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    ACIDIC AQUEOUS COMPOSITION FOR ELECTROLYTICALLY DEPOSITING A COPPER DEPOSIT
    1.
    发明公开
    ACIDIC AQUEOUS COMPOSITION FOR ELECTROLYTICALLY DEPOSITING A COPPER DEPOSIT 审中-公开

    公开(公告)号：US20230142446A1

    公开(公告)日：2023-05-11

    申请号：US17920509

    申请日：2021-04-22

    申请人： Atotech Deutschland GmbH & Co. KG

    发明人： Ralf SCHMIDT ,  Josef GAIDA ,  Willi ROHLAND ,  Jens PALM ,  Himendra JHA

    IPC分类号： C25D3/38 ,  C07D233/60 ,  C07D249/04 ,  C07D251/54

    CPC分类号： C25D3/38 ,  C07D233/60 ,  C07D249/04 ,  C07D251/54

    摘要： The invention relates to an acidic aqueous composition for electrolytic copper plating, the composition comprising

    (i) copper (II) ions,
    (ii) one or more than one suppressor consisting of or comprising

    one single N-heteroaromatic mono-ring, said mono-ring comprising at least two ring nitrogen atoms and more than one substituent covalently connected to one of said ring nitrogen atoms and/or a ring carbon atom, wherein said substituent independently is or comprises
    one or more than one linear or branched polyalkylene glycol moiety,
    and/or
    one or more than one linear or branched polyalkylene glycol block polyalkylene glycol, or random polyalkylene glycol moiety,
    with the proviso that
    if said suppressor comprises a OH group, then it is a terminal OH group of said polyalkylene glycol moiety, polyalkylene glycol block polyalkylene glycol, and random polyalkylene glycol moiety, respectively, and
    said suppressor does not comprise NH2 groups, halogen atoms, and sulfur atoms;

    a method of electrolytic copper plating using the acidic aqueous composition; and specific suppressors as defined above.

    Concentrated storage-stable aqueous optical brightening solutions
    3.
    发明授权
    Concentrated storage-stable aqueous optical brightening solutions 有权

    公开(公告)号：US09951031B2

    公开(公告)日：2018-04-24

    申请号：US13513369

    申请日：2010-12-01

    申请人： Cedric Klein ,  Frederic Reveaud ,  David Puddiphatt ,  Andrew Clive Jackson

    发明人： Cedric Klein ,  Frederic Reveaud ,  David Puddiphatt ,  Andrew Clive Jackson

    IPC分类号： C07D251/54 ,  D21H21/30

    CPC分类号： C07D251/54 ,  D21H21/30 ,  Y10T428/249921 ,  Y10T442/2582 ,  Y10T442/60

    摘要： Concentrated storage stable aqueous solutions (S) comprising components (a), (b) and (c), wherein component (a) is at least one optical brightening agent of formula (1), in which the anionic charge on the brightener is balanced by a cationic charge composed of one or more cations selected from the group consisting of hydrogen, alkali metal cation, alkaline earth metal cation, ammonium, ammonium which is mono-, di- or trisubstituted by a C1-4 linear or branched alkyl radical and ammonium which is mono-, di- or trisubstituted by a C1-4 linear or branched hydroxyalkyl radical, and the concentration of component (a) is 0.08 to 0.3 mol per kg, based on the total weight of the concentrated storage-stable aqueous solutions (S), component (b) is at least one inorganic salt (SA), in a concentration of 2 to 15% by weight, based on the total weight of the concentrated storage-stable aqueous solutions (S), and component (c) is water, in a concentration of 10% to 88% by weight, based on the total weight of the concentrated storage-stable aqueous solutions (S).

    Preparation Process of a Flame Retardant Composition Made from Brominated Bismuth and/or Antimony Compounds Complexed with Melamine and Composition Obtained Thereby
    7.
    发明申请
    Preparation Process of a Flame Retardant Composition Made from Brominated Bismuth and/or Antimony Compounds Complexed with Melamine and Composition Obtained Thereby 有权

    公开(公告)号：US20170292076A1

    公开(公告)日：2017-10-12

    申请号：US15517355

    申请日：2015-07-28

    申请人： Sichim Alfa S.r.l.

    发明人： Anita Castellucci ,  Alessandro Bottoni

    IPC分类号： C09K21/10 ,  C07D251/70 ,  C08K5/3492

    CPC分类号： C09K21/10 ,  C07D251/54 ,  C07D251/70 ,  C07F9/902 ,  C07F9/94 ,  C08K3/04 ,  C08K3/36 ,  C08K5/34922 ,  C08K5/34928

    摘要： The invention relates to a preparation process of a flame retardant composition made from brominated bismuth and/or antimony compounds complexed with melamine, in which melamine, at least one between the bismuth carbonate and antimony sesquioxide, hydrobromic acid in aqueous solution are placed in contact with each other so as to trigger chemical reactions which lead to the formation of a complex of brominated bismuth or brominated antimony with melamine and melamine bromohydrate. The reagents are placed in contact in the presence of at least one reaction carrier defined by at least one compound chosen from the group consisting of melamine, melamine phosphate, melamine polyphosphate, ammonium phosphate, ammonium polyphosphate, triphenyl-phosphate, graphite, silica, lignin, coke and compounds containing triazine rings condensed or linked by —NH groups. The reaction carrier is not involved in the reactions. There are no polymeric compounds in quantities such as to create a polymer matrix. The reagents being introduced into the reactor in an amount defined by the stoichiometric ratios of said reactions. The reaction carrier is introduced into the reactor in an amount defined with respect to the total weight of the reagents so that it can perform a modulator function.

    Process for producing pyrophosphate
    9.
    发明授权
    Process for producing pyrophosphate 有权
    焦磷酸盐生产工艺

    公开(公告)号：US09493353B2

    公开(公告)日：2016-11-15

    申请号：US14652797

    申请日：2014-02-14

    申请人： ADEKA CORPORATION

    发明人： Genta Harada ,  Yutaka Yonezawa ,  Michio Nakamura ,  Yuri Okamoto ,  Kohei Omori

    IPC分类号： C07D251/14 ,  C07D251/42 ,  C07D251/48 ,  C07D251/54 ,  C07F9/6521 ,  C01B25/42 ,  C07D295/02 ,  C07F9/6509

    CPC分类号： C01B25/42 ,  C07D251/54 ,  C07D295/02 ,  C07F9/6509

    摘要： A process for producing a pyrophosphate, particularly melamine pyrophosphate useful as a flame retardant, efficiently in high yield is provided. The process includes firing an orthophosphate, preferably melamine orthophosphate, in the presence of a silicone oil, preferably methylphenyl silicone oil preferably at 120° to 350° C. Examples of useful firing equipment include a hot air dryer, a kneader, a Henschel mixture, a fluidized bed dryer, a rotary kiln, a paddle dryer, an extruder, a vibrating dryer, a far-infrared conveyor furnace, and a microwave firing furnace.

    摘要翻译： 提供了以高产率有效地生产焦磷酸盐，特别是可用作阻燃剂的焦磷酸三聚氰胺的方法。 该方法包括在硅油，优选甲基苯基硅油存在下，优选在120-350℃下焙烧正磷酸盐，优选正磷酸三聚氰胺。有用的焙烧设备的实例包括热空气干燥器，捏合机，亨舍尔混合物， 流化床干燥机，回转窑，桨式干燥机，挤出机，振动干燥机，远红外传送炉和微波烧制炉。