摘要:
A process for the preparation of tripeptides of the general formula IU-A-B-C-OH Iin which U denotes hydrogen or a urethane protective group and A, B and C denote amino acids, by reaction of a compound of the general formula IIU'-B-OH IIin which U' is a urethane protective group which can be eliminated by hydrogenolysis, with a compound of the general formula IIIH-C-OR IIIin which R denotes alkyl, by the PPA method, elimination of U', and reacting the resulting compound of the formula IVH-B-C-OR IVwith a compound of the formula VU-A-OH Vin the presence of propylphosphonic anhydride, and finally eliminating R enzymatically.
摘要:
The present invention relates to water-dispersible polyetherester-modified polyurethane ionomers containing 10 to 100 milliequivalents of ionic, preferably cationic, groups per 100 g of ionomer; 2 to 40% by weight of polyetherester groups; and 1 to 35% by weight of ethylene oxide units, in which the percentages are based on the weight of the polyetherester-modified polyurethane ionomer.The present invention also relates to a process for the preparation of these polyetherester-modified polyurethane ionomers and to aqueous compositions containing these polyetherester-modified polyurethane ionomers and polymers containing perfluoralkyl groups.
摘要:
The invention relates to linear and branched poly-p-arylene sulfides (PAS), preferably poly-p-phenylene sulfides (PPS), which have an extremely low proportion of defect or foreign structures, to a process for their production and to their use for the production of molded articles.
摘要:
The compressor cascade comprises a plurality of tandem-connected membrane pumps, each of the pumps having a plurality of stroke chambers whose volumes decrease in the direction of the fluid flow through the pumps. Each chamber has several parallel-connected input/output channels for interconnecting the individual membrane pumps and a check valve in each input/output channel for forcing the fluid in a specified direction. By electrostatic attraction forces, the membranes in the pumps are energized synchronously to resonance oscillations of the same frequency and deflection, building up the necessary operating pressure as the fluid is moved from the stroke chamber of one membrane pump into the smaller volume stroke chamber of the next succeeding membrane pump. The movement of the fluid through the membrane pumps of the compressor cascade leads to its compression, and the pressure at the end of the cascade is related to the reduction in volume of each succeeding stroke chamber.
摘要:
The invention relates to a process for the production of high molecular weight, optionally branched polyarylene sulfides having a low content of organically bound halogen. They are prepared by reaction of alkali sulfides and/or alkali hydrogen sulfides with aromatic dihalogen compounds in a polar organic solvent.
摘要:
In the conversion of trichloroethene and tetrachloroethene into dichloroacetyl chloride (DAC) or trichloroacetyl chloride (TAC) by means of oxygen, the reaction mixture is passed several times as a thin film through the reaction zone. The reaction time for achieving a certain conversion is in this way reduced.In the preparation of DAC, a constant content of acid chloride is established in the reaction mixture by removing some of the mixture and working this up by distillation, while the circulating reaction mixture is simultaneously topped up with fresh trichloroethene.In this way, side reactions are suppressed and the amount of by-products is reduced.
摘要:
A method for the catalytic epoxidation of olefins with hydrogen peroxide in the presence of rhenium-oxo-complexes or of a binuclear compound of the type .mu.-oxobis [porphyrinato-oxo-rhenium(V)] with octaethyl porphyrin or 5,10,15,20-tetraphenyl porphyrin or 5,10,15,20-tetra(4-pyridyl)-porphyrin as ligands.
摘要:
An arrangement for unloading and loading of x-ray sheet film cassettes of standardized but different sizes of their flat sides which also can be used for receiving different sheet film sorts and reloadable with respective sheet film sorts, comprises a light-tight closeable shaft for receiving a cassette, transporting unit for inserting and withdrawing of the cassettes, unit for positioning the cassette at a cassette corner which is the same for all cassettes, a mechanically-electronic comparison device for determining the format of a cassette, an opening device for the cassette, unit for withdrawing a film and inserting of a new film into the cassette, and unit for automatically distinguishing of cassette types with the same sizes or size regions and loadable with different film sorts and including at least one outwardly sensible marking provided on the cassettes of at least one type, at least one sensor arranged to sense the marking with a positioned cassette, and a comparison device which is connected for the sensor for automatic selection of a sheet film size or sort for further loading.
摘要:
A film supplying magazine which receives a pack of film sheets, covered with a light-tight sheathing and is insertable into a device which removes from said pack individual film sheets, comprises a box receiving a film pack, and a cover for closing the box. The sheathing has a winding flap while the magazine has an externally operated rotatable winding shaft to which the flap of the sheathing is connected so that the flap together with the sheathing is pulled off the pack and wound on the shaft when the latter is rotated. Velcro tapes are provided at the free end of the flap and at a portion of the winding shaft, which ensure an automatic connection between the flap and the shaft.
摘要:
This invention is directed to a system for reducing the yield loss from a metallurgical vessel, such as a ladle holding liquid metal having a slag layer thereon, by delaying the onset of slag entrapment in the metal stream during the tapping thereof. More particularly, such system includes a modification to the drain hole and/or bottom of such vessel.