Method for producing a glass ceramic having a garnet phase
    11.
    发明授权
    Method for producing a glass ceramic having a garnet phase 有权
    具有石榴石相的玻璃陶瓷的制造方法

    公开(公告)号:US07958746B2

    公开(公告)日:2011-06-14

    申请号:US11757609

    申请日:2007-06-04

    IPC分类号: C03C10/00

    摘要: The invention proposes a method for producing glass ceramics which is particularly well suited as light conversion material, especially for down conversion. One initially produces a starting glass, containing (on an oxide basis) 5-50% by weight of SiO2, 5-50% by weight of Al2O3 and 10-80% by weight of at least one oxide selected from the from the group formed by Y2O3, Lu2O3, Sc2O3, Gd2O3, Yb2O3, Ce2O3, as well as 0.1-30% by weight of at least one oxide selected from the group formed by B2O3, Th2O3, and oxides of the lanthanoids, except Lu2O3, Gd2O3, Yb2O3, Ce2O3. Thereafter, the material is heated up for ceramization at a heating rate of at least 100 K/min to a temperature in the range of between 1000° C. to 1400° C. until crystallites are formed that contain a garnet phase. Thereafter, the material is cooled down to room temperature. Alternatively, controlled cooling-down from the molten state is possible.

    摘要翻译: 本发明提出一种特别适合作为光转换材料的玻璃陶瓷的制造方法,特别是用于下转换。 最初产生起始玻璃,其含有5-50重量%的SiO 2,5-50重量%的Al 2 O 3和10-80重量%的至少一种氧化物的起始玻璃,所述氧化物选自由Y 2 O 3 ,Lu 2 O 3,Sc 2 O 3,Gd 2 O 3,Yb 2 O 3,Ce 2 O 3,以及选自B 2 O 3,Th 2 O 3的至少一种氧化物和除了Lu 2 O 3,Gd 2 O 3,Yb 2 O 3,Ce 2 O 3以外的镧系元素的氧化物的至少一种氧化物。 此后,将材料以至少100K /分钟的加热速率加热至陶瓷化,至1000℃至1400℃的温度,直至形成含有石榴石相的微晶。 此后,将材料冷却至室温。 或者,可以从熔融状态控制冷却。

    METHOD FOR GENERATING A GLASS CERAMIC COMPOSITE STRUCTURE
    12.
    发明申请
    METHOD FOR GENERATING A GLASS CERAMIC COMPOSITE STRUCTURE 有权
    生成玻璃陶瓷复合结构的方法

    公开(公告)号:US20110091730A1

    公开(公告)日:2011-04-21

    申请号:US12941262

    申请日:2010-11-08

    IPC分类号: B32B17/06 B29C65/14

    摘要: A method for making glass ceramic composite structures, wherein a first and at least a second glass component, with an intermediate layer of a joining solder consisting of glass placed between them, are assembled to form a raw composite structure, wherein the joining solder has a radiation absorption capacity higher than the components to be joined, and wherein the raw composite structure is irradiated with energy, for example IR energy, at least in the area of the joining solder until the joining solder has softened sufficiently to bond together the components and the joining solder to produce a composite glassy structure. Thereafter a ceramization treatment is performed.

    摘要翻译: 一种制造玻璃陶瓷复合结构的方法,其中组装具有由设置在它们之间的玻璃组成的接合焊料的中间层的第一和至少第二玻璃组分以形成原始复合结构,其中所述接合焊料具有 辐射吸收能力高于要接合的组分,并且其中原始复合结构至少在接合焊料的区域中被照射能量,例如IR能量,直到接合焊料充分软化以将组分粘合在一起 连接焊料以产生复合玻璃结构。 然后进行陶瓷化处理。

    Process of producing a glass-ceramic, the glass-ceramic made therby and its uses
    14.
    发明申请
    Process of producing a glass-ceramic, the glass-ceramic made therby and its uses 有权
    制造玻璃陶瓷的方法,玻璃陶瓷制成及其用途

    公开(公告)号:US20090215605A1

    公开(公告)日:2009-08-27

    申请号:US12392408

    申请日:2009-02-25

    IPC分类号: C03C10/00

    摘要: The process of making the glass-ceramic includes ceramicizing a starting glass at a heating or cooling rate during the ceramicization of at least 10 K/min, so that the glass-ceramic contains at least 50% by volume of ferroelectric crystallites with a maximum diameter of from 20 to 100 nm and not more than 10% by volume of nonferroelectric crystallitesis. The glass ceramic produced by the process contains no pores or not more than 0.01% by volume of the pores and a value of e′·V2max of the glass-ceramic is at least 20 (MV/cm)2, wherein e′ is the dielectric constant at 1 kHz and Vmax is the breakdown voltage per unit thickness. The ferroelectric crystallites preferably have a perovskite structure and are composed of substantially pure or doped BaTiO3 and/or BaTi2O5.

    摘要翻译: 制造玻璃陶瓷的过程包括在至少10K /分钟的陶瓷化过程中以加热或冷却速率陶瓷起始玻璃,使得玻璃陶瓷含有至少50体积%的具有最大直径的铁电微晶 为20〜100nm且不大于10体积%的非铁电晶体。 由该方法制造的玻璃陶瓷不含孔或不大于0.01体积%的孔,玻璃陶瓷的e'.V2max的值为至少20(MV / cm)2,其中e'为 介电常数为1 kHz,Vmax为每单位厚度的击穿电压。 铁电晶体优选具有钙钛矿结构,并且由基本上纯的或掺杂的BaTiO 3和/或BaTi 2 O 5构成。

    METHOD FOR PRODUCING A GLASS CERAMIC HAVING A GARNET PHASE
    15.
    发明申请
    METHOD FOR PRODUCING A GLASS CERAMIC HAVING A GARNET PHASE 有权
    用于生产具有GARNET相的玻璃陶瓷的方法

    公开(公告)号:US20080041106A1

    公开(公告)日:2008-02-21

    申请号:US11757609

    申请日:2007-06-04

    IPC分类号: C03B27/012 C03C10/00

    摘要: The invention proposes a method for producing glass ceramics which is particularly well suited as light conversion material, especially for down conversion. One initially produces a starting glass, containing (on an oxide basis) 5-50% by weight of SiO2, 5-50 % by weight of Al2O3 and 10-80% by weight of at least one oxide selected from the from the group formed by Y2O3, Lu2O3, Sc2O3, Gd2O3, Yb2O3, Ce2O3, as well as 0.1-30% by weight of at least one oxide selected from the group formed by B2O3, Th2O3, and oxides of the lanthanoids, except Lu2O3, Gd2O3, Yb2O3, Ce2O3. Thereafter, the material is heated up for ceramization at a heating rate of at least 100 K/min to a temperature in the range of between 1000° C. to 1400° C. until crystallites are formed that contain a garnet phase. Thereafter, the material is cooled down to room temperature. Alternatively, controlled cooling-down from the molten state is possible.

    摘要翻译: 本发明提出一种特别适合作为光转换材料的玻璃陶瓷的制造方法,特别是用于下转换。 最初产生起始玻璃,其含有(以氧化物为基准)5-50重量%的SiO 2,5-50重量%的Al 2 O 3 > 3重量%和10-80重量%的至少一种氧化物,其选自Y 2 N 3 O 3,Lu 2 3 3 3,3 3 3 3 ,Yb 2 O 3,Ce 2 O 3,以及0.1-30重量%的 选自由B 2 O 3 O 3,Th 2 O 3 3形成的基团中的至少一种氧化物和氧化物 的镧系元素,除了Lu 2 O 3 3,Gd 2 O 3 N 3,Yb 2, 3个O 3,3个O 3,3个O 3。 此后,将材料以至少100K /分钟的加热速率加热至陶瓷化,至1000℃至1400℃的温度,直至形成含有石榴石相的微晶。 此后,将材料冷却至室温。 或者,可以从熔融状态控制冷却。

    Pusher centrifuge
    19.
    发明授权
    Pusher centrifuge 失效
    推动式离心机

    公开(公告)号:US4217226A

    公开(公告)日:1980-08-12

    申请号:US956421

    申请日:1978-10-31

    IPC分类号: B04B3/02 B01D33/10 B01D35/16

    CPC分类号: B04B3/02

    摘要: Pusher centrifuge having a pusher plate and a guiding wall for the mixture to be fed onto the centrifuge drum, with a free flow space between the pusher plate and the guiding wall; the improvement that the surfaces of the pusher plate and guiding wall facing the mixture to be fed extend at least substantially perpendicular to the axis of the centrifuge drum or extend away from the axis of the drum in the radial area which extends from the outer surface of the inlet pipe to the inner surface of the layer of mixture lying on the drum.

    摘要翻译: 推进式离心机具有推动板和引导壁,用于将混合物供给到离心机滚筒上,推动板与引导壁之间具有自由流动空间; 推进板的表面和面向要进料的混合物的导向壁的表面的改进至少基本上垂直于离心机滚筒的轴线延伸,或者在从径向区域延伸的径向区域中延伸离开滚筒的轴线,该径向区域从 入口管到位于鼓上的混合物层的内表面。