METHOD FOR PREPARING Pt THIN FILMS USING ELECTROSPRAY DEPOSITION AND Pt THIN FILMS FORMED BY THE METHOD
    3.
    发明申请
    METHOD FOR PREPARING Pt THIN FILMS USING ELECTROSPRAY DEPOSITION AND Pt THIN FILMS FORMED BY THE METHOD 审中-公开
    使用电沉积沉积法制备Pt薄膜的方法和由该方法形成的Pt薄膜

    公开(公告)号:US20110177356A1

    公开(公告)日:2011-07-21

    申请号:US12849125

    申请日:2010-08-03

    IPC分类号: B32B15/01 B05D1/04

    摘要: The present invention relates to a method for preparing Pt thin films using electrospray deposition, more specifically a method for preparing platinum thin film using electrospray deposition, including dissolving a platinum (Pt) precursor in ethanol to prepare a precursor solution for spraying (Step 1); applying a DC voltage between a substrate holder and a nozzle of an electrospraying device and then spraying the precursor solution prepared in Step 1 on a substrate which is maintained at about 100° C. to about 180° C. to form a platinum thin film (Step 2); and subjecting the platinum thin film formed in Step 2 to a heat treatment (Step 3). According to the present invention, the thickness of the platinum thin film may be easily regulated by controlling the amount of a precursor solution sprayed, and the platinum thin film may be continuously prepared on a substrate which has a wide area, therefore a highly active platinum thin film may be obtained by using a small amount of platinum which is expensive, and the film may be usefully used as an Pt electrode used a stable cathode electrode for a process which converts the photo energy into electric or chemical energy, or for a wastewater treatment system or a water purification system.

    摘要翻译: 本发明涉及一种使用电喷雾沉积制备Pt薄膜的方法,更具体地说,一种使用电喷雾沉积制备铂薄膜的方法,包括将铂(Pt)前体溶解在乙醇中以制备用于喷雾的前体溶液(步骤1) ; 在基板保持器和电喷雾装置的喷嘴之间施加DC电压,然后将在步骤1中制备的前体溶液喷射到保持在约100℃至约180℃的基板上以形成铂薄膜( 第2步); 并对步骤2中形成的铂薄膜进行热处理(步骤3)。 根据本发明,可以通过控制喷射的前体溶液的量来容易地调节铂薄膜的厚度,并且可以在具有广泛面积的基板上连续制备铂薄膜,因此高活性铂 可以通过使用昂贵的少量铂来获得薄膜,并且该膜可以有用地用作用于将光能转化为电或化学能的方法的稳定阴极电极的Pt电极,或用于废水 处理系统或净水系统。

    Method for the production of dimethyl ether
    5.
    发明申请
    Method for the production of dimethyl ether 失效
    二甲醚生产方法

    公开(公告)号:US20070142482A1

    公开(公告)日:2007-06-21

    申请号:US10571867

    申请日:2004-01-29

    IPC分类号: C07C27/26

    摘要: The present invention is directed to a method for producing DME, which comprises separating a CO2 rich stream from a crude product stream containing DME and CO2 obtained by a DME synthesis from a feed syn gas; introducing the CO2 rich stream to a reverse water gas shift (RWGS) reactor wherein it is reacted with hydrogen in the presence of a catalyst to provide a CO rich stream, and recycling the CO rich stream to the step of the methanol synthesis step. In accordance with the present invention, a large amount of carbon dioxide gas generated during the preparing process of DME is effectively re-used, thus increasing the yield of DME and lowering the amount of carbon dioxide discharged.

    摘要翻译: 本发明涉及一种生产DME的方法,该方法包括从含有DME合成的DME和CO 2的粗产物流中分离富CO 2的物流, 一种饲料合成气; 将富CO 2流引入反向水煤气变换(RWGS)反应器中,其中在催化剂存在下与氢气反应以提供富CO流,并将富CO流再循环至 甲醇合成步骤。 根据本发明,在DME的制备过程中产生的大量二氧化碳气体被有效地再利用,从而提高了DME的产率并降低了排出的二氧化碳的量。

    Photoelectrochemical system for hydrogen production from water
    9.
    发明申请
    Photoelectrochemical system for hydrogen production from water 审中-公开
    用于氢气生产的光电化学系统

    公开(公告)号:US20080131762A1

    公开(公告)日:2008-06-05

    申请号:US11729145

    申请日:2007-03-28

    IPC分类号: H01M6/30

    摘要: The present invention provides a photoelectrochemical (PEC) system for the production of hydrogen from water, which comprises (A) an electrolytic bath comprising an electrode for catalytic oxidation, an electrode for catalytic reduction, an ion separation film disposed between the two electrodes, and an aqueous electrolyte solution into which the two electrodes and the ion separation film are immersed, and (B) a photoelectrode positioned at the outside of the electrolytic bath and electrically connected to the two electrodes. The inventive PEC system is characterized by disposing a photoelectrode at the position which does not contact aqueous electrolyte solution, thus preventing the lowering of the photoelectrode activities, and maximizing the hydrogen production efficiency.

    摘要翻译: 本发明提供一种用于从水中生产氢的光电化学(PEC)系统,其包括(A)包括用于催化氧化的电极的电解浴,用于催化还原的电极,设置在两个电极之间的离子分离膜,以及 浸渍有两个电极和离子分离膜的电解质水溶液,(B)位于电解槽外侧并与两个电极电连接的光电极。 本发明的PEC系统的特征在于在不接触电解质水溶液的位置处设置光电极,防止光电极活性的降低,使氢生产效率最大化。

    Desulfurizartion for Simultaneous Removal of Hydrogen Sulfide and Sulfur Dioxide
    10.
    发明申请
    Desulfurizartion for Simultaneous Removal of Hydrogen Sulfide and Sulfur Dioxide 审中-公开
    同时去除硫化氢和二氧化硫的脱硫剂

    公开(公告)号:US20070248518A1

    公开(公告)日:2007-10-25

    申请号:US11597684

    申请日:2005-06-08

    IPC分类号: B01D53/86

    CPC分类号: B01D53/8615

    摘要: A highly efficient desulfurization method for removing a hydrogen sulfide and a sulfur dioxide simultaneously comprises the step of contacting a gas containing the hydrogen sulfide and the sulfur dioxide with water, or an aqueous solution containing a first heterogeneous catalyst for desulfurization to oxidize the hydrogen sulfide with the sulfur dioxide. 3˜5% sulfur-containing tail gas exhausted from, especially, Claus Process can be treated at a high efficiency of over 99%.

    摘要翻译: 同时进行硫化氢和二氧化硫除去的高效脱硫方法包括使含有硫化氢和二氧化硫的气体与水接触的步骤,或含有用于脱硫的第一非均相催化剂的水溶液以使硫化氢与 二氧化硫。 特别是克劳斯过程排出的3〜5%含硫尾气可以以超过99%的高效率进行处理。