摘要:
A pyridine-compound is reacted with fluorine together with a Bronsted acid-compound or Lewis acid to form a N-fluoropyridinium salt which is very active to other compounds but is very selective for the preparation of a desired product and this product is very useful for a fluorine-introducing agent which makes it useful for the preparation of fluoro-compounds such as thyroid inhibitor.
摘要:
A pyridine-compound is reacted with fluorine together with a .[.Bronsted.]. .Iadd.Bronsted .Iaddend.acid-compound or Lewis acid to form a N-fluoropyridinium salt which is very active to other compounds but is very selective for the preparation of a desired product and this product is very useful for a fluorine-introducing agent which makes it useful for the preparation of fluoro-compounds such as thyroid inhibitor.
摘要:
In the purification of crude tetrachlorophthalic anhydride containing hexachlorobenzene as impurities, this invention relates to purification by decomposition in which crude tetrachlorophthalic anhydride is contacted with chlorine gas in fuming sulfuric acid or sulfuric anhydride in the presence of iodine or iodine trichloride to decompose the impurities and remove them or purification by washing in which hexachlorobenzene is separated by washing with a chlorinated solvent. This invention also relates to a process for purifying crude tetrachlorophthalic anhydride containing iodotrichlorophthalic anhydrides as impurities by applying a radical reaction treatment in a chlorinated solvent to convert iodotrichlorophthalic anhydrides to tetrachlorophthalic anhydride. Moreover, it relates to high-purity tetrachlorophthalic anhydride containing 10 ppm or less of hexachlorobenzene. With the process of this invention, it is possible to recover high-purity tetrachlorophthalic anhydride with extremely low contents of impurities readily in high yield.
摘要:
A method of determining the reliability of long-term predicted orbit data, includes: determining the reliability of long-term predicted orbit data, which is acquired by predicting a satellite orbit in a target period of at least one day, using predicted position data including predicted positions of a positioning satellite in time series and actual position data including actual positions of the positioning satellite corresponding to the predicted positions.
摘要:
The invention provides a high-yield method for producing onium salt derivatives useful as agents, such as acid-generators, employed in chemically amplified resists; and to provide novel onium salt derivatives. Reaction of an onium salt derivative containing a halide anion or a carboxylate anion with a sulfonic acid ester derivative or a phosphoric acid derivative provides an onium sulfate derivative or an onium phosphate derivative at high yield.
摘要:
A method for providing satellite orbit ephemeris includes: determining a positioning satellite in view of a reference position; and providing to a positioning device a satellite orbit ephemeris of the positioning satellite in view of the reference position, the satellite orbit ephemeris being valid for at least one day.
摘要:
A method for providing satellite orbit ephemeris includes: determining a positioning satellite in view of a reference position; and providing to a positioning device a satellite orbit ephemeris of the positioning satellite in view of the reference position, the satellite orbit ephemeris being valid for at least one day.
摘要:
The invention provides a high-yield method for producing onium salt derivatives useful as agents, such as acid-generators, employed in chemically amplified resists; and to provide novel onium salt derivatives. Reaction of an onium salt derivative containing a halide anion or a carboxylate anion with a sulfonic acid ester derivative or a phosphoric acid derivative provides an onium sulfate derivative or an onium phosphate derivative at high yield.
摘要:
The invention provides a high-yield method for producing onium salt derivatives useful as agents, such as acid-generators, employed in chemically amplified resists; and to provide novel onium salt derivatives. Reaction of an onium salt derivative containing a halide anion or a carboxylate anion with a sulfonic acid ester derivative or a phosphoric acid derivative provides an onium sulfate derivative or an onium phosphate derivative at high yield.