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61.发明授权Regeneration of an acidic ionic liquid catalyst by addition of brønsted acids 有权通过添加布朗斯台德酸来再生酸性离子液体催化剂公开(公告)号：US09079176B1
公开(公告)日：2015-07-14
申请号：US14229329
申请日：2014-03-28
申请人： UOP LLC
CPC分类号： B01J31/4053 , B01J31/0277 , B01J31/0288 , B01J31/26 , B01J31/4092 , B01J2231/323 , C07C2/60 , C07C2527/125 , C07C2531/02 , Y02P20/584 , C07C9/16
摘要： A method for regenerating deactivated acidic ionic liquid catalyst containing conjunct polymer is described. The method includes contacting the deactivated acidic ionic liquid catalyst containing the conjunct polymer with at least one Brønsted acid in a regeneration zone under regeneration conditions, resulting in a mixture comprising regenerated acidic ionic liquid catalyst, the Brønsted acid, the released conjunct polymer. The Brønsted acid is derived from a mineral acid and contains at least one organic group. The released conjunct polymer can be separated from the regenerated acidic ionic liquid catalyst and the at least one Brønsted acid.
摘要翻译： 描述了一种用于再生含有结合聚合物的失活酸性离子液体催化剂的方法。 该方法包括在再生条件下将含有结合聚合物的失活的酸性离子液体催化剂与再生区中的至少一种布朗斯台德酸接触，得到包含再生酸性离子液体催化剂布朗斯台德酸，释放的结合聚合物的混合物。 布朗斯台德酸衍生自无机酸，并含有至少一个有机基团。 释放的结合聚合物可以与再生的酸性离子液体催化剂和至少一种布朗斯台德酸分离。
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公开(公告)号：US08906819B2
公开(公告)日：2014-12-09
申请号：US12650037
申请日：2009-12-30
申请人： Michael D. Cooper , Nagesh Patel
发明人： Michael D. Cooper , Nagesh Patel
IPC分类号： B01J38/48 , B01J38/60 , B01J38/62 , B01J38/50 , B01J23/92 , B01J38/64 , B01J38/66 , B01J23/22 , B01J23/30
摘要： This invention is directed to a method for removing calcium material from a substrate or catalytic converter. In particular, this invention is directed to a method for removing calcium material, particularly in the form of calcium-containing fly ash, from a substrate using a partially protonated or non-protonated polycarboxylic acid treatment material.
摘要翻译： 本发明涉及从基材或催化转化器中除去钙物质的方法。 特别地，本发明涉及使用部分质子化或非质子化的多元羧酸处理材料从基材除去钙材料，特别是含钙飞灰的形式的方法。
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公开(公告)号：US20120004091A1
公开(公告)日：2012-01-05
申请号：US13233491
申请日：2011-09-15
申请人： Bo Kou , Julie Chabot
发明人： Bo Kou , Julie Chabot
CPC分类号： C10G47/02 , C10G47/26 , C10G47/32 , C10G65/00 , C10G65/10 , C10G65/18 , C10G2300/205 , C10G2300/206 , C10G2300/701 , C10G2300/802
摘要： A method to prepare an improved catalyst feed to a system to upgrade heavy oil. The method comprises: providing a spent catalyst that has been used in a hydroprocessing operation has with a solid content ranging from 5 to 50 wt. % in soluble hydrocarbons and having less than 80% but more than 10% of original catalytic activity; removing at least 50% of the soluble hydrocarbons removed in a deoiling step; treating the deoiled spent catalyst with a treating solution containing at least one of plain water, a mineral acid, an oxidizing agent, and combinations thereof to reduce the concentration of at least one metal contaminant in the deoiled spent catalyst by at least 40%. After treatment, the treated deoiled spent catalyst is slurried in a hydrocarbon medium, and fed to the heavy oil upgrade system as part of the catalyst feed system with a fresh slurry catalyst.
摘要翻译： 一种制备改进的催化剂进料到系统以升级重油的方法。 该方法包括：提供已经在加氢操作中使用的废催化剂的固体含量范围为5-50wt。 ％的可溶性碳氢化合物，并且具有小于80％但大于10％的原始催化活性; 去除在脱油步骤中去除的至少50％的可溶性烃; 用含有浅水，无机酸，氧化剂及其组合中的至少一种的处理溶液处理脱油的废催化剂，以将去除的废催化剂中的至少一种金属污染物的浓度降低至少40％。 处理后，经处理的脱油废催化剂在烃介质中浆化，并作为催化剂进料系统的一部分用新鲜的浆料催化剂进料至重油升级系统。
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64.发明授权Ionic liquid catalyst regenerated using a regeneration metal in the presence of added hydrogen 有权离子液体催化剂在加入氢气存在下使用再生金属再生公开(公告)号：US07956002B2
公开(公告)日：2011-06-07
申请号：US12759424
申请日：2010-04-13
申请人： Saleh Elomari , Thomas V. Harris
发明人： Saleh Elomari , Thomas V. Harris
IPC分类号： B01J20/34 , B01J21/20 , B01J23/90 , B01J25/04 , B01J27/28 , B01J29/90 , B01J38/48 , B01J38/60 , B01J31/00 , B01J31/40 , B01J38/00
CPC分类号： B01J31/26 , B01J31/0284 , B01J31/4015 , B01J31/403 , B01J38/10
摘要： An ionic liquid catalyst, which has been regenerated by contacting a used ionic liquid catalyst with at least one regeneration metal in a regeneration zone in the presence of added hydrogen under regeneration conditions for a time sufficient to increase the activity of the ionic liquid catalyst. Also, an ionic liquid catalyst which has been regenerated by contacting a used ionic liquid catalyst with at least one regeneration metal in a regeneration zone in the presence of added hydrogen under regeneration conditions in the presence of an inert hydrocarbon in which conjunct polymers are soluble for a time sufficient to increase the activity of the ionic liquid catalyst.
摘要翻译： 一种离子液体催化剂，其通过在再生条件下在加入的氢气存在下在再生区中使用离子液体催化剂与至少一种再生金属接触一段时间来再生足以提高离子液体催化剂活性的时间。 此外，离子液体催化剂已经通过在再生区中在加氢的存在下在再生条件下在惰性烃存在下在再生区中使用离子液体催化剂与再生金属进行再生，其中结合聚合物可溶于 足以增加离子液体催化剂活性的时间。
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公开(公告)号：US20110008238A1
公开(公告)日：2011-01-13
申请号：US12920338
申请日：2009-03-02
CPC分类号： B01J23/96 , B01J21/18 , B01J23/42 , B01J37/20 , B01J38/02 , B01J38/60 , C01B21/1418 , C07C5/03 , C07C5/08 , Y02P20/584
摘要： A process for regenerating hydrogenation catalysts based on a platinum metal, where the hydrogenation catalysts based on a platinum metal are thermally regenerated at temperatures of from 50 to 600° C.
摘要翻译： 一种基于铂金属再生氢化催化剂的方法，其中基于铂金属的氢化催化剂在50-600℃的温度下热再生。
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公开(公告)号：US20100305365A1
公开(公告)日：2010-12-02
申请号：US12784870
申请日：2010-05-21
CPC分类号： B01J31/10 , B01J31/4007 , B01J2231/347 , C07C37/20 , Y02P20/584 , C07C39/16
摘要： The invention relates to a method for regenerating acidic cation exchangers, which are used as catalysts in the reaction of phenols with aldehydes or ketones to give bisphenols, in particular to give bisphenol A, with acids, with the proviso that, in the method according to the invention, these cation exchangers experience very little mechanical damage due to swelling processes during the regeneration process.
摘要翻译： 本发明涉及一种用于再生酸性阳离子交换剂的方法，其用作苯酚与醛或酮反应的催化剂，以产生双酚，特别是产生双酚A与酸，条件是在根据 在本发明中，这些阳离子交换剂在再生过程中由于溶胀过程而经历很少的机械损伤。
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公开(公告)号：US20100160146A1
公开(公告)日：2010-06-24
申请号：US12639707
申请日：2009-12-16
CPC分类号： B01J31/403 , B01J23/75 , B01J38/02 , B01J38/10 , B01J38/66 , B01J2531/845 , C10G2/332 , C10G2300/70
摘要： A process for regenerating one or more deactivated cobalt comprising Fischer-Tropsch catalyst particle(s) in situ in a reactor tube, said process comprising the steps of: (i) oxidising the catalyst particle(s) at a temperature between 20 and 400° C.; (ii) treating the catalyst particle(s) for more than 5 minutes with a solvent, (iii) drying the catalyst particle(s); and (iv) optionally reducing the catalyst with hydrogen or a hydrogen comprising gas. This process may be preceded by a step in which Fischer-Tropsch product is removed from the catalyst particle(s).
摘要翻译： 一种在反应器管中原位再生一种或多种包含费 - 托催化剂颗粒的失活的钴的方法，所述方法包括以下步骤：（i）在20-400℃的温度下氧化催化剂颗粒 C。; （ii）用溶剂处理催化剂颗粒超过5分钟，（iii）干燥催化剂颗粒; 和（iv）任选地用氢或包含气体的氢还原催化剂。 此过程之前可以是从催化剂颗粒中除去费 - 托产物的步骤。
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公开(公告)号：US20090291823A1
公开(公告)日：2009-11-26
申请号：US12534677
申请日：2009-08-03
申请人： Marcel Foerster
发明人： Marcel Foerster
摘要： The invention relates to a method for regenerating denox catalysts having an increased SO2/SO3 conversion rate as a result of the cumulation of iron compounds, and is characterized in that the catalysts are treated with an essentially aqueous acid solution, preferably having a pH between 0.5 and 4, and with an addition of antioxidants.
摘要翻译： 本发明涉及一种由于铁化合物的累积而再生具有增加的SO 2 / SO 3转化率的脱氧催化剂的方法，其特征在于催化剂用基本上含水的酸溶液处理，优选pH在0.5 和4，并加入抗氧化剂。
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公开(公告)号：US20050059544A1
公开(公告)日：2005-03-17
申请号：US10726203
申请日：2003-12-02
申请人： Karl Steigleder , Veronica Godfrey , Kerry Boehner
发明人： Karl Steigleder , Veronica Godfrey , Kerry Boehner
IPC分类号： B01J27/16 , B01J29/40 , B01J29/65 , B01J29/70 , B01J29/90 , B01J37/00 , B01J38/12 , B01J38/60 , B01J38/66 , B01J27/199
CPC分类号： B01J29/061 , B01J27/16 , B01J29/40 , B01J29/405 , B01J29/65 , B01J29/70 , B01J29/7034 , B01J29/90 , B01J37/0009 , B01J38/12 , B01J38/60 , B01J38/66 , B01J2229/26 , B01J2229/36 , B01J2229/40 , B01J2229/42
摘要： This invention relates to a process for reactivating a dehydrocyclodimerization catalyst. Dehydrocyclodimerization catalysts which contain an aluminum phosphate binder can be deactivated when they are exposed to hydrogen at temperatures above 500° C. The instant process restores substantially all of the catalyst's lost activity. The process involves treating the catalyst with a fluid comprising water and drying the catalyst. The process is employed particularly advantageously in combination with coke removal for reactivating catalysts that contain coke deposits and that have also been hydrogen deactivated. This invention also relates to a method of producing a dehydrocyclodimerization catalyst that is resistant to hydrogen deactivation.
摘要翻译： 本发明涉及一种使脱氢环二聚化催化剂再活化的方法。 含有磷酸铝粘合剂的脱氢环化二聚催化剂在高于500℃的温度下暴露于氢气时可以失活。本工艺基本恢复所有催化剂的失活活性。 该方法包括用包含水的流体处理催化剂并干燥催化剂。 该方法特别有利地结合焦炭去除以再活化含有焦炭沉积物的催化剂并且还被氢去活化。 本发明还涉及一种耐氢失活的脱氢环化二聚催化剂的制备方法。
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公开(公告)号：US06861383B2
公开(公告)日：2005-03-01
申请号：US10181597
申请日：2001-01-19
IPC分类号： B01J21/06 , B01J21/20 , B01J38/12 , B01J38/60 , B01J38/64 , B01J38/66 , B01J38/68 , C07B61/00 , C07D301/12 , C07D301/19 , B01J20/34
CPC分类号： C07D301/19 , B01J21/20 , B01J38/12 , B01J38/60 , B01J38/66 , Y02P20/584
摘要： A process for the preparation of a catalyst support material involving the steps of: (a) subjecting a used titania-on-silica catalyst to a decoking treatment, (b) washing the decoked catalyst with a washing liquid selected from an aqueous solution of a mineral acid, an aqueous solution of an ammonium salt and combinations thereof, and (c) drying and calcining the washed and decoked catalyst to yield the catalyst support material. The support material thus obtained is suitably used as support material for titania in a heterogeneous catalyst for the epoxidation of olefins into alkylene oxides.
摘要翻译： 一种制备催化剂载体材料的方法，包括以下步骤：（a）使用二氧化钛 - 二氧化硅催化剂进行脱焦处理，（b）用选自以下的洗涤液体洗涤脱色催化剂： 无机酸，铵盐的水溶液及其组合，以及（c）干燥和煅烧洗涤过的和经过开馏的催化剂以产生催化剂载体材料。 由此获得的载体材料适合用作用于将烯烃环氧化成环氧烷烃的非均相催化剂中的二氧化钛的载体材料。
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