PHLEGMATIZED METAL POWDER OR ALLOY POWDER AND METHOD AND REACTION VESSEL FOR THE PRODUCTION THEREOF
    275.
    发明申请
    PHLEGMATIZED METAL POWDER OR ALLOY POWDER AND METHOD AND REACTION VESSEL FOR THE PRODUCTION THEREOF 有权
    有色金属粉末或合金粉末及其生产方法和反应容器

    公开(公告)号:US20100272999A1

    公开(公告)日:2010-10-28

    申请号:US12746985

    申请日:2009-01-08

    Abstract: A method and a device are described for the production of metal powder or alloy powder of a moderate grain sizes less than 10 μm, comprising or containing at least one of the reactive metals zirconium, titanium, or hafnium, by metallothermic reduction of oxides or halogenides of the cited reactive metals with the aid of a reducing metal, wherein said metal powder or alloy powder is phlegmatized by adding a passivating gas or gas mixture during and/or after the reduction of the oxides or halogenides and/or is phlegmatized by adding a passivating solid before the reduction of the oxides or halogenides, wherein both said reduction and also said phlegmatization are performed in a single gas-tight reaction vessel which can be evacuated.

    Abstract translation: 描述了通过金属热还原氧化物或卤化物来生产中等粒度小于10μm的金属粉末或合金粉末的方法和装置,其包含或含有至少一种活性金属锆,钛或铪 的所述反应性金属,其中所述金属粉末或合金粉末通过在氧化物或卤化物还原期间和/或之后添加钝化气体或气体混合物和/或通过加入钝化气体或气体混合物而被钝化 在还原氧化物或卤化物之前钝化固体,其中所述还原和所述钝化都在可以抽空的单个气密反应容器中进行。

    PROCESS OF MANUFACTURING NANO-SCALE POWDERS
    276.
    发明申请
    PROCESS OF MANUFACTURING NANO-SCALE POWDERS 有权
    制造纳米鳞片粉的工艺

    公开(公告)号:US20100242680A1

    公开(公告)日:2010-09-30

    申请号:US12813106

    申请日:2010-06-10

    Applicant: WEI WU

    Inventor: WEI WU

    CPC classification number: B22F9/26 B22F1/0011 B22F2999/00 B22F2201/013

    Abstract: A process for synthesizing metal submicron and nano-scale powders for use in articles of manufacture. In a suitable reactor, single metal or multiple metal complexes are heated to a temperature whereby, upon contact with hydrogen gas, an exothermic reaction begins. The further temperature rise in response to the exothermic reaction is minimized by reducing the external heat input, thereby minimizing the agglomeration or sintering of the metal nano-scale particles resulting from the process. Preferably, after drawing a vacuum on the metal complexes in the reactor, the hydrogen is introduced at about, equal to or below ambient pressure and the reaction is purposely made slow to prevent agglomeration or sintering.

    Abstract translation: 用于合成用于制造制品的金属亚微米和纳米级粉末的方法。 在合适的反应器中,将单一金属或多种金属络合物加热到一个温度,由此在与氢气接触时开始放热反应。 通过减少外部热量输入来减小响应于放热反应的进一步温度升高,从而最小化由该方法产生的金属纳米尺度颗粒的聚集或烧结。 优选地,在反应器中的金属配合物上抽真空之后,在约等于或低于环境压力下引入氢气,并且有意地使反应缓慢以防止附聚或烧结。

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