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    Method of determining the filling level of a solid ammonia storage medium in an ammonia storage container
    21.
    发明授权
    Method of determining the filling level of a solid ammonia storage medium in an ammonia storage container 有权
    确定氨储存容器中固体氨储存介质的填充量的方法

    公开(公告)号：US08473226B2

    公开(公告)日：2013-06-25

    申请号：US12884527

    申请日：2010-09-17

    Applicant: Ulrich Joachim Quaade

    Inventor： Ulrich Joachim Quaade

    IPC: G06F23/00 ,  G06F23/14

    CPC classification number: H01M8/04208 ,  C01C1/006 ,  F01N3/2066 ,  F01N9/005 ,  F01N11/00 ,  F01N2550/05 ,  F01N2610/02 ,  F01N2610/06 ,  F01N2610/10 ,  F01N2900/1808 ,  F17C11/00 ,  Y02A50/2325

    Abstract: A method of determining an average degree of saturation with ammonia (X) of a solid ammonia storage medium porous or not and capable of ad- or absorbing and desorbing ammonia reversibly in a storage container is described. A part of the volume (Vcon) of the container is occupied by gaseous ammonia of a pressure (p) and defines a free volume (Vfree)). Ammonia flows out of the container with a flow (f). n pairs ((fi, pi), (Fi, pi)) of flows (fi), or accumulated flows (Fi), and pressures (pi) are sampled at a sequence of points of time (ti), i=1 . . . n and n≧2; an estimate volume value (Vfit) on the basis of the sampled pairs ((fi, pi), (Fi, pi)) is determined;and the degree of saturation with ammonia (X) is determined by applying a predetermined relationship (Rel) between a plurality of estimate volume values (Vfit) and a plurality of values of the average degree of saturation with ammonia (X) to the determined estimate volume value (Vfit).

    Abstract translation: 描述了一种使用多孔或不多孔的固体氨储存介质用氨（X）确定平均饱和度的方法，其能够在储存容器中可逆地吸附或吸收和解吸氨。 容器的一部分体积（Vcon）由压力（p）的气态氨占据并限定自由体积（Vfree））。 氨以流（f）流出容器。 流（fi）或累积流（Fi）的n对（（fi，pi），（Fi，pi））或累积流（Fi），并且压力（pi）在时间点（ti），i = 1的序列被采样。 的。 的。 n和n> = 2; 确定基于采样对（（fi，pi），（Fi，pi））的估计体积值（Vfit） 并且通过将多个估计体积值（Vfit）和具有氨（X）的平均饱和度的多个值之间的预定关系（Rel）应用于所确定的估计来确定与氨（X）的饱和度 体积值（Vfit）。

    Method of Determining the Filling Level of a Solid Ammonia Storage Medium in an Ammonia Storage Container
    22.
    发明申请
    Method of Determining the Filling Level of a Solid Ammonia Storage Medium in an Ammonia Storage Container 有权
    确定氨储存容器中固体氨储存介质填充量的方法

    公开(公告)号：US20120072135A1

    公开(公告)日：2012-03-22

    申请号：US12884527

    申请日：2010-09-17

    Applicant: Ulrich Joachim Quaade

    Inventor： Ulrich Joachim Quaade

    IPC: G01F23/14

    CPC classification number: H01M8/04208 ,  C01C1/006 ,  F01N3/2066 ,  F01N9/005 ,  F01N11/00 ,  F01N2550/05 ,  F01N2610/02 ,  F01N2610/06 ,  F01N2610/10 ,  F01N2900/1808 ,  F17C11/00 ,  Y02A50/2325

    Abstract: A method of determining an average degree of saturation with ammonia (X) of a solid ammonia storage medium porous or not and capable of ad- or absorbing and desorbing ammonia reversibly in a storage container is described. A part of the volume (Vcon) of the container is occupied by gaseous ammonia of a pressure (p) and defines a free volume (Vfree)). Ammonia flows out of the container with a flow (f). n pairs ((fi, pi), (Fi, pi)) of flows (fi), or accumulated flows (Fi), and pressures (pi) are sampled at a sequence of points of time (ti), i=1 . . . n and n≧2; an estimate volume value (Vfit) on the basis of the sampled pairs ((fi, pi), (Fi, pi)) is determined;and the degree of saturation with ammonia (X) is determined by applying a predetermined relationship (Rel) between a plurality of estimate volume values (Vfit) and a plurality of values of the average degree of saturation with ammonia (X) to the determined estimate volume value (Vfit).

    Abstract translation: 描述了一种使用多孔或不多孔的固体氨储存介质用氨（X）确定平均饱和度的方法，其能够在储存容器中可逆地吸附或吸收和解吸氨。 容器的一部分体积（Vcon）由压力（p）的气态氨占据并限定自由体积（Vfree））。 氨以流（f）流出容器。 流（fi）或累积流（Fi）的n对（（fi，pi），（Fi，pi））或累积流（Fi），并且压力（pi）在时间点（ti），i = 1的序列被采样。 。 。 n和n≥2; 确定基于采样对（（fi，pi），（Fi，pi））的估计体积值（Vfit） 并且通过将多个估计体积值（Vfit）和具有氨（X）的平均饱和度的多个值之间的预定关系（Rel）应用于所确定的估计来确定与氨（X）的饱和度 体积值（Vfit）。

    Method for Saturating and Re-Saturating Ammonia Storage Material in Containers
    23.
    发明申请
    Method for Saturating and Re-Saturating Ammonia Storage Material in Containers 有权
    容器中氨储存材料的饱和和再饱和方法

    公开(公告)号：US20110284121A1

    公开(公告)日：2011-11-24

    申请号：US12899667

    申请日：2010-10-07

    Applicant: Tue Johannessen ,  Ulrich Joachim Quaade ,  Johnny Johansen ,  Henrik Wagner-Pedersen

    Inventor： Tue Johannessen ,  Ulrich Joachim Quaade ,  Johnny Johansen ,  Henrik Wagner-Pedersen

    IPC: B65B31/00

    CPC classification number: B01D53/0454 ,  B01D53/0438 ,  B01D2257/406 ,  B01D2259/4525 ,  C01C1/006 ,  F17C11/00

    Abstract: A method for saturating or re-saturating ammonia storage material (1) capable of reversibly absorbing and desorbing ammonia in one or more storage containers (2), wherein said material is partly or fully depleted of ammonia, with ammonia to a predetermined saturation degree comprises a. placing the storage container(s) (2) in direct or indirect contact with a thermostatting medium (4) at a temperature level TT≦ about 65° C.; and b. connecting the storage container(s) (2) to a source of gaseous ammonia wherein at least during a part of the method the gaseous ammonia during saturating or re-saturation of the ammonia storage material (1) is at a pressure PS≦ about PT, wherein PS is the ammonia pressure during saturating or re-saturating of the ammonia storage material (1) and PT is the equilibrium vapor pressure of liquid ammonia at the temperature level TT.

    Abstract translation: 一种用于使氨储存材料（1）饱和或再饱和的方法，其能够在一个或多个储存容器（2）中可逆地吸收和解吸氨，其中所述材料部分或全部耗尽氨，氨与预定的饱和度包括 一个。 将储存容器（2）放置在温度等级TT＆amp; NlE下与恒温介质（4）直接或间接接触; 约65°C。 和b。 将所述储存容器（2）连接到气态氨源，其中至少在所述方法的一部分期间，所述氨储存材料（1）的饱和或再饱和期间的气态氨处于压力PS＆amp; 关于PT，其中PS是在氨储存材料（1）的饱和或再饱和期间的氨压力，PT是在温度水平TT下的液氨的平衡蒸气压。

    Use Of An Ammonia Storage Device In Production Of Energy
    27.
    发明申请
    Use Of An Ammonia Storage Device In Production Of Energy 审中-公开
    在能源生产中使用氨储存装置

    公开(公告)号：US20070207351A1

    公开(公告)日：2007-09-06

    申请号：US10593519

    申请日：2005-03-22

    Applicant: Claus Christensen ,  Tue Johannessen ,  Jens Norskov ,  Ulrich Quaade

    Inventor： Claus Christensen ,  Tue Johannessen ,  Jens Norskov ,  Ulrich Quaade

    IPC: H01M8/04

    CPC classification number: C01C1/006 ,  C01F5/00 ,  C01F5/26 ,  C01P2002/72 ,  H01M8/04216 ,  H01M8/0606 ,  H01M8/22

    Abstract: An electric power generating unit comprising (i) an ammonia storage device in the form of a container comprising an ammonia absorbing and releasing salt of the general formula: Ma(NH3)nXz, wherein M is one or more cations selected from alkali metals, alkaline earth metals, and transition metals such as Li, K, Mg, Ca, V, Cr, Mn, Fe, Co, Ni, Cu or Zn, X is one or more anions selected from fluoride, chloride, bromide, iodide, nitrate, thiocyanate, sulphate, molybdate, phosphate, and chlorate ions, a is the number of cations per salt molecule, Z is the number of anions per salt molecule, and n is the coordination number of 2 to 12. (ii) means for heating said container and ammonia absorbing and releasing salt for releasing ammonia gas and (iiia) a fuel cell for converting ammonia directly into electric power; or (iiib1) a reactor for dissociating ammonia into hydrogen and nitrogen and (iiib2) a fuel cell for converting hydrogen into electric power is useful for large stationary energy producing facilities, but also for use for is useful for large stationary energy producing facilities, but also for use for small rechargeable and/or replaceable power supply units for micro-fabricated or miniaturized ammonia decomposition reactors for use in mobile units and portable devices may be used for large energy producing facilities, and by use of small rechargeable and/or replaceable ammonia storage decomposition reactors, it is also possible to provide energy for mobile units and portable devices.

    Abstract translation: 一种发电单元，包括（i）包含氨吸收和释放盐的容器形式的氨储存装置，其具有以下通式：Ma（NH 3）n N 其中M是选自碱金属，碱土金属和过渡金属如Li，K，Mg，Ca，V，Cr，Mn，Fe，Co中的一种或多种阳离子， Ni，Cu或Zn，X是选自氟化物，氯化物，溴化物，碘化物，硝酸盐，硫氰酸盐，硫酸盐，钼酸盐，磷酸盐和氯酸根离子中的一种或多种阴离子，a是每个盐分子的阳离子数，Z是数 的阴离子，n是2〜12的配位数。（ii）加热所述容器和氨吸收和释放氨以释放氨气的装置和（iiia）用于将氨直接转化为电力的燃料电池的装置; 或（iiib1）用于将氨离解成氢和氮的反应器和（iib2）用于将氢转化为电力的燃料电池对于大型固定能量生产设备是有用的，但也用于大型固定能量生产设施，但是 也可用于用于移动单元和便携式设备的微型或微型氨分解反应堆的小型可再充电和/或可更换电源单元，可用于大型能源生产设备，并可使用小型可再充电和/或可更换氨 存储分解反应器，还可以为移动单元和便携式设备提供能量。

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