Apparatus and method for preparation of compounds or intermediates thereof from a solid material, and using such compounds and intermediates
    10.
    发明授权
    Apparatus and method for preparation of compounds or intermediates thereof from a solid material, and using such compounds and intermediates 有权
    从固体材料制备化合物或其中间体的装置和方法,以及使用这些化合物和中间体

    公开(公告)号:US09205392B2

    公开(公告)日:2015-12-08

    申请号:US13219706

    申请日:2011-08-28

    摘要: An apparatus is described, as including a reaction region for contacting a reactant gas with a reactive solid under conditions effective to form an intermediate product, and an opening for allowing an unreacted portion of the gaseous reagent and the intermediate product to exit the reaction region. The apparatus can be beneficially employed to form a final product as a reaction product of the intermediate product and the reactant gas. The reaction of the reactant gas and reactive solid can be conducted in a first reaction zone, with the reaction of the reactant gas and intermediate product conducted in a second reaction zone. In a specific implementation, the reaction of the reactant gas and intermediate product is reversible, and the reactant gas and intermediate product are flowed to the second reaction zone at a controlled rate or in a controlled manner, to suppress back reaction forming the reactive solid.

    摘要翻译: 描述了一种装置,其包括用于在有效形成中间产物的条件下使反应气体与反应性固体接触的反应区域,以及允许气态试剂和中间产物的未反应部分离开反应区域的开口。 该设备可以有利地用于形成作为中间产物和反应气体的反应产物的最终产物。 反应气体和反应性固体的反应可以在第一反应区进行,反应气体和中间产物的反应在第二反应区中进行。 在具体实施方案中,反应气体和中间产物的反应是可逆的,并且反应物气体和中间产物以受控的速率或受控的方式流到第二反应区,以抑制形成反应性固体的反应。