Abstract:
The invention relates to a method of preparing a particle-based composition, comprising: (i) bringing into contact a mixture comprising a dendritic structure and a metal compound precursor in a fluid, under temperature and pressure conditions such that the mixture is not soluble in the fluid; and (ii) chemically converting the metal compound precursor.
Abstract:
The process for producing, processing, sintering, pressing or extruding thermoelectric materials with heat treatment under inert gas or under reduced pressure at temperatures in the range from 100 to 900° C. comprises producing, processing, sintering, pressing or extruding in the presence of oxygen scavengers which form thermodynamically stable oxides in the presence of free oxygen under the production, processing, sintering, pressing or extrusion conditions and hence keep free oxygen away from the thermoelectric material.
Abstract:
Suppression or enhancement of various properties of a liquid fluid is aimed by improving uniform dispersion of nanoparticles by means of making a state in which no oxidized film exists on the surfaces of the nanoparticles to be dispersed in the liquid fluid. The location of the liquid fluid is confirmed with ease by enhancing the brightness of light emission of the fluid through uniform dispersion of the nanoparticles in the liquid fluid containing a material having a flame reaction. In this way, as to liquid fluids utilized in various industries, it is possible to offer a technology to desirably enhance or suppress a property desired to be enhanced and a property desired to be suppressed among various properties that its constituents have.
Abstract:
A process is described for preparing cubic metallic nanoparticles, comprising: preparing an aqueous solution containing a source of a metal from group VIII, a reducing agent R1 and a stabilizer; preparing an aqueous solution containing a source of a group VIII metal and a stabilizer at a temperature strictly higher than 70° C. and less than or equal to 80° C.; mixing at least a portion of the aqueous solution obtained in step a) with the aqueous solution obtained in step b) to obtain, in the presence of a reducing agent R2, metallic nanoparticles in the cubic form representing at least 70% by number of the entire quantity of metallic nanoparticles which are formed; depositing said metallic nanoparticles derived from step c) on a support.
Abstract:
A method and a device are described for the production of metal powder or alloy powder of a moderate grain sizes less than 10 μm, comprising or containing at least one of the reactive metals zirconium, titanium, or hafnium, by metallothermic reduction of oxides or halogenides of the cited reactive metals with the aid of a reducing metal, wherein said metal powder or alloy powder is phlegmatized by adding a passivating gas or gas mixture during and/or after the reduction of the oxides or halogenides and/or is phlegmatized by adding a passivating solid before the reduction of the oxides or halogenides, wherein both said reduction and also said phlegmatization are performed in a single gas-tight reaction vessel which can be evacuated.
Abstract:
A process for synthesizing metal submicron and nano-scale powders for use in articles of manufacture. In a suitable reactor, single metal or multiple metal complexes are heated to a temperature whereby, upon contact with hydrogen gas, an exothermic reaction begins. The further temperature rise in response to the exothermic reaction is minimized by reducing the external heat input, thereby minimizing the agglomeration or sintering of the metal nano-scale particles resulting from the process. Preferably, after drawing a vacuum on the metal complexes in the reactor, the hydrogen is introduced at about, equal to or below ambient pressure and the reaction is purposely made slow to prevent agglomeration or sintering.
Abstract:
An improved method of reducing a mixed metal oxide composition comprising oxides of nickel, cobalt, copper and iron in a hydrogen atmosphere to produce a mixture of the respective metals, the improvement wherein the atmosphere further comprises water vapour at a concentration, temperature and time to effect selective reduction of the oxides of nickel cobalt and copper relative to the iron oxide to produce the metallic mixture having a reduced ratio of metallic iron relative to metallic nickel, cobalt and copper.
Abstract:
Semi-finished or finished parts are made from a molybdenum alloy with intermetallic phases, preferably molybdenum-silicide, molybdenum-boron-silicide, optionally also molybdenum-boride phases. Starting from mechanically alloyed powder, hot compacted material exhibits superplastic forming behavior. It is thus possible to lower the forming temperature by at least 300° C., thus permitting processing on conventional plants.
Abstract:
The disclosure relates to a method for production of a component, such as a contact piece, for a switchgear assembly. To introduce a slot and apply a contact outer contour directly during the powder-metallurgical production process of the contact material, contouring in the form of a slot or slots is introduced into the powder-metal material, which is located in a mold, essentially in a direction parallel to a normal to a surface of the component, to form the component with a slot.
Abstract:
A process for preparing carbon and magnesium including composites, includes: a) contacting a carbon material including pores of which at least 30%, based on the total number of pores, have a pore diameter in the range 0.1 to 10×10−9 m with a molten metallic magnesium or magnesium alloy to obtain a intermediate composite; and b) cooling the intermediate composite to obtain a carbon and magnesium including composite. Also described is a carbon and magnesium including composite obtainable by the process of the invention, the use of a carbon and magnesium including composite obtainable by the process and a hydrogen storage system.