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    Composite polyamide membrane derived from aromatic monomer including anhydride and sulfonyl halide functional groups
    21.
    发明授权
    Composite polyamide membrane derived from aromatic monomer including anhydride and sulfonyl halide functional groups 有权
    衍生自芳族单体的复合聚酰胺膜包括酸酐和磺酰卤官能团

    公开(公告)号：US08999449B2

    公开(公告)日：2015-04-07

    申请号：US14197866

    申请日：2014-03-05

    Applicant: Dow Global Technologies LLC

    Inventor： Mou Paul ,  Tina L. Arrowood ,  Duane R. Romer

    IPC: B05D1/34 ,  B05D1/36 ,  B01D71/56 ,  B01D69/12 ,  B05D3/10

    CPC classification number: B01D71/56 ,  B01D69/125 ,  B05D1/34 ,  B05D1/36 ,  B05D3/107

    Abstract: A method for making a composite polyamide membrane including the step of applying a polyfunctional amine monomer and polyfunctional acyl halide monomer to a surface of the porous support and interfacially polymerizing the monomers to form a thin film polyamide layer, wherein the method is characterized by: i) conducting the interfacial polymerization in the presence of an aromatic anhydride monomer include at least one sulfonyl halide functional group, or ii) applying the aromatic anhydride monomer to the thin film polyamide layer.

    Abstract translation: 一种制备复合聚酰胺膜的方法，包括将多官能胺单体和多官能酰卤单体施用到多孔载体的表面并使单体界面聚合以形成薄膜聚酰胺层的步骤，其中该方法的特征在于：i ）在芳族酸酐单体的存在下进行界面聚合包括至少一种磺酰卤官能团，或ii）将芳族酸酐单体施加到薄膜聚酰胺层上。

    Bis(aryl)acetal compounds
    23.
    发明授权
    Bis(aryl)acetal compounds 有权
    双（芳基）缩醛化合物

    公开(公告)号：US08933239B1

    公开(公告)日：2015-01-13

    申请号：US13943232

    申请日：2013-07-16

    Applicant: Dow Global Technologies LLC

    Inventor： Matthias S. Ober ,  Duane R. Romer ,  John B. Etienne ,  Pulikkottil J. Thomas

    IPC: C07F5/05 ,  C07F5/04 ,  C07F5/02 ,  C07C43/225

    CPC classification number: C07F5/025 ,  C07C43/307 ,  C07F5/027 ,  C07F5/04 ,  C07F5/05

    Abstract: A bis(aryl)acetal has the formula wherein Y1 and Y2 are each independently chloro, bromo, iodo, mesylate, tosylate, triflate, or Bx, provided that Y1 and Y2 are not both selected from chloro, bromo, and iodo; each occurrence of Bx is independently a boron-containing functional group bonded to Ar1 or Ar2 via a boron atom; Ar1 and Ar2 are each independently unsubstituted or substituted C6-18 arylene, or unsubstituted or substituted C3-18 heteroarylene; provided that Ar1 and Ar2 are not covalently linked to each other to form a ring structure that includes —Ar1—O—C—O—Ar2—; and R1 and R2 are each independently hydrogen, unsubstituted or substituted C1-18 linear or branched alkyl, unsubstituted or substituted C3-20 cycloalkyl, unsubstituted or substituted C6-18 aryl, or unsubstituted or substituted C3-20 heteroaryl. The bis(aryl)acetal is useful as a monomer for oligoacetal and polyacetal synthesis via Suzuki polycondensation.

    Abstract translation: 双（芳基）缩醛具有下式：其中Y1和Y2各自独立地为氯，溴，碘，甲磺酸酯，甲苯磺酸酯，三氟甲磺酸酯或Bx，条件是Y1和Y2不都选自氯，溴和碘; 每次出现的Bx分别是通过硼原子与Ar 1或Ar 2键合的含硼官能团; Ar1和Ar2各自独立地为未取代的或取代的C6-18亚芳基，或未取代或取代的C3-18亚杂芳基; 条件是Ar 1和Ar 2不彼此共价连接以形成包括-Ar 1 -O-C-O-Ar 2 - 的环结构; 且R 1和R 2各自独立地为氢，未取代或取代的C 1-18直链或支链烷基，未取代或取代的C 3-20环烷基，未取代或取代的C 6-18芳基，或未取代或取代的C 3-20杂芳基。 双（芳基）缩醛可用作通过Suzuki缩聚的低缩醛和聚缩醛合成的单体。

    Non-cyclopentadienyl-based chromium catalysts for olefin polymerization
    28.
    发明授权
    Non-cyclopentadienyl-based chromium catalysts for olefin polymerization 有权
    用于烯烃聚合的非环戊二烯基铬催化剂

    公开(公告)号：US09422375B2

    公开(公告)日：2016-08-23

    申请号：US14931258

    申请日：2015-11-03

    Applicant: Dow Global Technologies LLC

    Inventor： Matthew D. Christianson ,  Timothy S. De Vries ,  Robert D J Froese ,  Matthias S. Ober ,  Jasson T. Patton ,  Duane R. Romer ,  Gordon R. Roof ,  Lixin Sun ,  Endre Szuromi ,  Curt N. Theriault ,  Dean M. Welsh ,  Timothy T. Wenzel ,  Paul H. Moran

    IPC: C07F11/00 ,  C08F4/78 ,  C08F10/00 ,  C08F210/06 ,  C08F110/06 ,  C08F110/02

    CPC classification number: C08F4/78 ,  C07F11/00 ,  C08F10/00 ,  C08F110/02 ,  C08F110/06 ,  C08F210/06 ,  C08F4/69112 ,  C08F210/16 ,  C08F2500/15

    Abstract: Provided is a non-cyclopentadienyl-based chromium-ligand complex, preferably a chromium-ligand complex of formula (J): LCr(RA)m(D)k (J), wherein L is a non-Cp monoanionic ligand; Cr (chromium) is in a formal oxidation state of +3 or +2; when Cr formally is Cr+3, either m is 1 and RA is hydrocarbylene (a hydrocarbylene chromium-ligand complex of formula (J)) or m is 2 and each RA independently is hydrocarbyl (a dihydrocarbyl chromium-ligand complex of formula (J)), wherein each hydrocarbyl or hydrocarbylene of RA independently is unsubstituted or substituted by from 1 to 5 RAS; each RAS independently is a neutral aprotic heteroalkyl, neutral aprotic heterocycloalkyl, neutral aprotic heteroaryl, or neutral aprotic aryl; when Cr formally is Cr+2, m is 1 and RA is hydrocarbyl (a hydrocarbyl chromium-ligand complex of formula (J)); k is an integer of 0 or 1; D is absent when k is 0 or D is a neutral ligand when k is 1; wherein the chromium-ligand complex of formula (J) is overall neutral and lacks a cyclopentadienyl-based (Cp-based) moiety. Also provided is a chromium catalyst comprising or prepared from the complex. Also provided is a process of making the catalyst and a process employing the chromium catalyst for polymerizing the olefin monomer, especially a straight chain 1-alkene, to prepare the polyolefin, especially a partially chain-straightened poly(1-alkene) or olefin block copolymer. Further provided is the partially chain-straightened poly(1-alkene) or olefin block copolymer prepared thereby. Also provided is a high throughput workflow.

    Abstract translation: 提供非环戊二烯基铬配体络合物，优选式（J）的铬配体络合物：LCr（RA）m（D）k（J），其中L是非Cp单阴离子配体; Cr（铬）处于+3或+2的正式氧化态; 当Cr正式为Cr + 3时，m为1，RA为亚烃基（式（J））的亚烃基铬 - 配体配合物）或m为2，各RA独立地为烃基（式（J）的二烃基铬 - 配体络合物 ）），其中RA的各个烃基或亚烃基独立地未被取代或被1至5个RAS取代; 每个RAS独立地是中性非质子杂烷基，中性非质子杂环烷基，中性非质子杂芳基或中性非质子性芳基; 当Cr正式为Cr + 2时，m为1，RA为烃基（式（J））的烃基铬 - 配体络合物）; k是0或1的整数; 当k为0时，D不存在，或当k为1时D为中性配体; 其中式（J）的铬配体络合物是总体中性的，并且缺少基于环戊二烯基的（Cp-基）部分。 还提供了包含或由络合物制备的铬催化剂。 还提供了制备催化剂的方法和使用铬催化剂聚合烯烃单体，特别是直链1-烯烃的方法，以制备聚烯烃，特别是部分链改性的聚（1-烯烃）或烯烃嵌段 共聚物。 进一步提供由其制备的部分链直链化的聚（1-烯烃）或烯烃嵌段共聚物。 还提供了高吞吐量的工作流程。

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