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130 条记录 (耗时 0.032 秒)

    High purity 2-naphthylacetonitrile and method for producing same
    62.
    发明授权
    High purity 2-naphthylacetonitrile and method for producing same 有权

    公开(公告)号：US12037307B2

    公开(公告)日：2024-07-16

    申请号：US17824393

    申请日：2022-05-25

    申请人： API CORPORATION

    发明人： Masaki Nagahama ,  Daiki Okado ,  Hirotsugu Taniike

    IPC分类号： C07C255/33 ,  C07C253/22

    CPC分类号： C07C253/22 ,  C07C255/33

    摘要： The present invention provides high purity 2-naphthylacetonitrile with fewer impurities that is useful as a starting material or intermediate for the synthesis of various pharmaceutical products, agricultural chemicals, and chemical products, and a production method thereof. A high purity 2-naphthylacetonitrile having an HPLC purity of 2-naphthylacetonitrile of not less than 95 area %, and containing naphthalene compounds represented by the formulas (a)-(j) at a content of a predetermined area % or below. A method for producing high purity 2-naphthylacetonitrile, including the following step 1 and step 2: step 1: a step of subjecting 2′-acetonaphthone to a Willgerodt reaction in the presence of an additive where necessary, and hydrolyzing the obtained amide compound to give 2-naphthylacetic acid; step 2: a step of reacting the 2-naphthylacetic acid obtained in step 1, a halogenating agent and sulfamide in the presence of a catalyst as necessary in an organic solvent to give 2-naphthylacetonitrile.

    Perfuming ingredients of the floral and/or anis type
    68.
    发明授权
    Perfuming ingredients of the floral and/or anis type 有权
    花香和/或茴香型香料成分

    公开(公告)号：US08268895B2

    公开(公告)日：2012-09-18

    申请号：US13123147

    申请日：2009-11-03

    申请人： Robert Moretti

    发明人： Robert Moretti

    IPC分类号： A61K8/30 ,  A61K8/02 ,  A61K8/00 ,  A61Q5/00 ,  A61Q15/00 ,  A61Q19/10 ,  A61Q13/00 ,  A61L9/00

    CPC分类号： C07C47/232 ,  A61Q5/02 ,  A61Q9/02 ,  A61Q13/00 ,  A61Q19/00 ,  C07C45/292 ,  C07C45/513 ,  C07C47/277 ,  C07C255/33 ,  C11B9/0061 ,  C11B9/0065

    摘要： The present invention concerns the use as perfuming ingredient, for instance to impart odor notes of the floral and/or green type, of a compound of formula 5 wherein R is an ortho, meta or para substituent of the phenyl, and represents a hydrogen atom or a C 1-2 alkyl or alkoxyl group; R 1 represents a hydrogen atom or a methyl or ethyl group; 10 R 2 represents a hydrogen atom or a C 1-3 alkyl group; and X represents a CHO, COOR 3, CH(OR 4) 2 or CN group, R 3 being a methyl or ethyl group, and R 4, taken seperately, being a methyl or ethyl group, or said R 4, taken together, a C 2-5 alkanediyl group; and at least one of said R, R 1 or R 2 represents a group containing at least one carbon atom.

    摘要翻译： 本发明涉及作为加香成分的用途，例如赋予花香和/或绿色类型的气味，式5的化合物，其中R是苯基的邻位，间位或对位取代基，代表氢原子 或C 1-2烷基或烷氧基; R 1表示氢原子或甲基或乙基; 10 R 2表示氢原子或C 1-3烷基; 并且X表示CHO，COOR 3，CH（OR 4）2或CN基团，R 3为甲基或乙基，R 4分别为甲基或乙基，或所述R 4一起， C 2-5烷二基; 并且所述R，R 1或R 2中的至少一个表示含有至少一个碳原子的基团。