Yb activated hafnium oxide phosphor and methods of making
    3.
    发明授权
    Yb activated hafnium oxide phosphor and methods of making 失效
    Yb活化铪氧化物荧光粉及其制备方法

    公开(公告)号:US4006097A

    公开(公告)日:1977-02-01

    申请号:US574275

    申请日:1975-05-05

    IPC分类号: C09K11/77 C09K11/46

    CPC分类号: C09K11/7701

    摘要: A phosphor composition having the general formula HfO.sub.2 :Yb with ytterbium being present in an amount of from 0.005 to 0.10 moles per mole of hafnium is disclosed. The phosphor can be prepared from the mixed oxides or from the oxalates, carbonates, or hydroxides by precipitating the latter from an aqueous solution. Firing takes place under a reducing atmosphere, preferably nitrogen, to reduce the ytterbium to the plus 2 ion. The phosphor is a bright green emitter under ultraviolet, x-radiation and cathode ray excitation.

    摘要翻译: 公开了具有通式HfO 2:Yb的镱的荧光体组合物,其镱的存在量为每摩尔铪0.005至0.10摩尔。 荧光体可以通过从水溶液中沉淀而由混合氧化物或草酸盐,碳酸盐或氢氧化物制备。 在还原气氛,优选氮气下进行烧制,以将镱还原成正2离子。 在紫外线,x辐射和阴极射线激发下,荧光体是亮绿色发射体。

    Isotopically enriched luminescent materials and methods of making same
    4.
    发明授权
    Isotopically enriched luminescent materials and methods of making same 失效
    同位素富集的发光材料及其制备方法

    公开(公告)号:US06838020B2

    公开(公告)日:2005-01-04

    申请号:US10298147

    申请日:2002-11-15

    申请人: Paul V. Kelsey

    发明人: Paul V. Kelsey

    摘要: The invention is directed to luminescent materials containing isotopically-enriched atomic elements and methods of making these luminescent materials. Individual embodiments of the invention include isotopically-enriched ZnO:Zn, ZnS:Cu:Cl, Zn2SiO4:Mn, Y2O2S:Eu, Gd2O2S:Tb and CaWO4 phosphors as well as methods of synthesizing these luminescent materials using isotopically-enriched starting materials.

    摘要翻译: 本发明涉及含有富含同位素的原子元素的发光材料和制造这些发光材料的方法。 本发明的各个实施方案包括同位素富集的ZnO:Zn,ZnS:Cu:Cl,Zn2SiO4:Mn,Y2O2S:Eu,Gd2O2S:Tb和CaWO4荧光体,以及使用同位素富集的原料合成这些发光材料的方法。

    Process for preparing self-supporting ceramic composite bodies and
bodies produced thereby
    5.
    发明授权
    Process for preparing self-supporting ceramic composite bodies and bodies produced thereby 失效
    制备自支撑陶瓷复合体的方法

    公开(公告)号:US5166105A

    公开(公告)日:1992-11-24

    申请号:US624836

    申请日:1990-12-10

    申请人: Paul V. Kelsey

    发明人: Paul V. Kelsey

    IPC分类号: C04B35/65 C22C1/10 C22C29/14

    摘要: This invention relates generally to a novel method of preparing self-supporting bodies, and to novel products made thereby. In its more specific aspects, this invention relates to a method of producing self-supporting bodies comprising one or more boron-containing compounds, e.g., a boride or a boride and a carbide, by reactive infiltration of a molten parent metal actinide into (1) a bed or mass containing boron carbide and, optionally, (2) at least one of a boron donor material (i.e., a boron-containing material) and a carbon donor material (i.e., a carbon-containing material), (3) a bed or mass comprising a mixture of a boron donor material and a carbon donor material and, optionally, (4) one or more inert fillers in any of the above masses, to form the body.

    摘要翻译: 本发明一般涉及一种制备自支撑体的新方法,以及由此制成的新颖产品。 在其更具体的方面,本发明涉及通过将熔融母体金属锕系元素反应性渗透到(1)中的方法来制备包含一种或多种含硼化合物,例如硼化物或硼化物和碳化物的自支撑体的方法 )含有碳化硼和任选地(2)硼供体材料(即含硼材料)和碳供体材料(即,含碳材料)中的至少一种的床或质量,(3) 包含硼供体材料和碳供体材料的混合物的床或质量,和任选地(4)一种或多种上述任一种质量的惰性填料以形成体。

    Plasma production of polycrystalline silicon
    6.
    发明授权
    Plasma production of polycrystalline silicon 失效
    等离子体生产多晶硅

    公开(公告)号:US06926876B2

    公开(公告)日:2005-08-09

    申请号:US10346601

    申请日:2003-01-17

    申请人: Paul V. Kelsey

    发明人: Paul V. Kelsey

    摘要: The invention is directed to a method of producing polycrystaline silicon metal from a silicon halide plasma source. The silicon halide is split into silicon and halide ions in an inductively coupled plasma and silicon ions are then condensed to form molten silicon metal that can be vacuum cast into polysilicon ingots. The halide ions are separated and recycled into silicon halide gas over a silicon dioxide bed. In this way, high grade polysilicon is produced without a metallurgical grade silicon precursor and the process these processes consumes the byproducts in a continuous manner madding it less expensive than traditional methods of producing polysilicon and more environmentally friendly.

    摘要翻译: 本发明涉及从卤化硅等离子体源生产多晶硅金属的方法。 硅卤化物被分裂成硅,并且在感应耦合的等离子体中的卤离子离子然后被冷凝,形成熔融的硅金属,其可被真空铸造成多晶硅锭。 卤化物离子被分离并在二氧化硅床上再循环到卤化硅气体中。 这样,高品质多晶硅就没有冶金级的硅前体而被生产,而这些工艺这些工艺以连续的方式消耗副产物,比传统生产多晶硅的方法更便宜,更环保。

    Process for preparing self-supporting ceramic composite bodies and
bodies produced thereby
    7.
    发明授权
    Process for preparing self-supporting ceramic composite bodies and bodies produced thereby 失效
    制备自支撑陶瓷复合体的方法

    公开(公告)号:US5288670A

    公开(公告)日:1994-02-22

    申请号:US979986

    申请日:1992-11-23

    申请人: Paul V. Kelsey

    发明人: Paul V. Kelsey

    摘要: This invention relates generally to a novel method of preparing self-supporting bodies, and to novel products made thereby. In its more specific aspects, this invention relates to a method of producing self-supporting bodies comprising one or more boron-containing compounds, e.g., a boride or a boride and a carbide, by reactive infiltration of a molten parent metal actinide into (1) a bed or mass containing boron carbide and, optionally, (2) at least one of a boron donor material (i.e., a boron-containing material) and a carbon donor material (i.e., a carbon-containing material), (3) a bed or mass comprising a mixture of a boron donor material and a carbon donor material and, optionally, (4) one or more inert fillers in any of the above masses, to form the body.

    摘要翻译: 本发明一般涉及一种制备自支撑体的新方法,以及由此制成的新颖产品。 在其更具体的方面,本发明涉及通过将熔融母体金属锕系元素反应性渗透到(1)中的方法来制备包含一种或多种含硼化合物,例如硼化物或硼化物和碳化物的自支撑体的方法 )含有碳化硼和任选地(2)硼供体材料(即含硼材料)和碳供体材料(即,含碳材料)中的至少一种的床或质量,(3) 包含硼供体材料和碳供体材料的混合物的床或质量,和任选地(4)一种或多种上述任一种质量的惰性填料以形成体。

    Method of preparing rare earth pyrohafnate phosphors
    8.
    发明授权
    Method of preparing rare earth pyrohafnate phosphors 失效
    制备稀土焦碳酸盐荧光粉的方法

    公开(公告)号:US4014812A

    公开(公告)日:1977-03-29

    申请号:US578763

    申请日:1975-05-19

    IPC分类号: C09K11/77 C09K11/78 C09K11/46

    CPC分类号: C09K11/7766

    摘要: Phosphors having the general formula (A.sub.1.sub.-x RE.sub.x).sub.2 Hf.sub.2 O.sub.7 are disclosed wherein A is selected from the group consisting of yttrium, gadolium, lanthanum, scandium and lutetium; RE is selected from the group consisting of praseodymium, samarium, europium, terbium, dysprosium, holmium, erbium and thulium; and x is from about 0.001 to 0.10. The phosphors are prepared by dissolving an oxide of A and an oxide of RE in a mineral acid and dissolving HfOCl.sub.2 in water and combining the two solutions. A precipitating agent such as oxalic acid is added and the precipitate is washed, dried and fired to produce the phosphors.

    摘要翻译: 公开了具有通式(A1-xREx)2Hf2O7的荧光体,其中A选自钇,钆,镧,钪和镥; RE选自镨,钐,铕,铽,镝,钬,铒和ium; x为约0.001〜0.10。 通过将A的氧化物和RE的氧化物溶解在无机酸中并将HfOCl 2溶解在水中并组合这两种溶液来制备荧光体。 加入沉淀剂如草酸,并将沉淀物洗涤,干燥并烧制以产生荧光体。