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    Layer-by-layer removal of graphene
    1.
    发明授权
    Layer-by-layer removal of graphene 有权
    逐层去除石墨烯

    公开(公告)号：US09005460B2

    公开(公告)日：2015-04-14

    申请号：US13878876

    申请日：2011-10-11

    申请人： James M. Tour ,  Ayrat M. Dimiev ,  Dmitry V. Kosynkin

    发明人： James M. Tour ,  Ayrat M. Dimiev ,  Dmitry V. Kosynkin

    IPC分类号： C03C25/68 ,  C01B31/04 ,  H01L21/306 ,  H01L21/308 ,  B82Y30/00 ,  B82Y40/00

    CPC分类号： C01B31/0484 ,  B82Y30/00 ,  B82Y40/00 ,  C01B32/182 ,  C01B32/19 ,  C01B32/192 ,  C01B32/194 ,  H01L21/30604 ,  H01L21/3085

    摘要： The present invention provides methods of selectively removing one or more graphene layers from a graphene material by: (1) applying a metal to a surface of the graphene material; and (2) applying a hydrogen containing solution to the surface of the graphene material that is associated with the metal. The hydrogen containing solution dissolves the metal along with one or more layers of graphene associated with the metal, thereby removing the layer(s) of graphene from the graphene material. In some embodiments, the hydrogen containing solution is an acidic solution, such as hydrochloric acid. In some embodiments, the metal is zinc. In some embodiments, the methods of the present invention are utilized to selectively remove one or more layers of graphene from one or more targeted sites on the surface of a graphene material.

    摘要翻译： 本发明提供了通过以下步骤从石墨烯材料中选择性地去除一个或多个石墨烯层的方法：（1）将金属施加到石墨烯材料的表面; 和（2）将含氢溶液施加到与金属相关联的石墨烯材料的表面。 含氢溶液与一个或多个与金属相关的石墨烯层一起溶解金属，从而从石墨烯材料去除石墨烯层。 在一些实施方案中，含氢溶液是酸性溶液，例如盐酸。 在一些实施方案中，金属是锌。 在一些实施方案中，本发明的方法用于从石墨烯材料表面上的一个或多个目标位点选择性地除去一层或多层石墨烯。

    LAYER-BY-LAYER REMOVAL OF GRAPHENE
    2.
    发明申请
    LAYER-BY-LAYER REMOVAL OF GRAPHENE 有权
    逐层去除石墨

    公开(公告)号：US20130319973A1

    公开(公告)日：2013-12-05

    申请号：US13878876

    申请日：2011-10-11

    申请人： James M. Tour ,  Ayrat M. Dimiev ,  Dmitry V. Kosynkin

    发明人： James M. Tour ,  Ayrat M. Dimiev ,  Dmitry V. Kosynkin

    IPC分类号： C01B31/04

    CPC分类号： C01B31/0484 ,  B82Y30/00 ,  B82Y40/00 ,  C01B32/182 ,  C01B32/19 ,  C01B32/192 ,  C01B32/194 ,  H01L21/30604 ,  H01L21/3085

    摘要： The present invention provides methods of selectively removing one or more graphene layers from a graphene material by: (1) applying a metal to a surface of the graphene material; and (2) applying a hydrogen containing solution to the surface of the graphene material that is associated with the metal. The hydrogen containing solution dissolves the metal along with one or more layers of graphene associated with the metal, thereby removing the layer(s) of graphene from the graphene material. In some embodiments, the hydrogen containing solution is an acidic solution, such as hydrochloric acid. In some embodiments, the metal is zinc. In some embodiments, the methods of the present invention are utilized to selectively remove one or more layers of graphene from one or more targeted sites on the surface of a graphene material.

    摘要翻译： 本发明提供了通过以下步骤从石墨烯材料中选择性地去除一个或多个石墨烯层的方法：（1）将金属施加到石墨烯材料的表面; 和（2）将含氢溶液施加到与金属相关联的石墨烯材料的表面。 含氢溶液与一个或多个与金属相关的石墨烯层一起溶解金属，从而从石墨烯材料中除去石墨烯层。 在一些实施方案中，含氢溶液是酸性溶液，例如盐酸。 在一些实施方案中，金属是锌。 在一些实施方案中，本发明的方法用于从石墨烯材料表面上的一个或多个目标位点选择性地除去一层或多层石墨烯。

    Methods for preparation of graphene nanoribbons from carbon nanotubes and compositions, thin films and devices derived therefrom
    4.
    发明授权
    Methods for preparation of graphene nanoribbons from carbon nanotubes and compositions, thin films and devices derived therefrom 有权
    从碳纳米管和组合物制备石墨烯纳米带的方法，由其衍生的薄膜和器件

    公开(公告)号：US08703090B2

    公开(公告)日：2014-04-22

    申请号：US12544017

    申请日：2009-08-19

    申请人： James M. Tour ,  Dmitry V. Kosynkin ,  Amanda Higginbotham ,  Brandi Katherine Price

    发明人： James M. Tour ,  Dmitry V. Kosynkin ,  Amanda Higginbotham ,  Brandi Katherine Price

    IPC分类号： D01F9/12 ,  C01B31/00 ,  C08F290/14

    CPC分类号： C01B31/0446 ,  B82Y30/00 ,  B82Y40/00 ,  C01B32/184 ,  C01B32/194 ,  C01B32/23 ,  C01B2204/06 ,  H01J9/025 ,  Y10S977/734 ,  Y10S977/842

    摘要： Methods for producing macroscopic quantities of oxidized graphene nanoribbons are disclosed herein. The methods include providing a plurality of carbon nanotubes and reacting the plurality of carbon nanotubes with at least one oxidant to form oxidized graphene nanoribbons. The at least one oxidant is operable to longitudinally open the carbon nanotubes. In some embodiments, the reacting step takes place in the presence of at least one acid. In some embodiments, the reacting step takes place in the presence of at least one protective agent. Various embodiments of the present disclosure also include methods for producing reduced graphene nanoribbons by reacting oxidized graphene nanoribbons with at least one reducing agent. Oxidized graphene nanoribbons, reduced graphene nanoribbons and compositions and articles derived therefrom are also disclosed herein.

    摘要翻译： 本文公开了生产宏观量的氧化石墨烯纳米带的方法。 所述方法包括提供多个碳纳米管并使多个碳纳米管与至少一种氧化剂反应以形成氧化石墨烯纳米带。 至少一种氧化剂可操作以纵向打开碳纳米管。 在一些实施方案中，反应步骤在至少一种酸的存在下进行。 在一些实施方案中，反应步骤在至少一种保护剂的存在下进行。 本公开的各种实施方案还包括通过使氧化石墨烯纳米带与至少一种还原剂反应来生产还原的石墨烯纳米带的方法。 氧化石墨烯纳米带，还原石墨烯纳米带以及由其衍生的组合物和制品也在本文中公开。

    METHODS FOR PREPARATION OF GRAPHENE NANORIBBONS FROM CARBON NANOTUBES AND COMPOSITIONS, THIN FILMS AND DEVICES DERIVED THEREFROM
    6.
    发明申请
    METHODS FOR PREPARATION OF GRAPHENE NANORIBBONS FROM CARBON NANOTUBES AND COMPOSITIONS, THIN FILMS AND DEVICES DERIVED THEREFROM 审中-公开
    从碳纳米管和组合物制备石墨纳米颗粒的方法，薄膜和其衍生的器件

    公开(公告)号：US20140120024A1

    公开(公告)日：2014-05-01

    申请号：US14148159

    申请日：2014-01-06

    申请人： James M. Tour ,  Dmitry V. Kosynkin ,  Amanda Dugue ,  Brandi Katherine Price-Hoelscher

    发明人： James M. Tour ,  Dmitry V. Kosynkin ,  Amanda Dugue ,  Brandi Katherine Price-Hoelscher

    IPC分类号： C01B31/04

    CPC分类号： C01B32/184 ,  B82Y30/00 ,  B82Y40/00 ,  C01B32/194 ,  C01B32/23 ,  C01B2204/06 ,  C04B14/024 ,  H01J9/025 ,  Y10S977/734 ,  Y10S977/842

    摘要： Methods for producing macroscopic quantities of oxidized graphene nanoribbons are disclosed herein. The methods include providing a plurality of carbon nanotubes and reacting the plurality of carbon nanotubes with at least one oxidant to form oxidized graphene nanoribbons. The at least one oxidant is operable to longitudinally open the carbon nanotubes. In some embodiments, the reacting step takes place in the presence of at least one acid. In some embodiments, the reacting step takes place in the presence of at least one protective agent. Various embodiments of the present disclosure also include methods for producing reduced graphene nanoribbons by reacting oxidized graphene nanoribbons with at least one reducing agent. Oxidized graphene nanoribbons, reduced graphene nanoribbons and compositions and articles derived therefrom are also disclosed herein.

    摘要翻译： 本文公开了生产宏观量的氧化石墨烯纳米带的方法。 所述方法包括提供多个碳纳米管并使多个碳纳米管与至少一种氧化剂反应以形成氧化石墨烯纳米带。 至少一种氧化剂可操作以纵向打开碳纳米管。 在一些实施方案中，反应步骤在至少一种酸的存在下进行。 在一些实施方案中，反应步骤在至少一种保护剂的存在下进行。 本公开的各种实施方案还包括通过使氧化石墨烯纳米带与至少一种还原剂反应来生产还原的石墨烯纳米带的方法。 氧化石墨烯纳米带，还原石墨烯纳米带以及由其衍生的组合物和制品也在本文中公开。

    Methods for Preparation of Graphene Nanoribbons From Carbon Nanotubes and Compositions, Thin Films and Devices Derived Therefrom
    9.
    发明申请
    Methods for Preparation of Graphene Nanoribbons From Carbon Nanotubes and Compositions, Thin Films and Devices Derived Therefrom 有权
    从碳纳米管和组合物制备石墨烯纳米带的方法，衍生自其的薄膜和器件

    公开(公告)号：US20100105834A1

    公开(公告)日：2010-04-29

    申请号：US12544017

    申请日：2009-08-19

    申请人： James M. Tour ,  Dmitry V. Kosynkin ,  Amanda Higginbotham ,  Brandi Katherine Price

    发明人： James M. Tour ,  Dmitry V. Kosynkin ,  Amanda Higginbotham ,  Brandi Katherine Price

    IPC分类号： C08F301/00 ,  D01F9/12 ,  C01B31/00 ,  C01B21/082

    CPC分类号： C01B31/0446 ,  B82Y30/00 ,  B82Y40/00 ,  C01B32/184 ,  C01B32/194 ,  C01B32/23 ,  C01B2204/06 ,  H01J9/025 ,  Y10S977/734 ,  Y10S977/842

    摘要： Methods for producing macroscopic quantities of oxidized graphene nanoribbons are disclosed herein. The methods include providing a plurality of carbon nanotubes and reacting the plurality of carbon nanotubes with at least one oxidant to form oxidized graphene nanoribbons. The at least one oxidant is operable to longitudinally open the carbon nanotubes. In some embodiments, the reacting step takes place in the presence of at least one acid. In some embodiments, the reacting step takes place in the presence of at least one protective agent. Various embodiments of the present disclosure also include methods for producing reduced graphene nanoribbons by reacting oxidized graphene nanoribbons with at least one reducing agent. Oxidized graphene nanoribbons, reduced graphene nanoribbons and compositions and articles derived therefrom are also disclosed herein.

    摘要翻译： 本文公开了生产宏观量的氧化石墨烯纳米带的方法。 所述方法包括提供多个碳纳米管并使多个碳纳米管与至少一种氧化剂反应以形成氧化石墨烯纳米带。 至少一种氧化剂可操作以纵向打开碳纳米管。 在一些实施方案中，反应步骤在至少一种酸的存在下进行。 在一些实施方案中，反应步骤在至少一种保护剂的存在下进行。 本公开的各种实施方案还包括通过使氧化石墨烯纳米带与至少一种还原剂反应来生产还原的石墨烯纳米带的方法。 氧化石墨烯纳米带，还原石墨烯纳米带以及由其衍生的组合物和制品也在本文中公开。