SYNTHESIS OF MSE-FRAMEWORK TYPE MOLECULAR SIEVES
    68.
    发明申请
    SYNTHESIS OF MSE-FRAMEWORK TYPE MOLECULAR SIEVES 有权
    MSE-FRAMEWORK型分子筛的合成

    公开(公告)号:US20150087841A1

    公开(公告)日:2015-03-26

    申请号:US14541777

    申请日:2014-11-14

    IPC分类号: C07D453/02 C07D211/12

    摘要: A method of synthesizing a crystalline molecular sieve having an MSE framework type comprises crystallizing a reaction mixture comprising a source of water, a source of an oxide of a tetravalent element, Y, selected from at least one of silicon, tin, titanium, vanadium, and germanium, optionally a source of a trivalent element, X, a source of an alkali or alkaline earth metal, M, and a source of organic dications, Q, such as 3-hydroxy-1-(4-(1-methylpiperidin-1-ium-1-yl)butyl)quinuclidin-1-ium, 3-hydroxy-1-(5-(1-methylpiperidin-1-ium-1-yl)pentyl)quinuclidin-1-ium, 1,1′-(butane-1,4-diyl)bis(1-methylpiperidin-1-ium), 1,1′-(pentane-1,5-diyl)bis(1-methylpiperidin-1-ium), 1,1′-(hexane-1,6-diyl)bis(1-methylpiperidin-1-ium), and 1,1′-((3as,6as)-octahydropentalene-2,5-diyl)bis(1-methylpiperidin-1-ium).

    摘要翻译: 合成具有MSE骨架类型的结晶分子筛的方法包括使包含水源,四价元素的氧化物源Y的反应混合物结晶,Y选自硅,锡,钛,钒, 和锗,任选的三价元素的源,X,碱金属或碱土金属的源,M和有机二价元素的Q,例如3-羟基-1-(4-(1-甲基哌啶-4-基) (1-(1-甲基哌啶-1-基)戊基)奎宁环ium,1,1'ium基-1- yl基)丁基)奎宁环ium,3-羟基-1- - (丁烷-1,4-二基)双(1-甲基哌啶-1-基),1,1' - (戊烷-1,5-二基)双(1-甲基哌啶-1-基),1,1' - (己烷-1,6-二基)双(1-甲基哌啶-1-基)和1,1' - ((3as,6as) - 八氢二烯-2,5-二基)双(1-甲基哌啶-1-基) ium)。

    EMM-11, A Novel Synthetic Crystalline Microporous Material, Its Preparation and Use
    69.
    发明申请
    EMM-11, A Novel Synthetic Crystalline Microporous Material, Its Preparation and Use 失效
    EMM-11,一种新型合成结晶微孔材料,其制备与应用

    公开(公告)号:US20120160773A1

    公开(公告)日:2012-06-28

    申请号:US13418216

    申请日:2012-03-12

    摘要: EMM-11 is a novel synthetic crystalline microporous material having a single crystalline phase with a unique 3-dimensional channel system comprising three sets of channels, namely a first set comprising 10-ring channels, and a second set and third set comprising 8-ring channels, having a unique T-atom connectivity and X-ray diffraction pattern which identify it as a novel material, and may be prepared with an organic structure directing agent, preferably, 3-isopropyl-1-methyl-1H-imidazol-3-ium. EMM-11 may be used in organic compounds conversion and absorptive processes.

    摘要翻译: EMM-11是具有单一结晶相的新型合成结晶微孔材料,其具有独特的3维通道系统,该三维通道系统包括三组通道,即包含10环通道的第一组,第二组和第三组包含8-环 通道,具有独特的T原子连接性和X射线衍射图,将其识别为新型材料,并且可以用有机结构导向剂(优选3-异丙基-1-甲基-1H-咪唑-3-基) ium。 EMM-11可用于有机化合物的转化和吸收过程。