摘要:
The present invention provides a method for preparing a carbon nanotube material. In the present invention, a mixture of polyolefin and modified montmorillonite is used as the carbon source. Under the action of a catalyst, a carbon nanotube is synthesized in air. The present invention can address the problem of “white pollution” caused by waste plastics, such as waste polyolefin polymers.
摘要:
The invention relates to a polymeric end-capping reagent for carbon dioxide-epoxide copolymers and a method for producing the same. The polymeric end-capping reagents provided by the invention are maleic anhydride copolymers and maleic anhydride terpolymers. The polymeric end-capping reagent for carbon dioxide-propylene oxide copolymers of the invention is produced by a radical solution copolymerization method, and has a number average molecular weight of Mn=4-6×104, a distribution index of 1.5-3.0. By using the polymeric end-capping reagent provided by the invention, the disadvantages of the small molecular end-capping reagent like volatilization during melting and precipitation on the melt surface during cooling, can be effectively overcome, moreover, the initial thermal decomposition temperatures of the carbon dioxide-propylene oxide copolymers end-capped with the polymeric end-capping reagents increase by about 30° C., as compared with that of the carbon dioxide-propylene oxide copolymer end-capped with “small molecular” maleic anhydride.
摘要:
The present invention relates to a process for preparing rare earth trichromatic phosphor, comprising the following steps: (1) providing precursors for at least one composition formula selected from the group consisting of CaBPO5:xEu:yTb, CaAlrB1-rPO5:xEu:yTb and Ca2B5O9Cl:xEu:yTb, wherein x=0.02–0.05 (mole ratio), y=0.001–0.01 (mole ratio) and r=0.5–0.8; (2) grinding and mixing the precursors; and (3) calcining the product obtained in step (2) at 800–1000° C. for 3–5 hours. According to the present process, only one matrix material and two rare earth reactive ions (Eu3+ and Tb3+) are required to synthesize rare earth trichromatic phosphor. That is to say, no reducing reagent is needed; and absence of reducing agent(s) reduces environmental pollution.
摘要翻译:本发明涉及一种制备稀土三基色荧光粉的方法,包括以下步骤:(1)提供至少一种选自CaBPO 5:xEu:yTb的组成式的前体, u r r> u u u u u u u u u u u u u u u u u u u u u u u u u u u u::/ / / / / / / / / / / / / / / / / / / / / / / / 其中x = 0.02-0.05(摩尔比),y = 0.001-0.01(摩尔比)和r = 0.5-0.8;其中x = 0.02-0.05(摩尔比) (2)研磨和混合前体; 和(3)将步骤(2)中得到的产物在800-1000℃煅烧3-5小时。 根据本发明,只需要一种基质材料和两种稀土反应离子(Eu 3+ + 3+和Tb 3+)来合成稀土三色荧光体。 也就是说,不需要还原剂; 并且没有还原剂减少了环境污染。
摘要:
A field effect transistor in sandwiched configuration having organic semiconductor, comprising: a substrate (1), a gate electrode (2) formed on the surface of the substrate (1), a gate insulation layer (3) formed on the substrate (1) and the gate insulation layer (2), which is characterized in that, further comprising: an active layer (4) formed on the gate insulation layer (3) but leaving a part of the gate insulation layer (3) to be exposed, a source and drain electrodes (5) formed on a part of the gate insulation layer (3) and a part of the active layer (4), and an active layer (6) formed on the exposed part of the gate insulation layer (3), the active layer (4), the source electrode and the drain electrode (5). Taking full advantage of that the organic semiconductor can be processed under low temperature, the present invention adopts two or more kinds of materials to form the active semiconductor layer to make the active layer good contact with the source/drain electrode more effectively and reduce the threshold voltage of the device, and contact the semiconductor with the source/drain electrode and the insulation layer closely and tightly.
摘要:
Provided is a preparation method for a tube. The method comprises the following steps: a) adding a polymer solution into a poor solvent, such that the polymer diffuses on the liquid level of the poor solvent, so as to obtain a polymer film, wherein the solvent in the polymer solution is dissolved in the poor solvent; b) curling the polymer film on the liquid level of the poor solvent by using a mold to obtain a bar; and c) removing the mold to obtain a tube. The present invention further provides the use of the above tubular as an artificial tubular tissue.
摘要:
Provided is a method for preparing a crosslinked polyvinyl chloride structure foamed material by using a physical foaming agent, comprising: melting and mixing a polyvinyl chloride resin, a modified resin, an isocyanate, an anhydride, a nucleating agent and a heat stabilizer to obtain a blank; immersing the blank into a foaming gas for foaming to obtain a foamed body; and subjecting the foamed body to crosslinking curing to obtain a crosslinked polyvinyl chloride structure foamed material. According to the present invention, the crosslinked polyvinyl chloride structure foamed material is prepared by means of a brand-new process route, and the composition and proportion of the PVC resin and other raw materials can be adjusted in a wide range; and carbon dioxide or nitrogen is used for foaming. Further provided is a crosslinked polyvinyl chloride structure foamed material.
摘要:
The present disclosure provides a method for efficiently inducing phase separation of a water-organic solvent mixed solution through an inorganic salt, comprising the following steps: A) adding the inorganic salt to the water-organic matter mixed solution, sonicating and then allowing to stand for complete dissolution of the inorganic salt, wherein the water-organic matter mixed solution is a water-acetonitrile mixed solution or a water-acetone mixed solution; the inorganic salt is one or more of LiCl, NaCl, KCl, CsCl, NaBr, KBr, Li2SO4, Na2SO4 and MgSO4; B) allowing the solution obtained in the step A) to stand in a constant temperature environment until phase separation is completed to obtain a product.
摘要:
A CDDP complex is formed by complexation of CDDP and a polymer having a structure of Formula (I). The CDDP complex has good biocompatibility and is degradable. A side chain of the polymer is grafted with polyethylene glycol, which gives the CDDP complex good dissolvability. When dissolved in an aqueous medium, the CDDP is protected by a hydrophilic polyethylene glycol chain segment and a hydrophobic amino acid chain segment, which can effectively avoid a sudden release of the CDDP due to the influence of the blood circulation system after intravenous injection, thus improving the stability of the CDDP complex. A carboxyl group contained in the CDDP complex has pH value sensitivity and tends to be deprotonated in a low pH environment, which is advantageous for promoting the release of a drug, and improving the efficiency of the drug.
摘要:
This invention relates to a white electroluminescent polymeric material and preparation thereof. Based on the physical idea that white light emission can be achieved by regulating the relative luminous intensities of blue- and orange-light emitting units located in a single polymer molecule, the present invention provides three types (main chain type, pendant chain type, and terminal group type) of high efficiency and stable white electroluminescent polymeric material systems.
摘要:
A method for extracting and separating a rare-earth element by extracting and separating the rare-earth element from an aqueous solution of rare-earth nitrate into n-heptane, with 2-ethylhexyl phosphonic acid mono-2-ethylhexyl ester trialkyl methyl ammonium or di-2-ethylhexyl phosphoric acid trialkyl methyl ammonium as an extractant, and n-heptane as a diluent by contacting the aqueous solution of rare-earth nitrate with the extractant and the diluent to extract and separate the rare earth element into n-heptane from the aqueous solution of rare earth nitrate.