METHOD FOR PRODUCING WATER-RESISTANT ALUMINUM NITRIDE POWDER
    3.
    发明公开
    METHOD FOR PRODUCING WATER-RESISTANT ALUMINUM NITRIDE POWDER 审中-公开
    用于生产耐水氮化铝

    公开(公告)号:EP2894126A4

    公开(公告)日:2016-04-13

    申请号:EP13834918

    申请日:2013-09-06

    Applicant: TOKUYAMA CORP

    Abstract: Provided is a method for producing a water-resistant aluminum nitride powder capable of adding a good water-resistant property to an aluminum nitride powder wherein yttria exists on a particle surface. The method is for producing a water-resistant aluminum nitride powder by carrying out a treatment to a particle surface of an aluminum nitride powder, the method including the successive steps of (i) making an aluminum nitride powder contact with an acid solution wherein yttria exists at least on a particle surface of the aluminum nitride powder; and (ii) making the aluminum nitride powder contact with a phosphorous acid compound, wherein the amount of yttria which is extracted when the aluminum nitride powder is filtered, washed with water, and dried after the step (i) and is thereafter subjected to extraction with 1 mol/L hydrochloric acid is no more than 1000 mg per 100 g of the aluminum nitride powder.

    METHOD FOR PRODUCING SINTERED ALUMINUM NITRIDE GRANULES
    10.
    发明公开
    METHOD FOR PRODUCING SINTERED ALUMINUM NITRIDE GRANULES 审中-公开
    生产烧结的氮化铝颗粒的方法

    公开(公告)号:EP2952476A4

    公开(公告)日:2016-08-10

    申请号:EP13873822

    申请日:2013-02-04

    Applicant: TOKUYAMA CORP

    Abstract: [Problem] To provide a method for producing sintered aluminum nitride granules, which have high thermal conductivity and an excellent property of being filled in a resin, have an average grain diameter of 10 to 200 µm, and are useful as a filler for heat-releasing materials such as a heat-releasing resin, grease, adhesive agent or coating agent, in a simple manner. [Solution] The method for producing sintered aluminum nitride granules according to the present invention is characterized by comprising: a reduction nitridation step of carrying out the reduction nitridation of porous alumina granules at a temperature of 1400 to 1700°C inclusive to produce porous aluminum nitride granules; and a sintering step of sintering the porous aluminum nitride granules, which are produced in the reduction nitridation step, at a temperature of 1580 to 1900°C inclusive.

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