Pressure measurement in microwave-assisted chemical synthesis
    42.
    发明申请
    Pressure measurement in microwave-assisted chemical synthesis 失效
    微波辅助化学合成中的压力测量

    公开(公告)号:US20030170149A1

    公开(公告)日:2003-09-11

    申请号:US09773898

    申请日:2001-01-31

    IPC分类号: B01J019/00

    摘要: A pressure-measuring vessel system for microwave assisted chemical processes is disclosed. The vessel system includes a pressure resistant vessel that is otherwise transparent to microwave radiation, a pressure-resistant closure for the mouth of the vessel, with portions of the closure including a pressure resistant synthetic membrane, a pressure transducer external to the vessel, and a tube extending from the transducer, through the membrane and into the vessel for permitting the pressure inside the vessel to be applied against the transducer while the closure and membrane otherwise maintain the pressure resistant characteristics of the vessel.

    摘要翻译: 公开了一种用于微波辅助化学工艺的压力测量容器系统。 容器系统包括对微波辐射透明的耐压容器,用于容器口部的耐压封闭件,封闭件的一部分包括耐压合成膜,容器外部的压力传感器和 管从换能器延伸通过膜并进入容器,以允许容器内的压力施加在换能器上,同时封闭件和膜另外保持容器的耐压特性。

    Microwave heating apparatus
    44.
    发明申请
    Microwave heating apparatus 有权
    微波加热装置

    公开(公告)号:US20020027135A1

    公开(公告)日:2002-03-07

    申请号:US09791789

    申请日:2001-02-26

    IPC分类号: H05B006/70 H01P003/12

    摘要: The present invention relates to an apparatus for heating a sample, such as chemical reaction mixtures, whose dielectric properties varies during the heating process. In particular, the present invention relates to a microwave heating apparatus comprising a microwave generator, a waveguide for guiding the generated microwaves to an applicator, and a deflector formed by a closed loop defining a plane, said deflector having an inherent resonance frequency and a thickness in a direction normal to said plane, the deflector being rotatable around an axis being at least substantially parallel to said plane, the deflector being positioned in the waveguide so as to form a resonant cavity with the sample and the waveguide applicator. The resonance conditions of the resonant cavity and the coupling factor of radiation from the waveguide to the cavity are easily adjustable by rotation of the deflector. The resonance conditions and the coupling factor can be adjusted in response to the dielectric properties of the sample in order to optimise the amount of absorbed power and thereby obtain control of the sample heating process.

    摘要翻译: 本发明涉及一种用于加热在加热过程中其介电特性变化的样品例如化学反应混合物的装置。 特别地,本发明涉及一种微波加热装置,其特征在于,包括微波发生器,用于将所产生的微波引导到施加器的波导和由限定平面的闭环形成的偏转器,所述偏转器具有固有的共振频率和厚度 在垂直于所述平面的方向上,所述偏转器可围绕至少基本上平行于所述平面的轴线旋转,所述偏转器定位在所述波导中,以便与所述样品和所述波导施加器形成谐振腔。 谐振腔的谐振条件和波导到腔的辐射的耦合因子可以通过偏转器的旋转而容易地调节。 可以响应于样品的介电性质来调节共振条件和耦合因子,以优化吸收功率的量,从而获得样品加热过程的控制。