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公开(公告)号：US5296417A
公开(公告)日：1994-03-22
申请号：US4889
申请日：1993-01-19
申请人： Terry D. Claar , Steven M. Mason , Kevin P. Pochopien , Danny R. White , William B. Johnson , Michael K. Aghajanian
发明人： Terry D. Claar , Steven M. Mason , Kevin P. Pochopien , Danny R. White , William B. Johnson , Michael K. Aghajanian
CPC分类号： C04B35/56 , C04B35/5607 , C04B35/5611 , C04B35/5622 , C04B35/5805 , C04B35/58064 , C04B35/58071 , C04B35/58078 , C04B35/652 , C04B35/653 , C04B41/5062 , C04B41/507 , C04B41/87 , C22C29/00 , Y10T428/12007
摘要： Self-supporting bodies are produced by reactive infiltration of a parent metal into a boron carbide material which may contain one or both of a boron donor material and a carbon donor material. The reactive infiltration typically results in a composite comprising a boron-containing compound, a carbon-containing compound and residual metal, if desired. The mass to be infiltrated may contain one or more inert fillers admixed with the boron carbide material, boron-containing compound and/or carbon-containing compound. The relative amounts of reactants and process conditions may be altered or controlled to yield a body containing varying volume percents of ceramic, metal, ratios of one ceramic to another and porosity.
摘要翻译： 自支撑体通过母体金属的反应性渗透到可以含有硼给体材料和碳供体材料中的一种或两种的碳化硼材料中而产生。 如果需要，反应性渗透通常导致包含含硼化合物，含碳化合物和残余金属的复合材料。 待渗透的物质可以含有与碳化硼材料，含硼化合物和/或含碳化合物混合的一种或多种惰性填料。 可以改变或控制反应物和工艺条件的相对量，以产生包含不同体积百分比的陶瓷，金属，一种陶瓷与另一陶瓷的比例和孔隙率的物体。
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公开(公告)号：US5165463A
公开(公告)日：1992-11-24
申请号：US520927
申请日：1990-05-09
CPC分类号： C04B41/88 , C04B41/5155 , C22C1/1036 , B22F2003/1014 , C22C2001/1063
摘要： A metal matrix composite is formed by contacting a molten matrix alloy with a permeable mass of filler material or preform in the presence of an infiltrating atmosphere. Under these conditions, the molten matrix alloy will spontaneously infiltrate the permeable mass of filler material or preform under normal atmospheric pressures. Once a desired amount of spontaneous infiltration has been achieved, or during the spontaneous infiltration step, the matrix metal which has infiltrated the permeable mass of filler material or preform is directionally solidified. The directionally solidified metal matrix composite may be heated to a temperature in excess of the liquidus temperature of the matrix metal and quenched. This technique allows the production of spontaneously infiltrated metal matrix composites having improved microstructures and properties.
摘要翻译： 金属基质复合材料是通过使熔融基质合金与渗透气体的渗透性物质或预型体接触而形成的。 在这些条件下，熔融基质合金会在正常大气压下自发渗入填料或预型体的渗透物质。 一旦实现了所需量的自发渗透，或者在自发渗透步骤期间，渗透了填充材料或预型体的可渗透物质的基质金属被定向凝固。 可以将定向凝固的金属基质复合材料加热到超过基质金属的液相线温度并淬火。 该技术允许生产具有改进的微结构和性质的自发渗透的金属基质复合材料。
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公开(公告)号：US5084425A
公开(公告)日：1992-01-28
申请号：US667916
申请日：1991-03-11
申请人： Robert C. Kantner , Michael K. Aghajanian , Stanislav Antolin , Alan S. Nagelberg , Ratnesh K. Dwivedi
发明人： Robert C. Kantner , Michael K. Aghajanian , Stanislav Antolin , Alan S. Nagelberg , Ratnesh K. Dwivedi
CPC分类号： C04B35/652 , C22C29/12
摘要： This invention relates to a self-supporting ceramic strucutre comprising an oxidation reaction product of a parent metal and a vapor-phase oxidant characterized by an altered microstructure attributable to the addition of one or more process modifiers relative to substantially the same oxidation reaction product produced without a process modifier.
摘要翻译： 本发明涉及一种自支撑陶瓷结构，其包括母体金属和气相氧化剂的氧化反应产物，其特征在于相对于基本上相同的氧化反应产物而添加一种或多种工艺改性剂的改变的微结构， 一个过程修饰符。
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64.发明授权Method of forming metal matrix composite bodies by utilizing a crushed polycrystalline oxidation reaction product as a filler, and products produced thereby 失效通过利用破碎的多晶氧化反应产物作为填料形成金属基质复合体的方法，以及由此产生的产物
公开(公告)号：US5007476A
公开(公告)日：1991-04-16
申请号：US269306
申请日：1988-11-10
CPC分类号： C22C1/1036 , C22C2001/1057 , C22C2001/1063 , Y10T428/12007 , Y10T428/12486
摘要： The present invention relates to a novel method for forming metal matrix composite bodies and novel metal matrix composite bodies produced thereby. Particularly, a polycrystalline oxidation reaction product of a parent metal and an oxidant is first formed. The polycrystalline oxidation reaction product is thereafter comminuted into an appropriately sized filler material which can be placed into a suitable container or formed into a preform. The filler material or preform of comminuted polycrystalline oxidation reaction product is thereafter placed into contact with a matrix metal alloy in the presence of an infiltration enhancer, and/or an infiltration enhancer precursor and/or an infiltrating atmosphere, at least at some point during the process, whereupon the matrix metal alloy spontaneously infiltrates the filler material or preform. As a result of utilizing comminuted or crushed polycrystalline oxidation reaction product, enhanced infiltration (e.g., enhanced rate or amount) is achieved. Moreover, novel metal matrix composite bodies are produced.
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公开(公告)号：US4828008A
公开(公告)日：1989-05-09
申请号：US49171
申请日：1987-05-13
IPC分类号： C22C47/10 , C04B35/58 , C22C1/10 , C22C21/00 , C22C29/00 , C22C29/02 , C22C29/12 , C22C29/14 , C22C29/16 , C22C32/00 , C22C47/00 , C22C47/02 , C22C47/04 , C22C47/08 , C22C49/06 , C22C49/14 , C22C101/10
CPC分类号： C22C29/00 , C22C1/1036 , C22C32/00 , C22C47/08 , C22C49/14 , B22F2998/00 , B22F2999/00 , C22C2001/1063 , Y10T428/12007 , Y10T428/12486
摘要： A ceramic-reinforced aluminum matrix composite is formed by contacting a molten aluminum-magnesium alloy with a permeable mass of ceramic material in the presence of a gas comprising from about 10 to 100% nitrogen, by volume, balance non-oxidizing gas, e.g., hydrogen or argon. Under these conditions, the molten alloy spontaneously infiltrates the ceramic mass under normal atmospheric pressures. A solid body of the alloy can be placed adjacent a permeable bedding of ceramic material, and brought to the molten state, preferably to at least about 700.degree. C., in order to form the aluminum matrix composite by infiltration. In addition to magnesium, auxiliary alloying elements may be employed with aluminum. The resulting composite products may contain a discontinuous aluminum nitride phase in the aluminum matrix and/or an aluminum nitride external surface layer.
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公开(公告)号：US4777014A
公开(公告)日：1988-10-11
申请号：US837448
申请日：1986-03-07
IPC分类号： B22D19/00 , B29C43/10 , C04B35/58 , C04B35/622 , C04B35/65 , C22C1/05 , C22C1/10 , C22C29/14 , B22F1/00
CPC分类号： B29C43/10 , C04B35/5156 , C04B35/58 , C04B35/5805 , C04B35/58064 , C04B35/58071 , C04B35/58078 , C04B35/6365 , C04B35/652 , C04B35/653 , C22C1/1036 , C22C29/14 , C22C2001/1057
摘要： Self-supporting bodies are produced by reactive infiltration of a parent metal with a boron source typically resulting in a composite comprising a parent metal boride and metal. The mass to be infiltrated may contain one or more inert fillers admixed with the boron source to produce a composite by reactive infiltration, which composite comprises a matrix of metal and parent metal boride embedding the filler. The relative amounts of reactants and process conditions may be altered or controlled to yield a body containing varying volume percents of ceramic, metal and/or porosity.
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67.发明授权公开(公告)号：US08741212B2
公开(公告)日：2014-06-03
申请号：US13420449
申请日：2012-03-14
IPC分类号： C04B35/563 , C04B35/565 , C04B35/581 , C04B35/584
CPC分类号： C04B35/565 , C04B35/573 , C04B2235/3826 , C04B2235/3891 , C04B2235/404 , C04B2235/428 , C04B2235/5436 , C04B2235/5472 , C04B2235/6562 , C04B2235/6565 , C04B2235/77 , C04B2235/80 , C04B2235/96 , C04B2235/9607 , C22C29/06
摘要： Composite bodies made by a silicon metal infiltration process that feature a silicon intermetallic, e.g., a metal silicide. Not only does this give the composite material engineer greater flexibility in designing or tailoring the physical properties of the resulting composite material, but the infiltrant also can be engineered compositionally to have much diminished amounts of expansion upon solidification, thereby enhancing net-shape-making capabilities. These and other consequences of engineering the metal component of composite bodies made by silicon infiltration permit the fabrication of large structures of complex shape.
摘要翻译： 通过硅金属渗透方法制成的复合体，其特征在于硅金属间化合物，例如金属硅化物。 这不仅使得复合材料工程师在设计或定制所得复合材料的物理性能方面具有更大的灵活性，而且浸润剂也可以组合工程化以在固化时具有大大减少的膨胀量，从而增强网状制造能力 。 通过硅渗透制造的复合材料的金属组分的这些和其他后果允许制造复杂形状的大结构。
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68.发明授权Diamond-reinforced composite materials and articles, and methods for making same 有权金刚石增强复合材料和制品及其制造方法公开(公告)号：US08474362B1
公开(公告)日：2013-07-02
申请号：US12313372
申请日：2008-11-19
申请人： Prashant G. Karandikar , Sam Salamone , Allyn L. McCormick , Michael K. Aghajanian , Glen Evans
发明人： Prashant G. Karandikar , Sam Salamone , Allyn L. McCormick , Michael K. Aghajanian , Glen Evans
IPC分类号： F41H5/04
CPC分类号： F41H5/0435 , C04B35/563 , C04B35/565 , C04B35/573 , C04B2235/3821 , C04B2235/427 , C04B2235/428 , C04B2235/48 , C04B2235/616 , C04B2235/6562 , C04B2235/6565 , C04B2235/6581 , C04B2235/77 , C04B2235/80 , F41H5/0492
摘要： A diamond-reinforced SiC ceramic composite material and shaped article. The addition of diamond to the microstructure greatly enhances properties such as hardness and Young's modulus. Such a composite material has considerable promise as an armor material. In particular, significant increases in ballistic performance can be achieved versus a non-diamond-containing composite, particularly versus the M993 threat. Reaction bonded silicon carbide (RBSC) ceramics with 7% diamond were shown to offer ballistic performance levels that matched the best commercial ceramics tested on the program.
摘要翻译： 金刚石增强SiC陶瓷复合材料和成型制品。 将金刚石添加到微观结构中大大增强了诸如硬度和杨氏模量的性能。 这种复合材料作为装甲材料具有相当大的希望。 特别是与非金刚石复合材料相比，可以显着提高弹道性能，特别是与M993威胁相比。 具有7％金刚石的反应结合碳化硅（RBSC）陶瓷被证明具有与在程序上测试的最佳商业陶瓷相匹配的弹道性能水平。
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公开(公告)号：US20120277087A1
公开(公告)日：2012-11-01
申请号：US13420449
申请日：2012-03-14
IPC分类号： C04B35/515 , C04B35/80 , B05D3/00 , C04B35/58
CPC分类号： C04B35/565 , C04B35/573 , C04B2235/3826 , C04B2235/3891 , C04B2235/404 , C04B2235/428 , C04B2235/5436 , C04B2235/5472 , C04B2235/6562 , C04B2235/6565 , C04B2235/77 , C04B2235/80 , C04B2235/96 , C04B2235/9607 , C22C29/06
摘要： Composite bodies made by a silicon metal infiltration process that feature a silicon intermetallic, e.g., a metal silicide. Not only does this give the composite material engineer greater flexibility in designing or tailoring the physical properties of the resulting composite material, but the infiltrant also can be engineered compositionally to have much diminished amounts of expansion upon solidification, thereby enhancing net-shape-making capabilities. These and other consequences of engineering the metal component of composite bodies made by silicon infiltration permit the fabrication of large structures of complex shape.
摘要翻译： 通过硅金属渗透方法制成的复合体，其特征在于硅金属间化合物，例如金属硅化物。 这不仅使得复合材料工程师在设计或定制所得复合材料的物理性能方面具有更大的灵活性，而且浸润剂也可以组合工程化以在固化时具有大大减少的膨胀量，从而增强网状制造能力 。 通过硅渗透制造的复合材料的金属组分的这些和其他后果允许制造复杂形状的大结构。
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公开(公告)号：US07332221B2
公开(公告)日：2008-02-19
申请号：US10432456
申请日：2001-11-20
CPC分类号： F41H5/0435 , B32B2315/02 , C04B35/563 , C04B35/565 , C04B35/573 , C04B35/62655 , C04B2235/3821 , C04B2235/3826 , C04B2235/405 , C04B2235/422 , C04B2235/428 , C04B2235/48 , C04B2235/5248 , C04B2235/5436 , C04B2235/5472 , C04B2235/6562 , C04B2235/6565 , C04B2235/6581 , C04B2235/77 , C04B2235/80 , C04B2235/94 , C04B2235/96 , C04B2237/365 , F41H5/0414 , Y10T428/30 , Y10T428/31634
摘要： A composite body produced by a reactive infiltration process that possesses high mechanical strength, high hardness and high stiffness has applications in such diverse industries as precision equipment and ballistic armor. Specifically, the composite material features a boron carbide filler or reinforcement phase, and a silicon component with a porous mass having a carbonaceous component. Potential deleterious reaction of the boron carbide with silicon during infiltration is suppressed by alloying or dissolving boron into the silicon prior to contact of the silicon infiltrant with the boron carbide. In a preferred embodiment of the invention related specifically to armor, good ballistic performance can be advanced by loading the porous mass or preform to be infiltrated to a high degree with one or more hard fillers such as boron carbide, and by limiting the size of the largest particles making up the mass. The instant reaction bonded silicon carbide (RBSC) composite bodies surpass previous RBSC's as armor materials, and in this capacity approach the ballistic performance of current carbide armor ceramics but with potentially lower cost manufacturing methods, e.g., infiltration techniques.
摘要翻译： 通过具有高机械强度，高硬度和高刚度的反应性渗透方法生产的复合体可用于精密设备和防弹装甲等多种行业。 具体地说，复合材料具有碳化硼填料或增强相，而具有多孔质量的硅组分具有含碳成分。 渗碳过程中碳化硼与硅的潜在有害反应可以通过在硅渗透剂与碳化硼接触之前将硼合金化或溶解到硅中来抑制。 在本发明的一个优选实施方案中，具体涉及铠装，通过将一种或多种硬质填料例如碳化硼加载到高度渗透的多孔质量体或预型体，可以提高良好的弹道性能，并且通过限制 弥补质量的最大颗粒。 即时反应结合的碳化硅（RBSC）复合体超过以前的RBSC作为装甲材料，并且在这种能力下接近目前的碳化铠装陶瓷的弹道性能，但具有潜在的较低成本的制造方法，例如渗透技术。
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