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    Process of Producing Cyclohexylbenzene
    21.
    发明申请
    Process of Producing Cyclohexylbenzene 有权
    生产环己基苯的工艺

    公开(公告)号：US20140371498A1

    公开(公告)日：2014-12-18

    申请号：US13883742

    申请日：2011-12-02

    Applicant: Keith H. Kuechler ,  James R. Lattner ,  Christopher L. Becker ,  Jihad M. Dakka ,  Tan-Jen Chen

    Inventor： Keith H. Kuechler ,  James R. Lattner ,  Christopher L. Becker ,  Jihad M. Dakka ,  Tan-Jen Chen

    IPC: C07C2/74 ,  C07C6/12 ,  C07C5/367

    CPC classification number: C07C2/74 ,  C07C5/367 ,  C07C6/126 ,  C07C2521/08 ,  C07C2523/14 ,  C07C2523/42 ,  C07C2601/08 ,  C07C2601/14 ,  C07C13/28

    Abstract: In a process for producing cyclohexylbenzene, benzene is contacted with hydrogen under hydroalkylation conditions effective to form a first effluent stream comprising cyclohexylbenzene, cyclohexane, methylcyclopentane, and unreacted benzene. At least a portion of the first effluent stream is contacted with a dehydrogenation catalyst under dehydrogenation conditions to convert at least a portion of the cyclohexane to benzene thereby forming a second effluent stream. The amount of methylcyclopentane in the second effluent stream is different by no more than 65% of the total amount of the portion of the first effluent stream, said amounts being on a weight basis. A methylcyclopentane-containing stream is removed from either the first or the second effluent stream and at least a portion of the second effluent stream containing benzene is recycled to the hydroalkylation step.

    Abstract translation: 在生产环己基苯的方法中，苯在有效形成包含环己基苯，环己烷，甲基环戊烷和未反应苯的第一流出物流的加氢烷基化条件下与氢气接触。 在脱氢条件下，将至少一部分第一流出物流与脱氢催化剂接触以将至少一部分环己烷转化为苯，从而形成第二流出物流。 第二流出物流中的甲基环戊烷的量不同于第一流出物流的部分总量的不超过65％，所述量基于重量。 从第一或第二流出物流中除去含甲基环戊烷的物流，并将含有苯的第二流出物流的至少一部分再循环至加氢烷基化步骤。

    Process for producing cyclohexylbenzene
    25.
    发明授权
    Process for producing cyclohexylbenzene 有权
    生产环己基苯的方法

    公开(公告)号：US08519194B2

    公开(公告)日：2013-08-27

    申请号：US13145007

    申请日：2009-11-24

    Applicant: Tan-Jen Chen ,  Francisco M. Benitez ,  John S. Buchanan ,  Jane C. Cheng ,  Jon E. Stanat

    Inventor： Tan-Jen Chen ,  Francisco M. Benitez ,  John S. Buchanan ,  Jane C. Cheng ,  Jon E. Stanat

    IPC: C07C45/27 ,  C07C27/08 ,  C07C2/64 ,  C07C2/66

    CPC classification number: B01J29/7676 ,  B01J29/7476 ,  C07C2/76 ,  Y02P20/52 ,  C07C13/28

    Abstract: In a process for producing cyclohexylbenzene, benzene and hydrogen are fed to at least one reaction zone comprising a catalyst system which comprises a molecular sieve and at least one hydrogenation metal. The MCM-22 family molecular sieve having an X-ray diffraction pattern including d-spacing maxima at 12.4±0.25, 6.9±0.15, 3.57±0.07 and 3.42±0.07 Angstrom, and the hydrogenation metal is selected from the group consisting of palladium, ruthenium, nickel, zinc, tin, cobalt, and combinations of any two or more thereof. Hydroalkylation conditions of temperature and pressure are selected to produce a hydroalkylation conversion in a range of from about 15% to about 75% The benzene and hydrogen are then contacted in the at least one reaction zone under said selected hydroalkylation condition to produce an effluent containing cyclohexylbenzene.

    Abstract translation: 在生产环己基苯的方法中，将苯和氢气进料至至少一个包含催化剂体系的反应区，该催化剂体系包含分子筛和至少一种氢化金属。 具有12.4±0.25,6.9±0.15,3.57±0.07和3.42±0.07埃的d间距最大值的X射线衍射图的MCM-22族分子筛，氢化金属选自钯， 钌，镍，锌，锡，钴及其任何两种或更多种的组合。 选择温度和压力的烷基化条件以产生约15％至约75％的加氢烷基转化率。然后在所述选择的加氢烷基化条件下，使苯和氢在至少一个反应区中接触，以产生含有环己基苯 。

    Dehydrogenation Process
    28.
    发明申请
    Dehydrogenation Process 有权
    脱氢工艺

    公开(公告)号：US20120271079A1

    公开(公告)日：2012-10-25

    申请号：US13516401

    申请日：2010-12-17

    Applicant: Teng Xu ,  Edward A. Lemon, JR. ,  Tan-Jen Chen ,  Terry E. Helton

    Inventor： Teng Xu ,  Edward A. Lemon, JR. ,  Tan-Jen Chen ,  Terry E. Helton

    IPC: C07C5/42 ,  C07C2/74

    CPC classification number: C07C5/31 ,  C07C2/74 ,  C07C5/367 ,  C07C2529/12 ,  C07C2529/14 ,  C07C2529/44 ,  C07C2529/46 ,  C07C2529/74 ,  C07C2529/76 ,  C07C2601/14 ,  C07C13/28 ,  C07C9/15 ,  C07C9/16 ,  C07C15/04

    Abstract: A processes for producing a dehydrogenation reaction product stream comprising the step of contacting a hydrocarbon stream comprising cyclohexane and methyl cyclopentane with a dehydrogenation catalyst comprising at least one metal or compound thereof and at least one molecular sieve and under conditions effective to convert at least a portion of the cyclohexane to benzene and to convert at least a portion of the methyl cyclopentane to at least one paraffin. The hydrocarbon stream is produced by hydroalkylating benzene and hydrogen to form a hydroalkylation reaction product stream which is separated to yield the hydrocarbon stream.

    Abstract translation: 一种用于生产脱氢反应产物流的方法，包括使包含环己烷和甲基环戊烷的烃物流与包含至少一种金属或其化合物的脱氢催化剂和至少一种分子筛接触的步骤，并且在有效地将至少一部分 的环己烷至苯并将至少一部分甲基环戊烷转化为至少一种石蜡。 烃流是通过加氢烷基化苯和氢来形成加氢烷基化反应产物流，其被分离以产生烃流。

    Dehydrogenation Process
    29.
    发明申请
    Dehydrogenation Process 审中-公开
    脱氢工艺

    公开(公告)号：US20120271078A1

    公开(公告)日：2012-10-25

    申请号：US13512805

    申请日：2010-12-17

    Applicant: Tan-Jen Chen ,  Terry E. Helton ,  Teng Xu

    Inventor： Tan-Jen Chen ,  Terry E. Helton ,  Teng Xu

    IPC: C07C5/42

    CPC classification number: C07C5/31 ,  C07C2/74 ,  C07C5/367 ,  C07C2521/04 ,  C07C2521/06 ,  C07C2521/08 ,  C07C2521/10 ,  C07C2521/12 ,  C07C2521/18 ,  C07C2523/58 ,  C07C2523/78 ,  C07C2529/74 ,  C07C2601/14 ,  Y02P20/52 ,  C07C13/28 ,  C07C9/15 ,  C07C9/16 ,  C07C15/04

    Abstract: In a dehydrogenation process a hydrocarbon stream comprising at least one non-aromatic six-membered ring compound and at least one five-membered ring compound is contacted with a dehydrogenation catalyst comprising: (i) a support; (ii) a first component comprising at least one metal component selected from Group 1 and Group 2 of the Periodic Table of Elements; and (iii) a second component comprising at least one metal component selected from Groups 6 to 10 of the Periodic Table of Elements, wherein the catalyst composition exhibits an oxygen chemisorption of greater than 50%. The contacting is conducted under conditions effective to convert at least a portion of the at least one non-aromatic six-membered ring compound in the hydrocarbon stream to benzene and to convert at least a portion of the at least one five-membered ring compound in the hydrocarbon stream to paraffins.

    Abstract translation: 在脱氢方法中，包含至少一种非芳族六元环化合物和至少一种五元环化合物的烃流与脱氢催化剂接触，所述脱氢催化剂包括：（i）载体; （ii）包含选自元素周期表第1族和第2族的至少一种金属成分的第一成分; 和（iii）包含选自元素周期表第6至10族的至少一种金属组分的第二组分，其中催化剂组合物显示出大于50％的氧化学吸附。 该接触在有效将烃流中的至少一种非芳香族六元环化合物的至少一部分转化为苯并将至少一部分至少一种五元环化合物转化为 烃流至石蜡。

    Process for producing cyclohexylbenzene
    30.
    发明授权
    Process for producing cyclohexylbenzene 有权
    生产环己基苯的方法

    公开(公告)号：US08084648B2

    公开(公告)日：2011-12-27

    申请号：US12747295

    申请日：2009-01-13

    Applicant: John S. Buchanan ,  Jane C. Cheng ,  Tan-Jen Chen ,  James R. Lattner

    Inventor： John S. Buchanan ,  Jane C. Cheng ,  Tan-Jen Chen ,  James R. Lattner

    IPC: C07C45/53 ,  C07C37/08 ,  C07C2/68

    CPC classification number: C07C409/14 ,  C07C13/28 ,  C07C37/08 ,  C07C45/53 ,  C07C407/00 ,  C07C2601/14 ,  C07C49/08 ,  C07C39/04

    Abstract: In a process for producing cyclohexylbenzene, hydrogen and a liquid feed comprising benzene are introduced into a reaction zone and are contacted in the reaction zone under hydroalkylation conditions to produce cyclohexylbenzene. An effluent stream comprising cyclohexylbenzene and unreacted benzene is removed from the reaction zone and is divided into at least first and second portions, wherein the mass ratio of the effluent stream first portion to the effluent stream second portion is at least 2:1. The effluent stream first portion is then cooled and the cooled effluent stream first portion is recycled to the reaction zone.

    Abstract translation: 在生产环己基苯的方法中，将氢和含苯的液体原料引入反应区，并在加氢烷基化条件下在反应区中接触以制备环己基苯。 将包含环己基苯和未反应苯的流出物流从反应区除去，并分成至少第一和第二部分，其中流出物流第一部分与流出物流第二部分的质量比至少为2:1。 然后将流出物流第一部分冷却，将冷却的流出物流第一部分再循环至反应区。

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