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    Poly aluminum hydroxy complexes and process for their production
    62.
    发明授权
    Poly aluminum hydroxy complexes and process for their production 失效
    多羟基铝复合物及其生产方法

    公开(公告)号：US3655329A

    公开(公告)日：1972-04-11

    申请号：US3655329D

    申请日：1968-01-02

    申请人： WARNER LAMBERT CO

    发明人： SHIH I-KAO ,  BLASER ERIC

    IPC分类号： C01F7/34 ,  C01F1/00

    CPC分类号： C01F7/34

    摘要： WHICH ARE PREPARED BY NEUTRALIZING POLY ALUMINUM HYDROXIDE WITH A WATER SOLUBLE ACID HAVING A PKa of less than 5, for example, hydrochloric acid, hydrobromic acid, nitric acid, lactic acid, acetic acid, to obtain poly aluminum hydroxy complex of the formula: PAH-X, in which PAH is poly aluminum hydroxy and X is the anion; the PAH-X thus formed can be treated further with aqueous solution of water soluble salts to make other derivatives. These poly aluminum hydroxy PAH-X) complexes are useful as deodorant, anti-perspirant and astringent agents.

    A new class of poly aluminum hydroxy complexes of the formula:

    摘要翻译： 一类新型的聚铝羟基配合物，分子式如下：

    1 2 3 4 4a 5 6 6a-octahydrobenzofuro (3 2-c)indoles
    63.
    发明授权
    1 2 3 4 4a 5 6 6a-octahydrobenzofuro (3 2-c)indoles 失效
    1 2 3 4 4A 5 6 6A-OCTAHYDROBENZOFURO（3 2-C）吲哚

    公开(公告)号：US3649644A

    公开(公告)日：1972-03-14

    申请号：US3649644D

    申请日：1969-08-08

    申请人： WARNER LAMBERT CO

    发明人： SONNTAG ARCH CHRISTIAN ,  KLUTCHKO SYLVESTER ,  SHAVEL JOHN JR

    IPC分类号： C07D209/12 ,  C07D311/82 ,  C07D491/10 ,  C07D27/04

    CPC分类号： C07D491/10 ,  C07D209/12 ,  C07D311/82

    摘要： THE PRESENT INVENTION DISCLOSES A TETRACYCLIC HYDROGENATED BENZOFURO(3,2.C)INDOLE HAVING THE FORMULA:

    2-R4,3,3A-(-CH2-(CH2)N-X-)(-R3),R1,R2-1,2,3,8A-TETRA

    HYDRO-3AH-BENZOFURO(2,3-C)PYRROLE OR THE 1,8A-DIHYDRO

    COMPOUND OR THE 3,3A-(=CH-(CH2)N-X-)(-R3) COMPOUND

    WHEREIN N IS FROM 2 TO 4, INCLUSIVE; X IS SULFUR, OXYGEN, CH2, OR N-R5, WHEREIN R5 IS HYDROGEN, ALKYL, ARYL OR ARALKYL; R1 IS HYDROGEN, HYDROXY, ACYLOXY, ALKOXY, ALKYL OR HALOGEN; R2 IS HYDROGEN, HYDROXY, ACYOXY, ALKOXY, ALKYL OR HALOGEN; R1 AND R2 TAKEN TOGETHER ARE METHYLENEDIOXY; R3 IS ALKYL, ARYL OR ARALKYL; AND R4 IS HYDROGEN, LOWER ALKYL, SUBSTITUTED ALKYL OR ARALKYL, ACYL, ALKENYL, GUANYL, CH3$I$ OR (CH3)2$I$ (WHEN NO DOUBLE BOND IS PRESENT) AND WHICH MAY OR MAY NOT CONTAIN A DOUBLE BOND BETWEEN THE POSITION INDICATED. THESE COMPOUNDS ARE USEFUL AS CENTRAL NERVOUS SYSTEM STIMULANTS.

    N-phthalimidoacetyl-5-chloro-2-cyclopropyl-methylaminobenzhydrol
    64.
    发明授权
    N-phthalimidoacetyl-5-chloro-2-cyclopropyl-methylaminobenzhydrol 失效
    N-邻苯二甲酰基-5-氯代-2-环丙基 - 甲基氨基苯甲醛

    公开(公告)号：US3649643A

    公开(公告)日：1972-03-14

    申请号：US3649643D

    申请日：1969-03-10

    申请人： WARNER LAMBERT CO

    发明人： NOVACK ROBERT M

    IPC分类号： C07D209/48 ,  C07D27/52

    CPC分类号： C07D209/48

    摘要： THERE IS DESCRIBED N-PHTHALIMIDOACETYL - 5 - CHLORO-2CYCLOPROPYLMETHYLAMINOBENZHYDROL; A PROCESS FOR PRODUCING SAID COMPOUND; AND A METHOD FOR CONVERTING SAME INTO N-PHTHALIMIDOACETYL - 5 - CHLORO - 2 - CYCLOPROPYLMETHYLAMINOBENZOPHENONE. THE BENZHYDROL COMPOUND OF THIS INVENTION IS PREPARED BY REACTING 5-CHLORO-2-CYCLOPROPYLMETHYLAMINOBENZHYDROL WITH PHTHLIMIDOACETYL CHLORIDE IN THE PRESENCE OF AN ALKALI AT A TEMPERATURE BELOW NORMAL ROOM TEMPERATURES. IT IS CONVERTED TO THE AFOREMENTIONED KNOWN BENZOPHENONE BY REACTION WITH AN AQUEOUS ACETIC ACID SOLUTION OF CHROMIUM TRIOXIDE. N-PHTHALIMIDOACETYL - 5 - CHLORO - 2 - CYCPROPYLMETHYLAMINOBENZHYDROL IS USEFUL AND IT IS USED, AS THE PENULIMATE INTERMEDIATE IN A PROCESS FOR THE PREPARATION OF-CYCLOPROPYLMETHYL-5-PHENYL-M-CHLORO-1H-1,4BENZODIAZEPINE-2(3H)-ONE. THE NOVEL BENZHYDROL COMPOUND IS CONVERTEF INTO THE CORRESPONDING BENZOPHENONE AND THE LATTER, IN TURN IS CONVERTED INTO THE BENZODIAZEPINE COMPOUND. THE AFOREMENTIONED BENZODIAZEPINE COMPOUND IS A KNOWN TRANQUILIZER, EXHIBITING ANTI-ANXIETY AND SEDATIVE ACTIVITY WITHOUT UNDESIRABLE SIDE EFFECTS SUCH AS HYPNOSIS.