-
公开(公告)号：US20100266489A1
公开(公告)日：2010-10-21
申请号：US12738246
申请日：2008-08-20
申请人： Hartwig Rauleder , Ekkehard Mueh , Jaroslaw Monkiewicz , Hans Juergen Hoene , Raymund Sonnenschein
发明人： Hartwig Rauleder , Ekkehard Mueh , Jaroslaw Monkiewicz , Hans Juergen Hoene , Raymund Sonnenschein
CPC分类号： C01B33/046 , B01D53/02 , B01D2253/108 , C01B33/10784
摘要： The invention relates to a method for the treatment of a composition containing inorganic silanes and at least one foreign metal and/or a compound containing a foreign metal, wherein the composition is brought in contact with at least one adsorption agent, and for obtaining the composition, in which the content of foreign metal and/or of a compound containing a foreign metal is reduced, and to a corresponding composition having a reduced foreign metal content, and further to the use of organic resins, activated carbons, silicates, and/or zeolites for the reduction of foreign metals and/or compounds containing foreign metals in compositions of inorganic silanes.
摘要翻译： 本发明涉及一种处理包含无机硅烷和至少一种外来金属和/或含有外来金属的化合物的组合物的方法，其中所述组合物与至少一种吸附剂接触，并且用于获得组合物 ，其中外来金属和/或含有外来金属的化合物的含量降低，并且降低了外来金属含量降低的相应组合物，并且还使用有机树脂，活性炭，硅酸盐和/或 用于在无机硅烷组合物中还原外来金属和/或含有外来金属的化合物的沸石。
-
公开(公告)号：US20070249785A1
公开(公告)日：2007-10-25
申请号：US11569585
申请日：2005-04-04
申请人： Ekkehard Muh , Hartwig Rauleder , Harald Klein
发明人： Ekkehard Muh , Hartwig Rauleder , Harald Klein
IPC分类号： C07F7/18
CPC分类号： C07F7/188
摘要： The present invention relates to a specific process for preparing organosilane esters of the formula (I) and a composition comprising more than 98% by weight of organosilane esters of the formula (I) and less than 2.0% by weight of at least one hydrocarbon and to the use of such a composition as precursor for producing a layer or film having a dielectric constant of 1
摘要翻译： 本发明涉及制备式（I）的有机硅烷酯和包含大于98重量％的式（I）的有机硅烷酯和小于2.0重量％的至少一种烃的组合物的具体方法，以及 使用这种组合物作为制备介电常数为1 <κ4的层或膜的前体。
-
公开(公告)号：US06402961B1
公开(公告)日：2002-06-11
申请号：US09621076
申请日：2000-07-21
申请人： Stefan Bade , Uwe Schoen , Hartwig Rauleder
发明人： Stefan Bade , Uwe Schoen , Hartwig Rauleder
IPC分类号： B01D1508
CPC分类号： C07F7/1892
摘要： A process for preparing epoxysilanes by reacting a hydrogensilane with an allyl glycidyl ether in the presence of a catalyst and working up the crude product obtained, where the catalyst is removed from the crude product and the crude product is subsequently distilled.
摘要翻译： 一种通过在催化剂存在下使氢硅烷与烯丙基缩水甘油醚反应来制备环氧硅烷的方法，并处理所得到的粗产物，其中从粗产物中除去催化剂和粗产物。
-
84.发明授权公开(公告)号：US06297188B1
公开(公告)日：2001-10-02
申请号：US09427926
申请日：1999-10-27
申请人： Reinhold Schork , Burkhard Standke , Hartwig Rauleder , Albert-Johannes Frings , Michael Horn , Peter Jenkner , Jaroslaw Monkiewicz
发明人： Reinhold Schork , Burkhard Standke , Hartwig Rauleder , Albert-Johannes Frings , Michael Horn , Peter Jenkner , Jaroslaw Monkiewicz
IPC分类号： B01J3100
摘要： Particulate magnesium ethoxide having a high coarse particle content can be obtained in a simple and economical manner by the present invention, which provides a process for preparing particulate magnesium ethoxide having a coarse grain content, and includes reacting metallic, optionally activated, magnesium with liquid ethanol under pressure at a temperature above 78° C. The present invention also relates to particulate magnesium ethoxide having a coarse grain content, which contains: 500 &mgr;m.
摘要翻译： 通过本发明可以以简单和经济的方式获得具有高粗颗粒含量的颗粒状乙醇镁，其提供了制备具有粗颗粒含量的颗粒状乙醇镁的方法，并且包括使金属，任选活化的镁与液态乙醇 在78℃以上的压力下，本发明还涉及具有粗颗粒含量的颗粒状的乙醇镁，其含有：<40重量％的筛选分数<=500μm和> = 60重量％ 筛选分数> 500 mum。
-
公开(公告)号：US06242630B1
公开(公告)日：2001-06-05
申请号：US08908095
申请日：1997-08-11
申请人： Stefan Bade , Uwe Schoen , John Burkhard , Franz-Michael Bollenrath , Norbert Hofmann , Hermann-Josef Korte , Hartwig Rauleder , Uwe Tanger
发明人： Stefan Bade , Uwe Schoen , John Burkhard , Franz-Michael Bollenrath , Norbert Hofmann , Hermann-Josef Korte , Hartwig Rauleder , Uwe Tanger
IPC分类号： C07F708
CPC分类号： C07F7/14 , C07F7/0829 , C07F7/1876
摘要： A process for the continuous preparation of 3-halopropylorganosilanes of the general structure RbH3-a-bXaSiCH2CH2CH2Y (III), where: R is CH3, C2H5, C3H7, OCH3, OC2H5 or OC3H7, X is F, Cl, Br or I, Y is F, Cl, Br or I, and a and b are each one of the numbers 0, 1, 2 or 3 and the sum a+b is 1, 2 or 3, comprising reacting, as starting materials, an allyl halide with a silane carrying at least one H atom, wherein the starting materials are present in stoichiometric amounts or one of the starting materials is present in substoichiometric amounts, wherein the reaction carried out is a partial reaction of from 10% to 80%, on a molar basis, of the starting materials, based on either material, when both are present in stoichiometric amounts, or based on the substoichiometric material.
摘要翻译： 连续制备通常结构的3-卤代丙基有机硅烷的方法，其中R为CH 3，C 2 H 5，C 3 H 7，OCH 3，OC 2 H 5或OC 3 H 7，X为F，Cl，Br或I，Y为F，Cl，Br或I， 和b分别为数字0,1,2或3中的一个，并且和a + b为1,2或3，包括使烯丙基卤化物与携带至少一个H原子的硅烷作为原料，其中， 原料以化学计量的量存在，或者一种起始原料以亚化学计量的量存在，其中进行的反应是基于摩尔的10％至80％的起始原料的部分反应，基于任一材料 ，当两者都以化学计量的量存在时，或基于亚化学计量的材料。
-
公开(公告)号：US5939575A
公开(公告)日：1999-08-17
申请号：US978189
申请日：1997-11-25
CPC分类号： C07F7/1896
摘要： Acyloxysilanes are prepared by a process of reacting an organochlorosilane with an excess of monocarboxylic anhydride at elevated temperature, thereby forming product acyloxysilane and by-product acyl chloride transferring the reaction mixture to the middle inlet of a separation tower having a still pot at its base, removing excess carboxylic anhydride by distillation at the tower top under reduced pressure, removing acyl chloride by-product from the separation tower, uniformly removing acyloxysilane from the tower still pot, and reacting virtually quantitatively the residual acid chloride present in the acyloxysilane removed from the still pot by adding a metal carboxylate to the acyloxysilane and separating the metal chlorides formed from the product.
摘要翻译： 通过在高温下使有机氯硅烷与过量的单羧酸酐反应的方法制备出甲氧基硅烷，从而形成产物酰氧基硅烷和副产物酰氯，将反应混合物转移到其底部具有静止釜的分离塔的中间入口， 通过在减压下在塔顶蒸馏除去过量的羧酸酐，从分离塔除去酰氯副产物，从塔釜中均匀除去酰氧基硅烷，并且实际上定量地反应从静止物中除去的酰氧基硅烷中残留的酰氯 通过向酰氧基硅烷中加入金属羧酸盐并分离由产物形成的金属氯化物。
-
公开(公告)号：US5852206A
公开(公告)日：1998-12-22
申请号：US980116
申请日：1997-11-26
CPC分类号： C07F7/20 , C07F7/1896
摘要： A process for removing residual acidic chlorine from acyloxysilanes, comprises virtually quantitatively reacting metal carboxylates with the acidic chlorine present in the acyloxysilane, and the metal chlorides formed being separated off.
摘要翻译： 从酰氧基硅烷中除去残留的酸性氯的方法包括使羧酸金属羧酸与存在于酰氧基硅烷中的酸性氯化物实际上定量反应，形成的金属氯化物被分离出来。
-
88.发明授权Storage-stable solution of carbonated magnesium methoxide in methanol and its use 失效碳酸镁甲醇钠在甲醇中的储存稳定溶液及其用途
公开(公告)号：US5468705A
公开(公告)日：1995-11-21
申请号：US167353
申请日：1993-12-15
IPC分类号： C07C29/70 , C07C29/68 , C07C29/94 , C07C31/30 , C08F4/00 , C08F4/02 , C08F4/50 , C08F10/00 , D21H17/06 , D21H17/63 , D21H25/00 , D21H25/18 , C07F3/02 , B01J31/12 , D21H17/12 , D21H25/02
摘要： The present invention relates to a storage-stable solution of carbonated magnesium methoxide of the formula Mg(CH.sub.3 O).sub.2 (CO.sub.2).sub.n in methanol, and processes for their preparation by reacting metallic magnesium with methanol and CO.sub.2 or reacting magnesium methoxide in methanol with CO.sub.2, wherein the magnesium content of the solution is from 0.1 to 8% by weight, based on the total weight of the solution, and the CO.sub.2 content n is from 1 to 2.2. The present solution is used, inter alia, for the preservation of paper or for the preparation of a catalyst for the polymerization of olefins.
摘要翻译： 本发明涉及在甲醇中的式Mg（CH 3 O）2（CO 2）n的碳酸化甲醇镁的储存稳定溶液，以及通过使金属镁与甲醇和CO 2反应或使甲醇镁与甲醇中的甲醇反应制备的方法 ，其中溶液的镁含量为0.1至8重量％，基于溶液的总重量，并且CO 2含量n为1至2.2。 本溶液尤其用于保存纸或用于制备用于烯烃聚合的催化剂。
-
公开(公告)号：US5227542A
公开(公告)日：1993-07-13
申请号：US938511
申请日：1992-09-01
IPC分类号： C07C29/68
CPC分类号： C07C29/68
摘要： The invention involves spherical particles of magnesium alkoxide and a process for their preparation. Specifically, spherical magnesium alkoxide is produced by spray drying of an alcoholic solution of the corresponding carboxylated magnesium alkoxide and subsequent drying and decarboxylation, characterized in that the solution is sprayed via a two-material nozzle with inner atomization, which is operated in the part-load range at 10 to 30% of its capacity, into an inert accompanying gas which is under a pressure of 1.0 to 1.2 bar, has been preheated to 100.degree.-140.degree. C. and is fed cocurrently, after which the resulting finely divided carboxylated magnesium alkoxide is dried and is decarboxylated. The magnesium alkoxide is used for the preparation of a catalyst for the polymerization of .alpha.-olefins.
摘要翻译： 本发明涉及烷氧基镁的球形颗粒及其制备方法。 具体地说，通过喷雾干燥相应的羧化镁醇盐的醇溶液并随后进行干燥和脱羧来制造球形镁醇盐，其特征在于，所述溶液通过内部雾化的双材料喷嘴喷雾， 将负载范围为其容量的10〜30％，进入压力为1.0〜1.2巴的惰性伴随气体，预热至100-140℃，并且并流，然后将得到的细碎羧化 将醇氧化镁干燥并脱羧。 烷氧基镁用于制备α-烯烃聚合催化剂。
-
90.发明授权Process for the preparation of asymmetric terminally mono-unsaturated glycol ethers 失效制备不对称末端单不饱和二醇醚的方法
公开(公告)号：US4987268A
公开(公告)日：1991-01-22
申请号：US491774
申请日：1990-03-12
摘要： Monoalkylethers of alkyleneglycols and oligoalkyleneglycols are reacted completely with terminally unsaturated alkenyl halides to form terminally mono unsaturated glycolethers as product, wherein initially a complete reaction to the corresponding alcoholate takes place with only one equivalent of alcoholate former, such as alkali metal alcoholate or hydroxide, and two equivalents of glycolmonoether, then the alcoholate is reacted with one equivalent of alkenyl halide, whereupon a mixture of the desired product and the glycolmonoether of the alkali metal halide is filtered or distilled off, then this mixture is reacted with the second equivalent of the alcoholate former, whereupon the recovery of the product takes place by distillation from the reaction mixture and then, after addition of a further equivalent of glycolmonoether to the residue from the product recovery, the reaction of the first and the subsequent steps is repeated.
摘要翻译： 亚烷基二醇和低聚亚烷基二醇的单烷基醚与末端不饱和烯烃卤化物完全反应，形成作为产物的末端单不饱和糖单体，其中最初只用一当量的醇化物，例如碱金属醇盐或氢氧化物与相应的醇化物完全反应， 2当量的二醇单醚，然后醇化物与1当量的烯基卤反应，然后将所需产物和碱金属卤化物的二醇单醚的混合物过滤或蒸除，然后将该混合物与第二当量的醇化物 因此，通过蒸馏从反应混合物中回收产物，然后在从产物回收的残余物中加入另外当量的二醇单醚后，重复第一步骤和随后步骤的反应。
-
-
-
-
-
-
-
-
-
搜索结果
114 条记录 (耗时 0.023 秒)
