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    Preparation of stable, bright luminescent nanoparticles having compositionally engineered properties
    1.
    发明授权
    Preparation of stable, bright luminescent nanoparticles having compositionally engineered properties 有权
    具有组成工程化特性的稳定的，明亮的发光纳米颗粒的制备

    公开(公告)号：US08287761B2

    公开(公告)日：2012-10-16

    申请号：US12484836

    申请日：2009-06-15

    申请人： Marc Schrier ,  Donald Zehnder ,  Joseph Treadway ,  Joseph Bartel

    发明人： Marc Schrier ,  Donald Zehnder ,  Joseph Treadway ,  Joseph Bartel

    IPC分类号： C09K11/54 ,  C09K11/56 ,  C09K11/88

    CPC分类号： H01L33/28 ,  B82Y30/00 ,  C01P2004/04 ,  C01P2004/64 ,  C09C1/10 ,  C09K11/02 ,  C09K11/565 ,  C09K11/883 ,  Y10S977/824 ,  Y10S977/834 ,  Y10T428/2991

    摘要： A method is provided for preparing luminescent semiconductor nanoparticles composed of a first component X, a second component A, and a third component B, wherein X, A, and B are different, by combining B with X and A in an amount such that the molar ratio B:(A+B) is in the range of approximately 0.001 to 0.20 and the molar ratio X:(A+B) is in the range of approximately 0.5:1.0 to 2:1. The characteristics of the thus-prepared nanoparticles can be substantially similar to those of nanoparticles containing only X and B while maintaining many useful properties characteristic of nanoparticles containing only X and A. The nanoparticles so prepared can additionally exhibit emergent properties such as a peak emission energy less than that characteristic of a particle composed of XA or XB alone; this method is particularly applicable to the preparation of stable, bright nanoparticles that emit in the red to infrared regions of the electromagnetic spectrum. Luminescent semiconductor nanoparticles having exemplary properties are also provided.

    摘要翻译： 提供一种制备由第一组分X，第二组分A和第三组分B组成的发光半导体纳米颗粒的方法，其中X，A和B不同，通​​过将B与X和A组合使得其量使得 摩尔比B：（A + B）在约0.001至0.20的范围内，摩尔比X：（A + B）在约0.5:1.0至2:1的范围内。 如此制备的纳米颗粒的特征可以与仅含有X和B的纳米颗粒的特征基本相似，同时保持了仅含有X和A的纳米颗粒的许多有用特性。如此制备的纳米颗粒可另外显示出出现特性，例如峰值发射能 小于单独由XA或XB组成的颗粒的特征; 该方法特别适用于在电磁光谱的红色至红外区域中发射的稳定的明亮纳米粒子的制备。 还提供了具有示例性质的发光半导体纳米颗粒。

    METHODS FOR THE PREPARATION OF LUMINESCENT NANOPARTICLES USING TWO SOLVENTS
    2.
    发明申请
    METHODS FOR THE PREPARATION OF LUMINESCENT NANOPARTICLES USING TWO SOLVENTS 审中-公开
    使用两种溶剂制备发光纳米颗粒的方法

    公开(公告)号：US20070125983A1

    公开(公告)日：2007-06-07

    申请号：US11670565

    申请日：2007-02-02

    申请人： Joseph Treadway ,  Donald Zehnder ,  Marc Schrier

    发明人： Joseph Treadway ,  Donald Zehnder ,  Marc Schrier

    IPC分类号： C09K11/08 ,  B05D7/00

    CPC分类号： C09K11/883 ,  C09K11/08 ,  C09K11/0805 ,  C09K11/0811 ,  C09K11/54 ,  C09K11/565 ,  Y10T428/2984 ,  Y10T428/2991 ,  Y10T428/2993

    摘要： Methods for synthesizing luminescent nanoparticles and nanoparticles prepared by such methods are provided. The nanoparticles are prepared by a method in which an additive is included in the reaction mixture. The additive may be a Group 2 element, a Group 12 element, a Group 13 element, a Group 14 element, a Group 15 element, or a Group 16 element. In additions, a luminescent nanoparticle is provided that comprises a semiconductive core surrounded by an inorganic shell, an interfacial region and an additive present in the interfacial region or both the interfacial region and the shell.

    摘要翻译： 提供了通过这些方法制备发光纳米颗粒和纳米颗粒的方法。 通过反应混合物中包含添加剂的方法制备纳米颗粒。 添加剂可以是2族元素，12族元素，13族元素，14族元素，15族元素或16族元素。 另外，提供了一种发光纳米颗粒，其包括由无机壳包围的半导体芯，界面区域和存在于界面区域中的添加剂或界面区域和壳体两者。

    Preparation of stable, bright luminescent nanoparticles having compositionally engineered properties
    3.
    发明申请
    Preparation of stable, bright luminescent nanoparticles having compositionally engineered properties 有权
    具有组成工程化特性的稳定的，明亮的发光纳米颗粒的制备

    公开(公告)号：US20050214536A1

    公开(公告)日：2005-09-29

    申请号：US11011827

    申请日：2004-12-13

    申请人： Marc Schrier ,  Donald Zehnder ,  Joseph Treadway ,  Joseph Bartel

    发明人： Marc Schrier ,  Donald Zehnder ,  Joseph Treadway ,  Joseph Bartel

    IPC分类号： B05D7/00 ,  B32B1/00 ,  C09C1/10 ,  C09K11/02 ,  C09K11/56 ,  C09K11/88

    CPC分类号： H01L33/28 ,  B82Y30/00 ,  C01P2004/04 ,  C01P2004/64 ,  C09C1/10 ,  C09K11/02 ,  C09K11/565 ,  C09K11/883 ,  Y10S977/824 ,  Y10S977/834 ,  Y10T428/2991

    摘要： A method is provided for preparing luminescent semiconductor nanoparticles composed of a first component X, a second component A, and a third component B, wherein X, A, and B are different, by combining B with X and A in an amount such that the molar ratio B:(A+B) is in the range of approximately 0.001 to 0.20 and the molar ratio X:(A+B) is in the range of approximately 0.5:1.0 to 2:1. The characteristics of the thus-prepared nanoparticles can be substantially similar to those of nanoparticles containing only X and B while maintaining many useful properties characteristic of nanoparticles containing only X and A. The nanoparticles so prepared can additionally exhibit emergent properties such as a peak emission energy less than that characteristic of a particle composed of XA or XB alone; this method is particularly applicable to the preparation of stable, bright nanoparticles that emit in the red to infrared regions of the electromagnetic spectrum. Luminescent semiconductor nanoparticles having exemplary properties are also provided.

    摘要翻译： 提供一种制备由第一组分X，第二组分A和第三组分B组成的发光半导体纳米颗粒的方法，其中X，A和B不同，通​​过将B与X和A组合使得其量使得 摩尔比B：（A + B）在约0.001至0.20的范围内，摩尔比X：（A + B）在约0.5:1.0至2:1的范围内。 如此制备的纳米颗粒的特征可以与仅含有X和B的纳米颗粒的特征基本相似，同时保持了仅含有X和A的纳米颗粒的许多有用特性。如此制备的纳米颗粒可另外显示出出现特性，例如峰值发射能 小于单独由XA或XB组成的颗粒的特征; 该方法特别适用于在电磁光谱的红色至红外区域中发射的稳定的明亮纳米粒子的制备。 还提供了具有示例性质的发光半导体纳米颗粒。

    Preparation of stable, bright luminescent nanoparticles having compositionally engineered properties
    4.
    发明授权
    Preparation of stable, bright luminescent nanoparticles having compositionally engineered properties 有权
    具有组成工程化特性的稳定的，明亮的发光纳米颗粒的制备

    公开(公告)号：US08603362B2

    公开(公告)日：2013-12-10

    申请号：US13608296

    申请日：2012-09-10

    申请人： Marc Schrier ,  Donald Zehnder ,  Joseph Treadway ,  Joseph Bartel

    发明人： Marc Schrier ,  Donald Zehnder ,  Joseph Treadway ,  Joseph Bartel

    IPC分类号： C09K11/88

    CPC分类号： H01L33/28 ,  B82Y30/00 ,  C01P2004/04 ,  C01P2004/64 ,  C09C1/10 ,  C09K11/02 ,  C09K11/565 ,  C09K11/883 ,  Y10S977/824 ,  Y10S977/834 ,  Y10T428/2991

    摘要： A method is provided for preparing luminescent semiconductor nanoparticles composed of a first component X, a second component A, and a third component B, wherein X, A, and B are different, by combining B with X and A in an amount such that the molar ratio B:(A+B) is in the range of approximately 0.001 to 0.20 and the molar ratio X:(A+B) is in the range of approximately 0.5:1.0 to 2:1. The characteristics of these nanoparticles can be substantially similar to those of nanoparticles containing only X and B while maintaining many useful properties characteristic of nanoparticles containing only X and A; and can additionally exhibit emergent properties such as a peak emission energy less than that characteristic of a particle composed of XA or XB alone. This method is particularly applicable to the preparation of stable, bright nanoparticles that emit in the red to infrared regions of the electromagnetic spectrum.

    摘要翻译： 提供一种制备由第一组分X，第二组分A和第三组分B组成的发光半导体纳米颗粒的方法，其中X，A和B不同，通​​过将B与X和A组合使得其量使得 摩尔比B：（A + B）在约0.001至0.20的范围内，摩尔比X：（A + B）在约0.5:1.0至2:1的范围内。 这些纳米颗粒的特征可以与仅含有X和B的纳米颗粒的特征基本相似，同时保持仅含有X和A的纳米颗粒的许多有用特性; 并且可以另外表现出突出性质，例如小于单独由XA或XB组成的颗粒的特征的峰值发射能量。 该方法特别适用于制备在电磁光谱的红色至红外区域发射的稳定的明亮纳米粒子。

    Sintered CZTS Nanoparticle Solar Cells
    5.
    发明申请
    Sintered CZTS Nanoparticle Solar Cells 审中-公开
    烧结CZTS纳米粒子太阳能电池

    公开(公告)号：US20120067408A1

    公开(公告)日：2012-03-22

    申请号：US12884049

    申请日：2010-09-16

    申请人： Charlie Hotz ,  Margaret Hines ,  Donald Zehnder ,  Damoder Reddy ,  Jing Tang

    发明人： Charlie Hotz ,  Margaret Hines ,  Donald Zehnder ,  Damoder Reddy ,  Jing Tang

    IPC分类号： H01L31/0352 ,  H01B1/02 ,  H01B1/12 ,  H01L31/18

    CPC分类号： H01L31/20 ,  H01L31/0322 ,  H01L31/03923 ,  H01L31/0749 ,  Y02E10/541 ,  Y02P70/521

    摘要： The present invention discloses an absorber composition and photovoltaic device (PV) using the composition comprising nanoparticles and/or sintered nanoparticles comprising compounds having the formula MAxMByMCz(LAaLBb)4 where MA, MB and MC comprise elements chosen from the group consisting of Fe, Co, Ni, Cu, Zn, Cd, Sn and Pb, LA and LB are chalcogens and x is between 1.5 and 2.2, y and z are independently the same or different and are between 0.5 and 1.5 and (a+b)=1.Particularly preferred synthetic routes to uniform thin films in PV devices comprising sintered nanoparticles of Cu2ZnSnSe4 and Cu2ZnSnS4 are disclosed.

    摘要翻译： 本发明公开了使用包含纳米颗粒和/或烧结纳米颗粒的组合物的吸收剂组合物和光伏器件（PV），其包含具有式MAxMByMCz（LAaLBb）4的化合物，其中MA，MB和MC包含选自Fe，Co ，Ni，Cu，Zn，Cd，Sn和Pb，LA和LB是硫属元素，x在1.5和2.2之间，y和z独立相同或不同，在0.5和1.5之间，（a + b）= 1。 公开了在包括Cu 2 ZnSnSn 4和Cu 2 ZnSn Sn的烧结纳米颗粒的PV装置中均匀薄膜的特别优选的合成路线。