公开(公告)号：US10060033B2

公开(公告)日：2018-08-28

申请号：US14915330

申请日：2014-08-04

申请人： MERCK PATENT GMBH

发明人： Klaus Bonrad ,  Joerg Schneider ,  Rudolf Hoffman ,  Mareiki Kaloumenos

IPC分类号： C07F9/66 ,  C23C18/12 ,  C07F3/00 ,  C07F5/00 ,  C07F7/00 ,  C07F7/22 ,  C07F3/06 ,  H01G4/10 ,  H01G4/33 ,  H01L21/02 ,  H01L21/445 ,  H01L29/45 ,  H01L29/66 ,  H01L29/786

CPC分类号： C23C18/1216 ,  C07F3/003 ,  C07F3/06 ,  C07F5/003 ,  C07F7/003 ,  C07F7/2204 ,  C07F7/2224 ,  C23C18/1291 ,  H01G4/10 ,  H01G4/33 ,  H01L21/02554 ,  H01L21/02565 ,  H01L21/02628 ,  H01L21/02664 ,  H01L21/445 ,  H01L29/45 ,  H01L29/66969 ,  H01L29/7869

摘要： The present invention relates to novel precursors in the form of metal complexes with 2-substituted 1,3-diketones and to a process for the preparation thereof. The invention furthermore relates to the use thereof for the production of thin metal-oxide layers. The latter are constituents in a very wide variety of electronic components and devices having various functions.

公开(公告)号：US09914998B2

公开(公告)日：2018-03-13

申请号：US14853462

申请日：2015-09-14

申请人： NDSU RESEARCH FOUNDATION

发明人： Guruvenket Srinivasan ,  Robert A. Sailer ,  Justin Hoey

IPC分类号： C23C16/24 ,  C23C16/448 ,  C23C16/34 ,  C23C18/02 ,  C23C18/12 ,  C09D183/16 ,  C23C16/02 ,  C23C16/56 ,  H01L21/02 ,  C08G77/60

CPC分类号： C23C16/4486 ,  C08G77/60 ,  C09D183/16 ,  C23C16/0209 ,  C23C16/24 ,  C23C16/345 ,  C23C16/56 ,  C23C18/02 ,  C23C18/1204 ,  C23C18/122 ,  C23C18/1258 ,  C23C18/127 ,  C23C18/1291 ,  H01L21/02118 ,  H01L21/02532 ,  H01L21/0259 ,  H01L21/02592 ,  H01L21/0262

摘要： An apparatus and a non-vapor-pressure dependent method of chemical vapor deposition of Si based materials using direct injection of liquid hydrosilane(s) are presented. Liquid silane precursor solutions may also include metal, non-metal or metalloid dopants, nanomaterials and solvents. An illustrative apparatus has a precursor solution and carrier gas system, atomizer and deposit head with interior chamber and a hot plate supporting the substrate. Atomized liquid silane precursor solutions and carrier gas moves through a confined reaction zone that may be heated and the aerosol and vapor are deposited on a substrate to form a thin film. The substrate may be heated prior to deposition. The deposited film may be processed further with thermal or laser processing.

公开(公告)号：US09895714B2

公开(公告)日：2018-02-20

申请号：US15054988

申请日：2016-02-26

申请人： Cornell University

发明人： David T. Moore ,  Hiroaki Sai ,  Kwan Wee Tan ,  Lara A. Estroff ,  Ulrich B. Wiesner

IPC分类号： C07C211/63 ,  B05D3/00

CPC分类号： B05D3/007 ,  B05D1/005 ,  B05D3/0254 ,  C23C18/1204 ,  C23C18/1245 ,  C23C18/1291 ,  H01L51/4213 ,  Y02P20/542

摘要： A film comprising a crystalline halide perovskite composition having the following formula: AMX3  (1) wherein: A is an organic cation selected from the group consisting of methylammonium, tetramethylammonium, formamidinium, and guanidinium; M is at least one divalent metal; and X is independently selected from halide atoms; wherein the crystalline film of the halide perovskite composition possesses at least one of an average grain size of at least 30 microns, substantial crystal orientation evidenced in an ordering parameter of at least 0.6, and a level of crystallinity of at least 90%. Methods for producing films of these halide perovskite compositions using ionic liquids instead of volatile organic solvents are also described herein.

公开(公告)号：US20170363928A1

公开(公告)日：2017-12-21

申请号：US15535433

申请日：2015-12-11

申请人： UNIVERSITE DE LIEGE ,  INISMa

发明人： Rudi CLOOTS ,  Catherine HENRIST ,  Jessica DENAYER ,  Anthony MAHO ,  Francis CAMBIER ,  Véronique LARDOT ,  Geoffroy BISTER ,  Philippe AUBRY

IPC分类号： G02F1/15 ,  G02F1/1347 ,  C23C18/12 ,  G02F1/155 ,  G02F1/153

CPC分类号： G02F1/1523 ,  C03C17/3417 ,  C23C18/02 ,  C23C18/1216 ,  C23C18/1225 ,  C23C18/1258 ,  C23C18/1291 ,  G02F1/1347 ,  G02F1/15 ,  G02F1/1521 ,  G02F1/1525 ,  G02F1/1533 ,  G02F1/155 ,  G02F2202/38 ,  H01B1/08 ,  Y02P20/129

摘要： A process of making an electrochromic or an electrolytic film by Ultrasonic Spray Pyrolysis (USP) deposition on a substrate comprising: mixing a surfactant to an aqueous precursor solution comprising an electrochromic component or an electrolytic component to provide a spray solution; introducing the spray solution into an ultrasonic spray deposition nozzle at a constant flow rate between 0.1 mL/min and 2 mL/min and applying an ultrasonic frequency between 80 and 120 kHz to generate atomized droplets of the precursor solution; entraining the atomized droplets with a controlled jet of air as gas carrier at a pressure between 0.50 to 2.0 psi, onto a pre-heated substrate at a temperature of 200 to 450° C.; thermally converting the atomized droplets when depositing onto the pre-heated substrate to generate an electrochromic or an electrolytic film.

公开(公告)号：US09670232B2

公开(公告)日：2017-06-06

申请号：US14174759

申请日：2014-02-06

申请人： Transtron Solutions LLC

发明人： Kyle L. Fujdala ,  Christopher Melton

IPC分类号： C09D11/52 ,  C23C18/12 ,  C07F3/06 ,  C07F5/00 ,  C07F5/02 ,  C07F5/06 ,  H01L29/786 ,  C07F5/04 ,  C23C18/06 ,  H01L29/66

CPC分类号： C07F3/06 ,  C07F5/00 ,  C07F5/003 ,  C07F5/022 ,  C07F5/04 ,  C07F5/069 ,  C09D11/52 ,  C23C18/06 ,  C23C18/1216 ,  C23C18/1275 ,  C23C18/1279 ,  C23C18/1283 ,  C23C18/1291 ,  H01L29/66969 ,  H01L29/7869

摘要： Molecular precursor compounds, processes and compositions for making Zn-Group 13 mixed oxide materials including IZO, GZO, AZO and BZO, by providing inks comprising a molecular precursor compound having the formula MAaZn(OROR)3a+2, and printing or depositing the inks on a substrate. The printed or deposited ink films can be treated to convert the molecular precursor compounds to a material.

公开(公告)号：US09634321B2

公开(公告)日：2017-04-25

申请号：US14765994

申请日：2013-03-12

申请人： SACHEM, INC.

发明人： Craig S. Allen ,  Jianjun Hao

IPC分类号： H01M4/04 ,  H01M4/36 ,  H01M4/485 ,  H01M4/505 ,  H01M4/525 ,  H01M4/62 ,  C23C18/12 ,  C01F7/34 ,  H01M4/131 ,  H01M10/0525 ,  C01B33/12 ,  H01M4/02

CPC分类号： H01M4/366 ,  C01B33/12 ,  C01F7/34 ,  C01P2002/72 ,  C01P2004/03 ,  C01P2004/42 ,  C01P2004/61 ,  C01P2004/86 ,  C23C18/1216 ,  C23C18/1245 ,  C23C18/127 ,  C23C18/1291 ,  H01M4/0402 ,  H01M4/0471 ,  H01M4/131 ,  H01M4/485 ,  H01M4/505 ,  H01M4/525 ,  H01M4/62 ,  H01M10/0525 ,  H01M2004/028

摘要： The present invention provides a process for depositing an oxide coating on an inorganic substrate, including providing an aqueous composition containing a tetraalkylammonium polyoxoanion and hydrogen peroxide; contacting the aqueous composition with an inorganic substrate for a time sufficient to deposit a hydroxide derived from the polyoxoanion on surfaces of the inorganic substrate to form an initially coated inorganic substrate; and heating the initially coated inorganic substrate for a time sufficient to convert the hydroxide to an oxide to form on the inorganic substrate an oxide coating derived from the polyoxoanion. The inorganic substrate may be a ceramic material or a semiconductor material, a glass or other dielectric material, and the ceramic material may be a lithium ion battery cathode material.

公开(公告)号：US09236157B2

公开(公告)日：2016-01-12

申请号：US13393822

申请日：2010-09-02

申请人： Vladimir L. Kuznetsov ,  Peter P. Edwards

发明人： Vladimir L. Kuznetsov ,  Peter P. Edwards

IPC分类号： B05D5/12 ,  H01B1/08 ,  C23C18/08 ,  C23C18/12 ,  B05D3/10

CPC分类号： H01B1/08 ,  B05D3/10 ,  B05D5/12 ,  C23C18/08 ,  C23C18/1208 ,  C23C18/1216 ,  C23C18/1233 ,  C23C18/1245 ,  C23C18/1254 ,  C23C18/1258 ,  C23C18/1291 ,  C23C18/1295 ,  Y10T428/24479 ,  Y10T428/24628 ,  Y10T428/24802

摘要： The invention provides a process for producing a transparent conducting film, which film comprises a doped zinc oxide wherein the dopant comprises Si, which process comprises: disposing a composition which is a liquid composition or a gel composition onto a substrate, wherein the composition comprises Zn and Si; and heating said substrate. The invention further provides transparent conducting films obtainable by the process of the invention, including transparent conducting films which comprise a doped zinc oxide wherein the dopant comprises Si, and wherein the film covers a surface area equal to or greater than 0.01 m2. The invention also provides a coated substrate, which substrate comprises a surface, which surface is coated with a transparent conducting film, wherein the film comprises a doped zinc oxide wherein the dopant comprises Si, and wherein the area of said surface which is coated with said film is equal to or greater than 0.01 m2. The invention further provides coatings comprising the films of the invention, processes for producing such films and coatings, and various uses of the films and coatings.

摘要翻译： 本发明提供一种制造透明导电膜的方法，该膜包括掺杂的氧化锌，其中掺杂剂包括Si，该方法包括：将一种作为液体组合物或凝胶组合物的组合物设置在基材上，其中组合物包含Zn 和Si; 并加热所述衬底。 本发明还提供了可通过本发明方法获得的透明导电膜，其包括透明导电膜，其包含掺杂的氧化锌，其中所述掺杂剂包含Si，并且其中所述膜覆盖等于或大于0.01m2的表面积。 本发明还提供一种涂覆的基底，该基底包括表面，该表面涂覆有透明导电膜，其中所述膜包括掺杂的氧化锌，其中所述掺杂剂包含Si，并且其中所述表面的面积涂覆有所述 膜等于或大于0.01m2。 本发明还提供了包含本发明的膜的涂层，用于生产这种膜和涂层的方法以及膜和涂层的各种用途。

公开(公告)号：US09040983B2

公开(公告)日：2015-05-26

申请号：US14058403

申请日：2013-10-21

申请人： Industrial Technology Research Institute

发明人： Wen-Ching Sun ,  Tzer-Shen Lin ,  Sheng-Min Yu

IPC分类号： H01L29/24 ,  H01L31/0216 ,  H01L29/06 ,  H01L21/02 ,  C23C18/12 ,  H01L31/0224 ,  H01L31/068 ,  H01L31/18 ,  H01L29/66 ,  H01L33/44 ,  H01L29/20

CPC分类号： H01L31/02167 ,  C23C18/1216 ,  C23C18/1245 ,  C23C18/1258 ,  C23C18/1287 ,  C23C18/1291 ,  H01L21/02178 ,  H01L21/02282 ,  H01L29/0607 ,  H01L29/2003 ,  H01L29/66462 ,  H01L31/022425 ,  H01L31/068 ,  H01L31/1868 ,  H01L33/44 ,  Y02E10/547 ,  Y02P70/521

摘要： A passivation layer structure of a semiconductor device is provided, which includes a passivation layer formed of halogen-doped aluminum oxide and disposed on a semiconductor layer on a substrate, in which the semiconductor layer includes indium gallium zinc oxide (IGZO) or nitride-based III-V compounds. A method for forming the passivation layer structure of a semiconductor device is also disclosed.

摘要翻译： 提供半导体器件的钝化层结构，其包括由卤素掺杂的氧化铝形成的钝化层，并且设置在衬底上的半导体层上，其中半导体层包括铟镓锌氧化物（IGZO）或氮化物基 III-V族化合物。 还公开了一种用于形成半导体器件的钝化层结构的方法。

公开(公告)号：US20150024924A1

公开(公告)日：2015-01-22

申请号：US14381979

申请日：2013-02-25

申请人： INVENTRAM FIKRI MULKIYET HAKLARI YONETIM TICARET VE YATIRIM ANONIM SIRKETI

发明人： Ayse Senatalar ,  Melkon Tatlier

IPC分类号： B01J20/32 ,  B01J19/08

CPC分类号： B01J20/3238 ,  B01J19/087 ,  B01J2219/085 ,  C23C18/12 ,  C23C18/1212 ,  C23C18/1287 ,  C23C18/1291 ,  C23C18/14

摘要： The present invention relates to a zeolite coating preparation assembly (1) and operation method wherein zeolite adsorbents are coated by crystallization process on various surfaces heated by induction. The objective of the present invention is to provide a zeolite coating preparation assembly (1) and operation method; by which time saving is achieved owing to heating by induction, material saving is achieved since large heating resistances and complicated reactors are not used; and which is thus more economical; and wherein thicker and more stable coatings with high diffusion coefficients are prepared by using a more practical reaction system in a shorter period of time in comparison to the known methods, and wherein mass production is enabled.

摘要翻译： 本发明涉及一种沸石涂料制备组合物（1）及其操作方法，其中沸石吸附剂通过结晶过程涂覆在通过感应加热的各种表面上。 本发明的目的是提供一种沸石涂料制备组合物（1）和操作方法; 由于通过感应加热实现了节省，由于不使用大的耐热性和复杂的反应器，因此节省了材料; 因此更经济; 并且其中与已知方法相比，通过使用更实际的反应体系在更短的时间内制备具有高扩散系数的更厚和更稳定的涂层，并且其中批量生产是可以实现的。

公开(公告)号：US20140377452A1

公开(公告)日：2014-12-25

申请号：US14482086

申请日：2014-09-10

申请人： LG Chem Ltd.

发明人： Yo-han Kwon ,  Joo Sung Lee ,  Je-Young Kim ,  Jong-Hun Kim

IPC分类号： H01M4/04 ,  H01M4/139

CPC分类号： H01M4/0404 ,  C23C18/1291 ,  H01M4/0411 ,  H01M4/139 ,  H01M4/621 ,  H01M4/622 ,  H01M4/623 ,  H01M4/667 ,  H01M4/668 ,  H01M4/765 ,  H01M10/0413 ,  H01M10/0436 ,  H01M10/052 ,  H01M10/0565 ,  H01M10/058 ,  H01M2004/025 ,  Y02E60/122 ,  Y02P70/54 ,  Y02T10/7011 ,  Y10T29/49115

摘要： The present invention relates to a method for manufacturing a cable-type secondary battery comprising an electrode that extends longitudinally in a parallel arrangement and that includes a current collector having a horizontal cross section of a predetermined shape and an active material layer formed on the current collector, and the electrode is formed by putting an electrode slurry including an active material, a polymer binder, and a solvent into an extruder, by extrusion-coating the electrode slurry on the current collector while continuously providing the current collector to the extruder, and by drying the current collector coated with the electrode slurry to form an active material layer.

摘要翻译： 电缆型二次电池的制造方法技术领域本发明涉及一种电缆型二次电池的制造方法，其特征在于，包括以并列方式纵向延伸的电极，其包括具有规定形状的水平截面的集电体和形成在所述集电体上的活性物质层 并且通过将包含活性物质，聚合物粘合剂和溶剂的电极浆料放入挤出机中，通过在集电体上挤出涂布电极浆料，同时将集流体连续地提供给挤出机，并且通过 干燥涂覆有电极浆料的集电体以形成活性材料层。