Method of flameproofing wood with inorganic ammonium salts and
dicyandiamide/formaldehyde reaction products
    41.
    发明授权
    Method of flameproofing wood with inorganic ammonium salts and dicyandiamide/formaldehyde reaction products 失效
    用无机铵盐和双氰胺/甲醛反应产物对木材进行隔热的方法

    公开(公告)号:US4301217A

    公开(公告)日:1981-11-17

    申请号:US85562

    申请日:1979-10-17

    摘要: A process for flameproofing wood is claimed, which comprises treating the wood with aqueous preparations which contain(a) at least one water-soluble ammonium salt of a non-volatile inorganic acid, e.g. ammonium sulfate or ammonium phosphate,(b) at least one water-soluble cationic reaction product of dicyandiamide, formaldehyde, optionally an ammonium salt and/or an alkylenepolyamine containing at most 18 carbon atoms, or the acid salt thereof.Components (a) and (b) are applied in succession or preferably simultaneously and the wood is subsequently dried. The flameproof finish obtained is resistant to rinsing. The wood provided with the flameproof finish is used in particular as mine timber.

    摘要翻译: 要求保护木材的防火方法,其包括用含有(a)至少一种非挥发性无机酸的水溶性铵盐的含水制剂处理木材,例如非挥发性无机酸。 硫酸铵或磷酸铵,(b)至少一种双氰胺,甲醛,任选的铵盐和/或含有至多18个碳原子的亚烷基多胺的水溶性阳离子反应产物或其酸式盐。 组分(a)和(b)连续地或优选同时施用,随后干燥木材。 获得的防火涂料耐冲洗。 提供防火漆的木材特别用作矿山木材。

    Method for the fireproofing of synthetic fiber material
    42.
    发明授权
    Method for the fireproofing of synthetic fiber material 失效
    合成纤维材料防火方法

    公开(公告)号:US4211814A

    公开(公告)日:1980-07-08

    申请号:US932082

    申请日:1978-08-08

    摘要: The invention provides a fireproofing composition which contains at least(a) a bromine compound of the formula ##STR1## wherein A.sub.1 and A.sub.2 are cycloalkyl,R is alkylene,m and n each are an integer from 2 to 7, andp is an integer from 1 to 5;(b) optionally a brominated cycloalkane;(c) a dispersing agent;(d) optionally a protective colloid; and(e) optionally water.This fireproofing composition is used for fireproofing synthetic fiber material.

    摘要翻译: 本发明提供了一种防火组合物,其至少包含(a)下式的溴化合物,其中A1和A2是环烷基,R是亚烷基,m和n各自是2至7的整数,p是整数 从1到5; (b)任选的溴化环烷烃; (c)分散剂; (d)任选的保护胶体; 和(e)任选的水。 该防火组合物用于防火合成纤维材料。

    Compositions of Fluorescent Whitening Agents
    46.
    发明申请
    Compositions of Fluorescent Whitening Agents 失效
    荧光增白剂的组成

    公开(公告)号:US20080073617A1

    公开(公告)日:2008-03-27

    申请号:US11665886

    申请日:2005-10-17

    IPC分类号: D21H21/30 D21H17/37 D21H17/53

    CPC分类号: D21H21/30 D21H17/37 D21H17/53

    摘要: The invention relates to a composition comprising a) at least one water-soluble fluorescent whitening agent, b) a polymer formed from an ethylenically unsaturated monomer or monomer blend, characterized in that at least one monomer is acrylamide and the water-soluble polymer has an average (weight average) molecular weight of between 500 and 49,000, optionally, c) polyethylene glycol with a weight average molecular weight of between 500 and 6000 and d) water and the use of the composition for the fluorescent whitening of paper in coating and size press or film press applications.

    摘要翻译: 本发明涉及包含a)至少一种水溶性荧光增白剂的组合物,b)由烯属不饱和单体或单体共混物形成的聚合物,其特征在于至少一种单体是丙烯酰胺,并且水溶性聚合物具有 平均(重均分子量)在500和49,000之间,任选地,c)重均分子量在500和6000之间的聚乙二醇和d)水,并且使用组合物用于涂布和尺寸的纸的荧光增白 印刷机或胶卷机应用。

    Amphoteric fluorescent whitening agents
    47.
    发明授权
    Amphoteric fluorescent whitening agents 失效
    两性荧光增白剂

    公开(公告)号:US07247174B2

    公开(公告)日:2007-07-24

    申请号:US10534315

    申请日:2003-11-11

    IPC分类号: C11D3/42

    CPC分类号: D21H21/30

    摘要: The present invention provides novel bis-triazinylaminostilbene amphoteric fluorescent whitening agents, comprising both individual components and mixtures thereof, a process for their preparation, intermediates useful for their prepartion and use of the fluorescent whitening agents for the fluorescents whitening of paper.

    摘要翻译: 本发明提供了新颖的双 - 三嗪基氨基芪两性荧光增白剂,其包括单独组分及其混合物,其制备方法,可用于其制备的中间体和使用荧光增白剂用于荧光增白纸。

    Composition for the fluorescent whitening of paper
    48.
    发明申请
    Composition for the fluorescent whitening of paper 审中-公开
    用于荧光增白的组合物

    公开(公告)号:US20060185805A1

    公开(公告)日:2006-08-24

    申请号:US10566742

    申请日:2004-07-28

    IPC分类号: D21H23/00

    CPC分类号: D21H21/30

    摘要: Composition for the fluorescent whitening of paper, which comprises a) a fluorescent whitening agent (FWA) derived from 4,4′-bis[(1,3,5-triazin-2-yl)amino]stilbene-2,2′-disulphonic acid and characterized by one or both of the triazine rings carrying an —NH2 substituent; b) water and c) optionally, further auxiliaries, the use thereof in either the pulp mass, in coating or in the metering size-press or film press and to a process thereto.

    摘要翻译: 用于纸的荧光增白的组合物,其包含a)衍生自4,4'-双[(1,3,5-三嗪-2-基)氨基]芪-2,2'-酮的荧光增白剂(FWA) 二磺酸,其特征在于一个或两个携带-NH 2 N取代基的三嗪环; b)水和c)任选地,其它辅助剂,其在纸浆质量,涂料中或在计量尺寸压力机或膜压机中的用途及其过程。

    Process for the preparation of stilbene compounds
    49.
    发明授权
    Process for the preparation of stilbene compounds 失效
    二苯乙烯化合物的制备方法

    公开(公告)号:US06365737B1

    公开(公告)日:2002-04-02

    申请号:US09622472

    申请日:2000-08-17

    IPC分类号: C07D25168

    摘要: A process for the preparation of a 4,4′-bis-(triazinylamino)-stilbene-2,2′-disulphonic acid compound of formula (1) is disclosed, characterized in that (a) in a first reaction step cyanurchloride is reacted with the disodium salt of 4,4′-diaminostilbene-2,2′-disulfonic acid to give the intermediate of formula (2); (b) in a second reaction step the compound of formula (2) is reacted with a compound of formula R1—H and/or R2—H to give the compound of formula (3); (c) in a third step the compound of formula (3) is reacted with the compound of the formula R3H, and reaction step (a) and/or (c) are carried out in a medium consisting of a mixture of water and a polyglycol to give the compound of formula (1), wherein R1, R2 and R3, independently, are phenylamino; phenylamino substitued by C1-C3alkyl, halogen, cyano, COOR or COR; CONH—R; SO2NH—R; NH—COR; mono- or disulphonated phenylamino; morpholino; piperidino; pyrrolidino; —NH2; —NH(C1-C4alkyl); —N(C1-C4alkyl)2; —NH(C2-C4hydroxyalkyl); —N(C2-C4hydroxyalkyl)2; —N(C1-C4alkyl)(C2-C4hydroxyalkyl); NHC2-C4 alkylsulphonic acid; —OC1-C4alkyl; an aminoacid or aminoacid amide residue from which a hydrogen atom on the amino group has been removed; R1 and R2 may further independently represent hydrogen; C1-C4alkyl; phenyl; naphthyl; phenyl or naphthyl substituted by C1-C4alkyl, C1-C4alkoxy, halogen, C2-C5alkanoyl-amino, nitro, sulpho or C1-C4alkylated amino; R is hydrogen; or C1-C3alkyl; and M is H, Na, Li, K, Ca, Mg, ammonium, or ammonium that is mono-, di-, tri- or tetrasubstituted by C1-C4alkyl, C2-C4hydroxyalkyl or a mixture thereof.

    摘要翻译: 公开了制备式(1)的4​​,4'-双 - (三嗪基氨基) - 茋-2,2'-二磺酸化合物的方法,其特征在于(a)在第一反应步骤中,氰化氢反应 与4,4'-二氨基芪-2,2'-二磺酸的二钠盐得到式(2)的中间体; (b)在第二反应步骤中,将式(2)化合物与式R 1 -H和/或R 2 -H的化合物反应,得到式(3)化合物; (c)在第三步中,式(3)化合物与式R3H的化合物反应,反应步骤(a)和/或(c)在由水和 得到式(1)化合物,其中R 1,R 2和R 3独立地是苯基氨基; 由C 1 -C 3烷基,卤素,氰基,COOR或COR取代的苯基氨基; CONH-R; SO2NH-R; NH-COR; 单或二磺基苯基氨基; 吗啉代 哌啶子 吡咯烷 -NH2; -NH(C 1 -C 4烷基); -N(C 1 -C 4烷基)2; -NH(C 2 -C 4羟烷基); -N(C 2 -C 4羟烷基)2; -N(C 1 -C 4烷基)(C 2 -C 4羟烷基); NHC2-C4烷基磺酸; -OC1-C4烷基; 已除去氨基上的氢原子的氨基酸或氨基酸酰胺残基; R 1和R 2可以进一步独立地表示氢; C 1 -C 4烷基; 苯基; 萘基; 被C 1 -C 4烷基,C 1 -C 4烷氧基,卤素,C 2 -C 5烷酰基 - 氨基,硝基,磺基或C 1 -C 4烷基化氨基取代的苯基或萘基; R是氢; 或C 1 -C 3烷基; 并且M是被C 1 -C 4烷基,C 2 -C 4羟烷基或其混合物单,二,三或四取代的H,Na,Li,K,Ca,Mg,铵或铵。

    Triazinylaminostilbene compounds
    50.
    发明授权
    Triazinylaminostilbene compounds 有权
    三嗪基氨基芪化合物

    公开(公告)号:US06331626B1

    公开(公告)日:2001-12-18

    申请号:US09666768

    申请日:2000-09-21

    IPC分类号: C07D25170

    摘要: The present invention provides a hydrate of the 4,4′-di-triazinylamino-2,2′-di-sulfostilbene compound having the formula: in which M and M1 independently represent hydrogen, an alkaline-, an alkaline earth metal or ammonium, x is a number within the range of from 1 to 30, and the crystal form of the hydrate (I) being characterised by an X-ray diffraction pattern which is essentially as set out in the accompanying FIGS. 1 to 11; or a mixture containing one or more of the hydrates of the 4,4′-di-triazinylamino-2,2′-di-sulfostilbene compound having the formula (I); processes for the preparation of the new hydrates; and the use of the new hydrates for the preparation of concentrated aqueous formulations of fluorescent whitening agents.

    摘要翻译: 本发明提供了具有下式的4,4'-二 - 三嗪基氨基-2,2'-二磺基芪化合物的水合物:其中M和M1独立地表示氢,碱金属,碱土金属或铵, x是1至30范围内的数字,并且水合物(I)的晶体形式的特征在于X射线衍射图,其基本上如附图中所示。 1至11; 或含有一种或多种具有式(I)的4,4'-二 - 三嗪基氨基-2,2'-二磺基芪化合物的水合物的混合物; 新水合物的制备过程; 以及使用新的水合物来制备荧光增白剂的浓缩水性制剂。