NOVEL TONER EXTERNAL ADDITIVE AND TONER COMPOSITION COMPRISING SAME

    公开(公告)号:US20240192621A1

    公开(公告)日:2024-06-13

    申请号:US18551358

    申请日:2022-05-18

    IPC分类号: G03G9/093 G03G9/097

    摘要: A toner external additive composition of the present invention comprises, as a core component, tin oxide, to be usable as an alternative material for conventional titanium dioxide (TiO2), and thus can respond to future regulations on titanium dioxide and environment. In addition, the toner external additive composition and a toner composition comprising same comprise, as a shell component, a silane-based compound and aluminum hydroxide to reduce triboelectric charge so that a ghost phenomenon is alleviated and increase image density so that print quality is improved. Particularly, if aluminum hydroxide is used in a specific amount range, a print quality improvement effect can be further improved.

    Method for continuously preparing biodegradable aliphatic/aromatic polyester copolymer

    公开(公告)号:US09637589B2

    公开(公告)日:2017-05-02

    申请号:US14423641

    申请日:2013-05-20

    摘要: Provided is a method of continuous preparation of a biodegradable aliphatic/aromatic polyester copolymer, the method including: performing a first esterification reaction of an aliphatic dihydroxy compound and an aliphatic dicarboxylic acid at a temperature of 185° C. or less; continuously performing a second esterification reaction of a reaction product obtained by the first esterification reaction; obtaining a pre-polymer by continuously performing a first polycondensation reaction of a reaction product obtained by the second esterification reaction; and continuously performing polycondensation reaction of the pre-polymer, wherein an aromatic carboxylic acid is added to a reactor in which the first esterification reaction or the second esterification reaction is performed, to prepare the biodegradable aliphatic/aromatic polyester copolymer. According to the method of continuous preparation of the biodegradable aliphatic/aromatic polyester copolymer as described above, the amount of the aliphatic dihydroxy compound used, which is a starting material, is reduced and accordingly, manufacturing costs are reduced.

    Method for preparing biodegradable polyester resin

    公开(公告)号:US09617378B2

    公开(公告)日:2017-04-11

    申请号:US14915711

    申请日:2014-08-25

    CPC分类号: C08G63/88 C08G63/16 C08G63/78

    摘要: A method of preparing a biodegradable polyester resin is provided. The method of preparing a biodegradable polyester resin includes: (a) synthesizing the biodegradable polyester resin having a reheating crystallization initiation temperature (Tch1), a reheating crystallization peak temperature (Tch), and a reheating crystallization end temperature (Tch2); and (b) crystallizing the biodegradable polyester resin synthesized in step (a) by cooling the resin from a temperature of T1 to a temperature of T2 and then maintaining the resin at a temperature of T2 for a time of tc. Thus, the biodegradable polyester resin with improved solidification rate may be obtained.

    Preparation method of acetylated cellulose ether, and acetylated cellulose ether prepared thereby
    5.
    发明授权
    Preparation method of acetylated cellulose ether, and acetylated cellulose ether prepared thereby 有权
    乙酰化纤维素醚的制备方法和由此制备的乙酰化纤维素醚

    公开(公告)号:US09469694B2

    公开(公告)日:2016-10-18

    申请号:US14363991

    申请日:2012-11-16

    摘要: Disclosed are a method of preparing acetylated cellulose ether, and acetylated cellulose ether prepared thereby. Here, the disclosed method of preparing the acetylated cellulose ether includes dissolving acetylated cellulose ether in an organic solvent to obtain a mixture comprising a solution of the acetylated cellulose ether; removing an insoluble component that is insoluble in the organic solvent from the mixture; and adding the mixture to water to precipitate the acetylated cellulose ether. The acetylated cellulose ether prepared thereby has a turbidity of less than 40 formazin turbidity units (FTU).

    摘要翻译: 公开了制备乙酰化纤维素醚的方法和由此制备的乙酰化纤维素醚。 这里所公开的制备乙酰化纤维素醚的方法包括将乙酰化纤维素醚溶解在有机溶剂中,得到包含乙酰化纤维素醚溶液的混合物; 从混合物中除去不溶于有机溶剂的不溶性成分; 并将混合物加入水中以沉淀乙酰化的纤维素醚。 由此制备的乙酰化纤维素醚具有小于40 formazin浊度单位(FTU)的浊度。

    Method for continuous production of biodegradable aliphatic/aromatic polyester copolymer
    10.
    发明授权
    Method for continuous production of biodegradable aliphatic/aromatic polyester copolymer 有权
    连续生产生物降解脂肪/芳族聚酯共聚物的方法

    公开(公告)号:US09403938B2

    公开(公告)日:2016-08-02

    申请号:US14651489

    申请日:2013-07-18

    摘要: A continuous preparation method of a biodegradable aliphatic/aromatic polyester copolymer includes: performing a first esterification reaction of an aliphatic dihydroxy compound with an aliphatic dicarboxylic acid at a temperature of 185° C. or less; continuously performing a second esterification reaction of a reaction product from the first esterification reaction; continuously performing a first polycondensation reaction of a reaction product from the second esterification reaction to obtain a prepolymer; continuously performing a second polycondensation reaction of the prepolymer to obtain a second polycondensation reaction product having a melting index from about 15 g/10 min to about 25 g/10 min; and continuously performing a third polycondensation reaction of the second polycondensation reaction product to prepare the biodegradable aliphatic/aromatic polyester copolymer, wherein the performing of the first esterification reaction or the continuously performing of the second esterification reaction includes adding an aromatic carboxylic acid.

    摘要翻译: 生物降解性脂肪族/芳香族聚酯共聚物的连续制备方法包括:在185℃以下的温度下进行脂族二羟基化合物与脂肪族二羧酸的第一次酯化反应; 连续进行来自第一酯化反应的反应产物的第二次酯化反应; 连续进行来自第二酯化反应的反应产物的第一次缩聚反应,得到预聚物; 连续进行预聚物的第二缩聚反应,得到熔融指数为约15g / 10min至约25g / 10min的第二缩聚反应产物; 并连续进行第二缩聚反应产物的第三缩聚反应,制备生物降解性脂肪族/芳香族聚酯共聚物,其中进行第一酯化反应或连续进行第二酯化反应包括加入芳族羧酸。