riichiro ,  PARVULESCU, Andrei-Nicolae ,  REINHARDT, Caroline ,  SIGGEL, Lorenz ,  MÜLLER, Ulrich

    IPC分类号： C09K8/58 ,  C07D233/58

    CPC分类号： C07D233/58 ,  C09K8/58

    摘要： The invention relates to a method for tertiary mineral oil production, in which an aqueous suspension, comprising at least one porous metal-organic framework material,is injected through at least one injection borehole into a mineral oil deposit, and crude oil is withdrawn from the deposit through at least one production borehole. The invention further relates to the use of an aqueous suspension, comprising at least one porous metal-organic framework material. The invention further relates to the use of at least one porous metal-organic framework material or an aqueous suspension for tertiary mineral production.

    摘要翻译： 本发明涉及一种用于三次矿物油生产的方法，其中包含至少一种多孔金属 - 有机骨架材料的水性悬浮液通过至少一个注入孔注入矿物油沉积物中，并将原油从 通过至少一个生产井眼沉积。 本发明还涉及包含至少一种多孔金属 - 有机骨架材料的水性悬浮液的用途。 本发明还涉及至少一种多孔金属 - 有机骨架材料或水性悬浮液用于三次矿物生产的用途。

    METHOD FOR UPTAKING A SPILLED LIQUID
    7.
    发明申请
    METHOD FOR UPTAKING A SPILLED LIQUID 审中-公开
    一种溢出液体的方法

    公开(公告)号：WO2015025250A1

    公开(公告)日：2015-02-26

    申请号：PCT/IB2014/063911

    申请日：2014-08-14

    申请人： BASF SE ,  BASF CHINA COMPANY LIMITED

    发明人： MAURER, Stefan ,  KIMURA, Riichiro ,  PARVULESCU, Andrei-Nicolae ,  PETRY, Julia ,  SIGGEL, Lorenz ,  MÜLLER, Ulrich

    IPC分类号： C02F1/28 ,  B01J20/26 ,  B01D15/00

    CPC分类号： B01J20/28042 ,  B01J20/226 ,  C02F1/285 ,  C02F1/40 ,  C02F2101/32 ,  C02F2103/365

    摘要： The present invention relates to a method for at least partly uptaking a spilled liquid comprising at least one liquid hydrocarbon, the method comprising the step of contacting the at least one liquid hydrocarbon with a binder agent comprising at least one porous metal-organic framework material, wherein the at least one metal-organic framework material comprises at least one organic compound coordinated to at least one metal ion, wherein the at least one organic com- pound is based on imidazole, which is unsubstituted or substituted with one or more substituents independently selected from the group consisting of C 1-6 alkyl, phenyl and benzyl. The invention further relates to the use of such a binder agent for at least partly uptaking the liquid.

    摘要翻译： 本发明涉及至少部分吸收包含至少一种液体烃的溢出液体的方法，该方法包括使至少一种液态烃与包含至少一种多孔金属 - 有机骨架材料的粘合剂接触的步骤， 其中所述至少一种金属 - 有机骨架材料包含与至少一种金属离子配位的至少一种有机化合物，其中所述至少一种有机化合物是基于咪唑，其是未取代的或被一个或多个独立选择的取代基取代的取代基 由C1-6烷基，苯基和苄基组成。 本发明还涉及这种粘合剂用于至少部分吸收液体的用途。

    HIGHLY EFFICIENT SOLIDOTHERMAL SYNTHESIS OF ZEOLITIC MATERIALS
    8.
    发明申请
    HIGHLY EFFICIENT SOLIDOTHERMAL SYNTHESIS OF ZEOLITIC MATERIALS 审中-公开
    高效固体材料的热固性合成

    公开(公告)号：WO2018059316A1

    公开(公告)日：2018-04-05

    申请号：PCT/CN2017/102887

    申请日：2017-09-22

    申请人： BASF SE ,  BASF (CHINA) COMPANY LIMITED

    发明人： PARVULESCU, Andrei-Nicolae ,  MUELLER, Ulrich ,  MCGUIRE, Robert ,  ARNOLD, Lena ,  DAI, Yu ,  MAURER, Stefan ,  XIAO, Fengshou ,  MENG, Xiangju ,  BIAN, Chaoqun ,  WU, Qinming

    IPC分类号： C01B39/02 ,  C01B39/38

    摘要： A process for preparing a zeolitic material having a zeolitic framework structure which exhibits a molar ratio (aAl 2 O 3 ) : SiO 2 or a crystalline precursor thereof, comprising (i) pre-paring a mixture comprising H 2 O, one or more compounds comprising Si from which SiO 2 in the zeolitic framework structure is formed, said one or more compounds compris-ing a silica gel exhibiting a molar ratio (c H 2 O) : SiO 2 and optionally one or more com-pounds comprising Al from which Al 2 O 3 in the zeolitic framework structure is formed; (ii) subjecting the mixture obtained in (i) to crystallization at a crystallization temperature in the range of from 110 to 350 ℃, preferably in the range of from 190 to 350 ℃, and for a crystallization time in the range of from 0.1 to 48 h.

    摘要翻译： 制备具有沸石骨架结构的沸石材料的方法，所述沸石骨架结构表现出摩尔比（aAl 2 O 3：SiO 2）：SiO 2： 其包含（i）预混合包含H 2 O，一种或多种包含Si的混合物，其中SiO 2在 形成沸石骨架结构，所述一种或多种化合物包含表现出摩尔比（c H 2 O）:SiO 2 2和任选地一种或多种 包含形成沸石骨架结构中的Al 2 O 3的Al的化合物; （ii）使（i）中得到的混合物在110-350℃，优选190-350℃的结晶温度下结晶，结晶时间范围为0.1-1.0 48小时。

    SOLIDOTHERMAL SYNTHESIS OF ZEOLITIC MATERIALS AND ZEOLITES OBTAINED THEREFROM
    9.
    发明申请
    SOLIDOTHERMAL SYNTHESIS OF ZEOLITIC MATERIALS AND ZEOLITES OBTAINED THEREFROM 审中-公开
    由此获得的ZEOLITIC MATERIALS和ZEOLITES的固体合成

    公开(公告)号：WO2016058541A1

    公开(公告)日：2016-04-21

    申请号：PCT/CN2015/091979

    申请日：2015-10-15

    申请人： BASF SE ,  BASF (CHINA) COMPANY LIMITED

    发明人： MAURER, Stefan ,  MUELLER, Ulrich ,  XIAO, Feng-Shou ,  MENG, Xiangju ,  WU, Qinming

    IPC分类号： C01B39/00 ,  C01B37/00

    CPC分类号： C01B39/48 ,  C01B37/02 ,  C01B39/087 ,  C01B39/40

    摘要： Provided is a process for preparing a zeolitic material comprising YO 2 in its framework structure, wherein Y stands for a tetravalent element. The process comprises the steps of: (1) providing a mixture comprising one or more sources for YO 2 , one or more fluoride containing compounds, and one or more structure directing agents; (2) crystallizing the mixture obtained in step (1) for obtaining the zeolitic material; wherein the mixture provided in step (1) and crystallized in step (2) contains 35 wt.% or less of H 2 O based on 100 wt.% of YO 2 . Also provided are a zeolitic material obtained according to the process, and a zeolitic material per se comprising SiO 2 in its framework structure, wherein the ratio of the total integration value of the peaks associated to Q3 signals to the total integration value of the peaks associated to Q4 signals is in the range of from 0:100 to 20:80 in the 29 Si MAS NMR spectrum of the zeolitic material. Further provided is use of the aforementioned zeolitic materials.

    摘要翻译： 提供了一种制备其框架结构中包含YO 2的沸石材料的方法，其中Y代表四价元素。 该方法包括以下步骤：（1）提供包含一种或多种用于YO 2，一种或多种含氟化合物和一种或多种结构导向剂的来源的混合物; （2）使步骤（1）中得到的混合物结晶得到沸石材料; 其中在步骤（1）中提供并在步骤（2）中结晶的混合物含有基于100重量％的YO 2的35重量％或更少的H 2 O。 还提供了根据该方法获得的沸石材料，并且沸石材料本身在其骨架结构中包含SiO 2，其中与Q3信号相关联的峰的总积分值与与峰相关的峰的总积分值的比率 Q4信号在沸石材料的29Si MAS NMR光谱中在0:100至20:80的范围内。 进一步提供使用上述沸石材料。

    ORGANOTEMPLATE-FREE SOLID-STATE SYNTHETIC METHOD FOR ZEOLITE MOLECULAR SIEVES
    10.
    发明申请
    ORGANOTEMPLATE-FREE SOLID-STATE SYNTHETIC METHOD FOR ZEOLITE MOLECULAR SIEVES 审中-公开
    无机硅固体分子筛固体合成方法

    公开(公告)号：WO2014086300A1

    公开(公告)日：2014-06-12

    申请号：PCT/CN2013/088654

    申请日：2013-12-05

    申请人： BASF SE ,  BASF (CHINA) COMPANY LIMITED

    发明人： MAURER, Stefan ,  MULLER, Ulrich ,  XIAO, Feng-Shou ,  MENG, Xiangju ,  WU, Qinming

    IPC分类号： C01B39/02 ,  C01B39/38 ,  B01J29/06

    CPC分类号： C01B39/46 ,  B01J29/08 ,  B01J29/18 ,  B01J29/40 ,  B01J29/70 ,  B01J35/002 ,  B01J35/1023 ,  B01J35/1038 ,  B01J37/009 ,  B01J37/04 ,  C01B39/02 ,  C01B39/14 ,  C01B39/20 ,  C01B39/26 ,  C01B39/38

    摘要： The present invention relates to a preparation method for zeolite molecular sieves. The object of the present invention is to provide a method for synthesizing zeolite molecular sieves by means of solid-state reactions without the usage of organic templates. The method comprises following steps: grinding and mixing the solid raw materials comprising the silicon source, the aluminum source and the alkali source, transferring the obtained mixture into an autoclave, conducting the crystallization for a period of 5 hours – 20 days at a temperature of 50-200 ℃. After filtering and drying the crystallized products, molecular sieves in a powder form can be obtained. By using the method of the present invention, different molecular sieves, including ZSM-5 zeolite, Beta zeolite, FAU zeolite, MOR zeolite, LTA zeolite and GIS zeolite, with a high crystallinity and an adjustable Si/Al ratio within a certain range can be obtained. The obtained products exhibit a high crystallinity and a high purity, and the method of the present invention does not require the use of organic templates and solvents, which avoids unnecessary consumptions during the production, simplifies the synthetic process, and also increases the yield from the autoclave reactor.

    摘要翻译： 本发明涉及沸石分子筛的制备方法。 本发明的目的是提供通过固相反应合成沸石分子筛的方法，而不使用有机模板。 该方法包括以下步骤：研磨和混合包含硅源，铝源和碱源的固体原料，将获得的混合物转移到高压釜中，在5〜20天的温度下进行结晶， 50-200℃。 过滤并干燥结晶产物后，可获得粉末形式的分子筛。 通过使用本发明的方法，在一定范围内具有高结晶度和可调Si / Al比的不同分子筛，包括ZSM-5沸石，β沸石，FAU沸石，MOR沸石，LTA沸石和GIS沸石， 得到。 所得产品具有高结晶度和高纯度，并且本发明的方法不需要使用有机模板和溶剂，其避免了在生产过程中不必要的消耗，简化了合成过程，并且还提高了从 高压釜反应器。