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    Process for producing secondary alkyl primary amines from n-paraffin
    22.
    发明授权
    Process for producing secondary alkyl primary amines from n-paraffin 失效
    从正链烷烃制备仲烷基伯胺的方法

    公开(公告)号：US4025561A

    公开(公告)日：1977-05-24

    申请号：US652582

    申请日：1976-01-26

    Applicant: Robert M. Suggitt ,  Walter C. Gates, Jr.

    Inventor： Robert M. Suggitt ,  Walter C. Gates, Jr.

    IPC: B01J23/58 ,  B01J23/78 ,  B01J23/84 ,  C10G45/04 ,  C07C85/11

    CPC classification number: C10G45/04 ,  B01J23/58 ,  B01J23/78 ,  B01J23/84

    Abstract: A process for converting mixtures of C.sub.6 to C.sub.30 n-paraffin and n-paraffin by-products to substantially pure n-paraffin which comprises catalytically hydrogenating the mixture at a temperature of from about 600.degree. to 750.degree. F. in the presence of a Group VIII metal on alumina catalyst where the catalyst contains from about 0.05 to 2.0 weight percent of an alkali metal oxide or alkaline earth metal oxide or thallous oxide. The catalyst can additionally contain a Group VIB or VIIB metal.

    Abstract translation: 将C6至C30正链烷烃和正链烷烃副产物的混合物转化为基本上纯的正链烷烃的方法，该方法包括在组合存在下在约600至750°F的温度下催化氢化混合物 Ⅷ金属在氧化铝催化剂上，其中催化剂含有约0.05至2.0重量％的碱金属氧化物或碱土金属氧化物或氧化铊。 催化剂还可以含有VIB族或VIIB族金属。

    Preparative process for preparing phenylenediacetate diesters
    23.
    发明授权
    Preparative process for preparing phenylenediacetate diesters 失效
    制备苯二乙酸二酯的制备方法

    公开(公告)号：US4016194A

    公开(公告)日：1977-04-05

    申请号：US616227

    申请日：1975-09-24

    Applicant: John F. Knifton ,  Robert M. Suggitt

    Inventor： John F. Knifton ,  Robert M. Suggitt

    IPC: C07C69/614 ,  C07C69/76

    CPC classification number: C07C69/614

    Abstract: This invention relates to the catalytic carbonylation of .alpha.,.alpha.'-dihaloxylenes to phenylenediacetate diesters by the catalytic insertion of carbon monoxide into the carbon-halogen bonds of said .alpha.,.alpha.'-dihaloxylenes in the presence of alkanols. The catalysts used in this novel process are two component homogeneous ligand-stabilized palladium(II) and nickel(II) halide complexes wherein said stabilizing ligands each contain at least one Group VB or VIB donor atom such as phosphorus, which is bonded to one or more aromatic and/or aliphatic radicals.

    Abstract translation: 本发明涉及通过在烷醇存在下将一氧化碳催化插入所述α，α'-二卤代烯烃的碳 - 卤素键来将α，α'-二卤代氧化物催化羰基化成亚苯基二乙酸酯二酯。 在该新方法中使用的催化剂是双组分均匀配体稳定的钯（II）和卤化镍（II）络合物，其中所述稳定配体各自含有至少一个VB族或VIB族供体原子，例如磷，其结合到一个或多个 更多的芳族和/或脂族基团。

    Partial oxidation process for producing a stream of hot purified gas
    25.
    发明授权
    Partial oxidation process for producing a stream of hot purified gas 失效
    用于生产热纯净气体流的部分氧化工艺

    公开(公告)号：US5403366A

    公开(公告)日：1995-04-04

    申请号：US77269

    申请日：1993-06-17

    Applicant: Thomas F. Leininger ,  Allen M. Robin ,  James K. Wolfenbarger ,  Robert M. Suggitt

    Inventor： Thomas F. Leininger ,  Allen M. Robin ,  James K. Wolfenbarger ,  Robert M. Suggitt

    IPC: C01B3/36 ,  C01B3/50 ,  C10J3/00 ,  C10J3/46 ,  C10K1/20 ,  C10K1/32 ,  C10K1/34

    CPC classification number: C10J3/466 ,  C10J3/06 ,  C10J3/463 ,  C10J3/485 ,  C10K1/002 ,  C10K1/024 ,  C10K1/026 ,  C10K1/101 ,  C10K1/20 ,  C10K3/02 ,  C10K3/04 ,  C10J2300/1223 ,  C10J2300/1606 ,  C10J2300/1656 ,  C10J2300/1662 ,  C10J2300/1665 ,  C10J2300/1671 ,  C10J2300/1884

    Abstract: A partial oxidation process for the production of a stream of hot clean gas substantially free from particulate matter, alkali metal compounds, hydrogen halides, hydrogen cyanide, sulfur-containing gases, and with or without ammonia for use as synthesis gas, reducing gas, or fuel gas. A pumpable hydrocarbonaceous fuel selected from the group consisting of liquid hydrocarbonaceous fuel or liquid emulsions thereof, an aqueous slurry of petroleum coke, and mixtures thereof and wherein said hydrocarbonaceous fuel contains halides, alkali metal compounds, sulfur, nitrogen and inorganic ash containing components, is reacted in a gasifier by partial oxidation to produce a hot raw gas stream comprising H.sub.2, CO, CO.sub.2, H.sub.2 O, CH.sub.4, NH.sub.3, HCN, HCl, HF, H.sub.2 S, COS, N.sub.2, Ar, particulate matter, vapor phase alkali metal compounds, and molten slag. The hot raw gas stream from the gasifier is cooled in a radiant cooler and cleaned. Optionally, ammonia is removed from the gas stream by being catalytically disproportionated into N.sub.2 and H.sub.2. The process gas stream is cooled and halides and HCN in the gas stream are reacted with a supplementary alkali metal compound to remove HCl, HF and HCN. Alkali metal halides and alkali metal cyanide, vaporized alkali metal compounds and residual fine particulate matter are removed from the gas stream by further cooling and filtering. The sulfur-containing gases in the process gas stream are then reacted at high temperature with a regenerable sulfur-reactive mixed metal oxide sulfur sorbent material to produce a sulfided sorbent material which is then separated from the hot clean purified gas stream having a temperature of at least 1000.degree. F.

    Abstract translation: 用于生产基本上不含颗粒物质，碱金属化合物，卤化氢，氰化氢，含硫气体以及用于或不用氨的热清洁气体流的部分氧化方法用作合成气，还原气体或 燃气。 选自液体烃类燃料或其液体乳液，石油焦炭的水性浆料及其混合物的可泵送烃类燃料，其中所述含烃燃料包含卤化物，碱金属化合物，硫，氮和含无机灰分的组分，是 在气化器中通过部分氧化反应产生包含H 2，CO，CO 2，H 2 O，CH 4，NH 3，HCN，HCl，HF，H 2 S，COS，N 2，Ar，颗粒物质，气相碱金属化合物， 和熔渣。 来自气化器的热原料气流在辐射冷却器中冷却并清洁。 任选地，通过催化歧化成N 2和H 2从气流中除去氨。 将工艺气流冷却并将卤化物和气流中的HCN与补充的碱金属化合物反应以除去HCl，HF和HCN。 通过进一步的冷却和过滤，将碱金属卤化物和碱金属氰化物，汽化的碱金属化合物和残留的细颗粒物质从气流中除去。 然后，工艺气体流中的含硫气体在高温下与可再生的硫反应性混合金属氧化物硫吸附剂材料反应以产生硫化吸附剂材料，然后将其从具有温度为 至少1000°F

    Production of demercurized synthesis gas, reducing gas, or fuel gas
    28.
    发明授权
    Production of demercurized synthesis gas, reducing gas, or fuel gas 失效
    生产脱气合成气，还原气或燃气

    公开(公告)号：US4863489A

    公开(公告)日：1989-09-05

    申请号：US305588

    申请日：1989-02-03

    Applicant: Robert M. Suggitt

    Inventor： Robert M. Suggitt

    IPC: C10J3/46

    CPC classification number: C10J3/485 ,  C10J3/84 ,  C10K1/007 ,  C10K1/04 ,  C10K1/08 ,  C10K1/101 ,  C10K1/32 ,  C10J2300/1223 ,  C10J2300/1846 ,  C10J2300/1884

    Abstract: A process for the production of demercurized synthesis gas, reducing gas or fuel gas. Mercury-containing fossil fuels e.g. coal were reacted by partial oxidation to produce gaseous mixtures comprising H.sub.2, CO, H.sub.2 O, CO.sub.2, H.sub.2 S, COS, entrained slag and/or ash, mercury vapor, and optionally CH.sub.4, NH.sub.3, N.sub.2 and Ar. Unexpectedly, the mercury vapor was produced in the reaction zone; and it was found to be thermodynamically stable even in the presence of H.sub.2 S under the strong reducing conditions that prevailed in the gas generator. No new sulfides of mercury were formed. The mercury vapors were removed from the main body of the process gas stream in a pressurized solvent scrubber at a relatively low temperature. By this means, the mercury vapor was condensed and simultaneously the mercury and sulfur contents of the clean process gas stream were reduced to low levels. In one embodiment, the last vestiges of mercury were removed from the demercurized product gas stream by carbon sorption.

    Method of producing n-paraffin oximes
    30.
    发明授权
    Method of producing n-paraffin oximes 失效
    生产正链烷肟的方法

    公开(公告)号：US3993554A

    公开(公告)日：1976-11-23

    申请号：US652585

    申请日：1976-01-26

    Applicant: Robert M. Suggitt ,  Walter C. Gates, Jr.

    Inventor： Robert M. Suggitt ,  Walter C. Gates, Jr.

    IPC: B01J23/58 ,  B01J23/78 ,  B01J23/80 ,  B01J23/84 ,  C10G45/04 ,  B01J1/10

    CPC classification number: B01J23/84 ,  B01J23/58 ,  B01J23/78 ,  B01J23/80 ,  C10G45/04 ,  Y10S204/903

    Abstract: A process for converting mixtures of C.sub.6 to C.sub.30 n-paraffin and n-paraffin by-products to substantially pure n-paraffin which comprises catalytically hydrogenating the mixture at a temperature of from about 600.degree. to 750.degree. F. in the presence of a Group VIII metal on alumina catalyst where the catalyst contains from about 0.05 to 2.0 weight percent of an alkali metal oxide or alkaline earth metal oxide or thallous oxide. The catalyst can additionally contain a Group VIB or VIIB metal. The n-paraffin is photochemically reacted with a gaseous nitrosating agent to form paraffin oximes and by-products and the by-products are recycled for catalytic hydrogenation.

    Abstract translation: 将C6至C30正链烷烃和正链烷烃副产物的混合物转化为基本上纯的正链烷烃的方法，该方法包括在组合存在下在约600至750°F的温度下催化氢化混合物 Ⅷ金属在氧化铝催化剂上，其中催化剂含有约0.05至2.0重量％的碱金属氧化物或碱土金属氧化物或氧化铊。 催化剂还可以含有VIB族或VIIB族金属。 将正链烷烃与气态亚硝化剂光化学反应以形成链烷烃肟和副产物，副产物被再循环用于催化氢化。

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