摘要:
The disclosure relates to methods for producing amide bonds and reagents related thereto. In some embodiments, the disclosure relates to methods of producing an amide comprising mixing an O-silylated thionoester and an amine under conditions such that an amide is formed. In another embodiment, the disclosure relates to mixing a thiolacid, a silylating agent, and an amine under conditions such that an amide is formed.
摘要:
A pressure compensator including a housing, an electroactive polymer (EAP) disposed in the housing and defining a volume therein, the volume being changeable upon application of an electric signal. A method for managing pressure in a tool including applying an electrical signal to the pressure compensator and changing a shape of the EAP to change the volume of the compensator whereby the pressure in the tool is altered. A borehole system including a borehole in a subsurface formation, a string in the borehole, a pressure compensator disposed within or as a part of the string.
摘要:
A trigger including a carrier, a shuttle movably disposed on the carrier, an energy member disposed between the carrier and the shuttle, a degrade-on-demand trip member disposed to maintain potential energy in the energy member until activated. A method for operating a downhole tool including sending a signal to the trip member of the trigger, degrading the trip member, converting potential energy stored in the energy member from potential energy to kinetic energy, and actuating the downhole tool with the shuttle. A wellbore system including a borehole in a subsurface formation, a string in the borehole, a trigger disposed within or as a part of the string.
摘要:
A magnesium halide adduct represented by the formula (I): MgX2.mROH.nE.pH2O, in which X is chlorine, bromine, a C1-C12 alkoxy, a C3-C10 cycloalkoxy or a C6-C10 aryloxy, with the proviso that at least one X is chlorine or bromine; R is a C1-C12 alkyl, a C3-C10 cycloalkyl or a C6-C10 aryl; E is an o-alkoxybenzoate compound represented by the formula (II): in which R1 and R2 groups are independently a C1-C12 linear or branched alkyl, a C3-C10 cycloalkyl, a C6-C10 aryl, a C7-C10 alkaryl or an C7-C10 aralkyl, the R1 and R2 groups are identical to or different from the R group; m is in a range of from 1.0 to 5.0; n is in a range of from 0.001 to 0.5; and p is in a range of from 0 to 0.8, is disclosed. A catalyst component useful in olefin polymerization, which comprises a reaction product of (1) the magnesium halide adduct, (2) a titanium compound, and optionally (3) an electron donor compound, is also disclosed.
摘要:
A catalyst component for olefin polymerization is disclosed, which comprises a reaction product of the following components: (1) a spheric carrier; (2) a titanium compound; and optionally, (3) an electron donor, wherein the spheric carrier comprises a reaction product of at least the following components: (a) a magnesium halide represented by a general formula of MgX2-nRn, wherein X is independently chloride or bromide, R is a C1-C14 alkyl, a C6-C14 aryl, a C1-C14 alkoxy, or a C6-C14 aryloxy, and n is 0 or 1; (b) an alcohol compound; and (c) an epoxy compound represented by a general formula (I), wherein R2 and R3 are independently hydrogen, a C1-C5 linear or branched alkyl, or a C1-C5 linear or branched haloalkyl. When the catalyst of the invention is used in olefin polymerization, in particular in propylene polymerization, at least one of the following desired effects can be achieved: high polymerization activity of catalyst, high stereospecificity of catalyst, good hydrogen response of catalyst, high stereoregularity of polymer having high melt index, and low content of polymer fines.
摘要:
The present invention discloses a method for assigning the carrier frequency in a trunking system, which includes: after the base station subsystem receiving a group call request, it assigns a carrier frequency reference for this group call, by which to establish the forward channels of the group users managed by the base station subsystem. With the method offered by the present invention, all the group members under a base station subsystem could be established on the same carrier frequency reference as far as possible, thereby sharing of the wireless channels.
摘要:
FIG. 1 is a perspective view of the oven, showing my new design, shown with the lid in open condition; FIG. 2 is a perspective view thereof; FIG. 3 is a front elevational view thereof; FIG. 4 is a rear elevational view thereof; FIG. 5 is a left side elevational view thereof; FIG. 6 is a right side elevational view thereof; FIG. 7 is a top plan view thereof; FIG. 8 is a bottom plan view thereof; FIG. 9 is a partially enlarged view thereof, taken from FIG. 1; and, FIG. 10 is a partially enlarged view thereof, taken from FIG. 2. The broken lines shown portions of the Oven that form no part of the claimed design.
摘要:
A downhole assembly includes a disintegrable article, which contains a polymer matrix comprising a polymer having an oxygen content of about 2 wt % to about 30 wt %; an energetic material configured to generate heat upon activation to facilitate a chemical decomposition of the polymer; and at least one of a reinforcing fiber or a filler. The disintegrable article is disintegrated by disposing the downhole assembly in a downhole environment; performing a downhole operation; exposing the polymer in the polymer matrix to the generated heat to chemically decompose the polymer producing a decomposed product containing a small molecule in a supercritical state; and disintegrating the disintegrable article with the small molecule in the supercritical state.
摘要:
A catalyst component for olefin polymerization is disclosed, which comprises a reaction product of the following components: (1) a spheric carrier; (2) a titanium compound; and optionally, (3) an electron donor, wherein the spheric carrier comprises a reaction product of at least the following components: (a) a magnesium halide represented by a general formula of MgX2-nRn, wherein X is independently chloride or bromide, R is a C1-C14 alkyl, a C6-C14 aryl, a C1-C14 alkoxy, or a C6-C14 aryloxy, and n is 0 or 1; (b) an alcohol compound; and (c) an epoxy compound represented by a general formula (I), wherein R2 and R3 are independently hydrogen, a C1-C5 linear or branched alkyl, or a C1-C5 linear or branched haloalkyl. When the catalyst of the invention is used in olefin polymerization, in particular in propylene polymerization, at least one of the following desired effects can be achieved: high polymerization activity of catalyst, high stereospecificity of catalyst, good hydrogen response of catalyst, high stereoregularity of polymer having high melt index, and low content of polymer fines.
摘要:
A non-faceted nanoparticle reinforced metal matrix composite having increased ductility, while maintaining strength. In particular, a non-faceted nanoparticle reinforced metal matrix composite is provided comprised of spherical or ellipsoidal shaped (non-faceted) nanoparticles comprising one or more of boron carbide, titanium diboride, silicon nitride, alumina and boron nitride, and a nanostructured matrix composite comprised of one or more metals and/or metal alloys. In addition, a method of manufacturing such a non-faceted nanoparticle reinforced metal matrix composite is provided.