摘要:
ozone is dissolved ozone in a liquid cryogen. A container containing a liquified cryogen is provided. A gaseous stream of ozone is allowed to flow into at least one adsorption unit containing an adsorbent material, thereby adsorbing ozone thereupon. The cryogen is allowed to flow from the container to the at least one adsorption unit and therethrough thereby extracting an amount of the ozone adsorbed upon the adsorbent material, wherein the cryogen is in either a liquid, gaseous or supercritical phase as it flows through the adsorption unit. ozone becomes dissolved in the cryogen.
摘要:
A method of treating an object containing a material of metal, oxidized metal, non-metal, and the like and combinations thereof. The method includes (a) exposing an object to a controlled gas atmosphere, and (b) during at least a portion of time during such exposing, subjecting a specific area of the material to an energy beam, preferably a focused energy beam, more preferably a focused and filtered energy beam, having sufficient intensity to provide for the treating of the specific area. Such treating includes heating, welding, cutting, dicing, soldering, singulating, reducing, oxidizing, fusing, melting, and the like and combinations thereof. The energy beam source can be a laser selected from a group which includes YAG lasers, excimer lasers, gas lasers, semiconductor lasers, solid-state lasers, dye lasers, X-ray lasers, free-electron lasers, ion lasers, gas mixture lasers, chemical lasers, and the like and combinations thereof. The method can further include contacting the material with a second material or several second materials. Such contacting can include welding, soldering, fusing, melting, joining, bonding, and the like and combinations thereof.
摘要:
Methods of cooling an object are presented, the methods comprising contacting a heat transfer fluid with a liquid cryogen to form a precooled, substantially pure heat transfer fluid, and contacting the object with the precooled substantially pure heat transfer fluid to form a cooled object and a recycle flow of the heat transfer fluid. The heat transfer fluid consists essentially of a compound selected from the group consisting of substantially pure hydrogen, substantially pure helium, substantially pure argon, substantially pure nitrogen, and substantially pure carbon dioxide. Each of the contacting steps may be either direct contact, indirect contact, or combinations thereof.
摘要:
Apparatus and process for removing carbon monoxide from a gas stream comprising a major portion of an inert gas and a minor portion of carbon monoxide are provided. The process involves contacting a feed gas stream with at least a primary metal oxide in a reaction zone of a reactor vessel at conditions effective to convert substantially all of the carbon monoxide to carbon dioxide, thus producing a purified gas stream consisting essentially of the inert gas and carbon dioxide and substantially free of carbon monoxide. This process has (inter alia) a particular application as a tertiary purification process for producing a more highly purified source of gaseous nitrogen from a source of nitrogen originally produced from a conventional membrane air separation system, wherein the oxygen concentration in the nitrogen stream my vary around a setpoint value, and then further (or secondarily) purified by converting excess oxygen in the nitrogen to carbon monoxide and carbon dioxide using a fuel gas/combustion process, wherein the carbon monoxide concentration varies due to varying oxygen concentration in the feed stream to the combustion process.
摘要:
A process and an apparatus for removing impurities from liquified gases at cryogenic temperatures is provided which can be utilized on site at every stage of transport and storage subsequent to manufacture and prior to use. Liquified gas to be purified which is at cryogenic temperatures is passed preferably through a prefilter to remove solid particulates, followed by passage through an adsorbent bed to remove impurities from the gas and then through a postfilter to remove any entrained particles of adsorbent material from the gas stream. The process can be made continuous between, for example, a storage tank and an adsorption device. The apparatus includes at least one chamber having adsorbent material substantially filling it. A prefilter removes particulates upsteam of the adsorbent chamber and a postfilter downstream of said adsorbent chamber removes entrained adsorbent bed material. Use of two or more adsorbent chambers permits regeneration of one or more chambers while the remaining adsorbent chambers are being used for adsorption.
摘要:
A flow of a gaseous mixture of first and second substances at a desired ratio is provided to a storage container or point of use. Each of the first and second substances has the property of existing only as a gas when it is maintained at one atmosphere and 0° C. A vessel contains the first substance in gas phase only and a second substance in both liquid and gas phases. The second substance is bubbled into the liquid phase of the first substance thereby resulting in the gas mixture in the vessel headspace. The interior vessel temperature, the pressure at which the second substance is bubbled, and a flow rate at which the gas mixture exits the vessel are all maintained at levels sufficient to provide the desired ratio.
摘要:
A packed bed of granulated porous glass is used to purify a gas mixture comprising two gases whose boiling points or sublimation points at one atmosphere are least 10° K apart.
摘要:
Methods and apparatus for purifying gases having organic impurities, including the use of granulated porous glass. The method of the invention includes the following steps. An impure gas comprising a first gas and an organic compound is provided. A packed bed of granulated porous glass is provided. The impure gas is allowed to flow into the packed bed, thereby preferentially adsorbing at least some of the organic compound on the granulated porous glass to yield a purified gas having a concentration of the organic compound that is lower than that of the impure gas. The purified gas is allowed to flow out of the packed bed.
摘要:
Methods and apparatus for purifying gases having organic impurities, including the use of granulated porous glass. A system for purifying an impure gas includes a source of an impure gas, a purification element operatively associated with the source of impure gas for purifying the impure gas, and a conduit operatively associated with the purification element for receiving a flow of purified impure gas from the purification element and directing the purified impure gas to a container or point of use. The impure gas includes a first gas and an organic compound. The purification element includes a vessel containing a packed bed of granulated porous glass.
摘要:
A circuit board is wave soldered as it is carried by a conveyor through a solder wave established in a solder reservoir. Disposed on both sides of the solder wave are gas plenums which discharge shield gas. Each gas plenum includes a top wall, a side wall, and a bottom wall. The side wall is spaced horizontally from the wave, and the bottom wall is submerged within the solder. The side and (optionally) top walls include orifices for directing shield gas (i) at high velocity toward the solder wave to protect the solder wave with an atmosphere of shield gas, and (ii) upwardly toward an underside of the circuit board to strip entrained air therefrom. Instead of being submerged within the solder, the bottom wall could be spaced above the solder and provided with orifices to emit shield gas downwardly between the plenum and solder reservoir to create an inert atmosphere above the solder. Dividers disposed within the plenum form sub-chambers communicating with orifices in respective walls of the plenum so that different gas velocities can be entitled from the orifices. The gas plenums can be rotatably adjustable and further adjustable either vertically or horizontally.