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    Fluorine-containing compound and method for producing fluorine-containing polymerizable monomer derived therefrom
    3.
    发明专利
    Fluorine-containing compound and method for producing fluorine-containing polymerizable monomer derived therefrom 有权
    含氟化合物及其制备含有含氟聚合性单体的方法

    公开(公告)号：JP2012201608A

    公开(公告)日：2012-10-22

    申请号：JP2011065811

    申请日：2011-03-24

    申请人： Central Glass Co Ltd ,  セントラル硝子株式会社

    发明人： SUGAFUJI ARIMASA

    IPC分类号： C07C37/20 ,  C07B61/00 ,  C07C39/24 ,  C07C67/08 ,  C07C69/653

    摘要： PROBLEM TO BE SOLVED: To provide a method for producing a fluorine-containing polymerizable monomer, with which a fluorine-containing compound with a hydroxy fluoroalkyl group bonded to the para position thereof is obtained with high selectivity by making phenols and a fluorine-containing ketone react with each other.SOLUTION: A fluorine-containing compound of general formula (3) is obtained by making a compound of general formula (1) and a fluorine-containing ketone of general formula (2) react with each other in the presence of a fluorine-containing acid catalyst (in formulas, R-Rrespectively and independently represent a hydrogen atom, a straight chain, branched or cyclic alkyl group, an alkenyl group, and so on, and optionally have a fluorine or oxygen atom, Rand Rare optionally bonded to each other and either of them has a fluorine atom, X is an integer of 0-2, and Y is an integer of 0-8).

    摘要翻译： 解决问题的方法：提供一种含氟聚合性单体的制造方法，通过使苯酚和氟得到高选择性的与其对位接合的含氟羟烷基的含氟化合物 的酮反应。 解决方案：通式（3）的含氟化合物通过使通式（1）的化合物和通式（2）的含氟酮在氟的存在下相互反应而获得 （式中，R 1 -R 3 分别独立地表示氢原子，直链，支链 或环状烷基，烯基等，并且任选具有氟或氧原子，R 2 >可以相互键合并且它们中的任一个具有氟原子，X是0-2的整数，Y是0-8的整数）。 版权所有（C）2013，JPO＆INPIT

    Method of producing 2-(4-hydroxyphenyl)hexafluoropropan-2-ol
    8.
    发明专利
    Method of producing 2-(4-hydroxyphenyl)hexafluoropropan-2-ol 审中-公开
    2-（4-羟基苯基）十六烷基-2-醇的生产方法

    公开(公告)号：JP2010235501A

    公开(公告)日：2010-10-21

    申请号：JP2009084395

    申请日：2009-03-31

    申请人： Central Glass Co Ltd ,  セントラル硝子株式会社

    发明人： KATSUHARA YUTAKA ,  ISHIMARU TAKEHISA

    IPC分类号： C07C37/20 ,  C07B61/00 ,  C07C39/24

    摘要： PROBLEM TO BE SOLVED: To provide a method of industrially producing 2-(4-hydroxyphenyl)hexafluoropropan-2-ol (a p-M isomer) from hexafluoroacetone and phenol, capable of securing high selectivity of the p-M isomer and of simplifying a purification process for obtaining a product of high purity.
    SOLUTION: There is provided the method of producing 2-(4-hydroxyphenyl)hexafluoropropan-2-ol by allowing hexafluoroacetone to react with phenol in the presence of hydrogen fluoride, wherein 1 to 5 moles of hexafluoroacetone and 1 to 200 moles of hydrogen fluoride relative to 1 mole of phenol are used at a reaction temperature of 0 to 50°C.
    COPYRIGHT: (C)2011,JPO&INPIT

    摘要翻译： 待解决的问题：提供从六氟丙酮和苯酚工业生产2-（4-羟基苯基）六氟丙-2-醇（pM异构体）的方法，能够确保pM异构体的高选择性和简化 用于获得高纯度产物的纯化方法。 解决方案：提供了在氟化氢存在下使六氟丙酮与苯酚反应制备2-（4-羟基苯基）六氟丙-2-醇的方法，其中1至5摩尔六氟丙酮和1至200摩尔 的氟化氢相对于1摩尔苯酚在0至50℃的反应温度下使用。 版权所有（C）2011，JPO＆INPIT