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1.
公开(公告)号:US20240270893A1
公开(公告)日:2024-08-15
申请号:US18435149
申请日:2024-02-07
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Thomas P. Klun , Zeba Parkar , John M. Riedesel , Richard J. Pokorny , Chad M. Amb , Benjamin R. Coonce , Robert S. Clough , Tianyu Wu , Saswata Chakraborty , Yongshang Lu , Benjamin C. Mac Murray , Ahmed S. Abuelyaman , Karl J.L. Geisler , Jodi L. Connell , Ta-Hua Yu
IPC: C08G18/44 , A61C7/00 , A61C7/08 , A61C13/00 , B29C71/00 , B29C71/02 , B29C71/04 , B33Y10/00 , B33Y30/00 , B33Y40/20 , B33Y70/00 , B33Y80/00 , C08G18/22 , C08G18/24 , C08G18/32 , C08G64/30 , C08K5/00 , C08K5/3437
CPC classification number: C08G18/44 , A61C7/002 , A61C7/08 , A61C13/0019 , B29C71/0009 , B29C71/02 , B29C71/04 , B33Y10/00 , B33Y40/20 , B33Y70/00 , B33Y80/00 , C08G18/222 , C08G18/227 , C08G18/242 , C08G18/3206 , C08G64/305 , C08K5/0041 , C08K5/3437 , B29C2071/0027 , B33Y30/00 , C08G2650/16
Abstract: The present disclosure provides an orthodontic article including the reaction product of the polymerizable composition. Further, the present disclosure provides polymerizable compositions and methods of making an orthodontic article. The method includes obtaining a polymerizable composition and selectively curing the polymerizable composition to form an orthodontic article. Further, methods are provided, including receiving, by a manufacturing device having one or more processors, a digital object comprising data specifying an orthodontic article; and generating, with the manufacturing device by an additive manufacturing process, the orthodontic article based on the digital object. A system is also provided, including a display that displays a 3D model of an orthodontic article; and one or more processors that, in response to the 3D model selected by a user, cause a 3D printer to create a physical object of an orthodontic article.
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2.
公开(公告)号:US11220462B2
公开(公告)日:2022-01-11
申请号:US16963874
申请日:2019-01-21
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Aaron R. Beaber , Marc G. Simpson , Kari Ann McGee , Amy S. Barnes , Zeba Parkar
IPC: C04B35/117 , C04B35/10 , C04B35/14 , C04B35/185 , C04B35/628 , C04B35/80 , D04C1/12 , D06M15/356
Abstract: Methods of making ceramic matrix prepregs are described. The methods include exposing a coated tow of ceramic fibers to a ceramic matrix slurry comprising a solvent and ceramic precursor. The coating is at least partially removed and the slurry infuses into the ceramic fibers to form prepreg. Steps to form ceramic matrix composites are also described, including forming the prepreg into a green body, and sintering the ceramic precursor.
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公开(公告)号:US20230322966A1
公开(公告)日:2023-10-12
申请号:US18326386
申请日:2023-05-31
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Thomas P. Klun , Zeba Parkar , John M. Riedesel , Richard J. Pokorny , Chad M. Amb , Benjamin R. Coonce , Robert S. Clough , Tianyu Wu , Saswata Chakraborty , Yongshang Lu , Benjamin C. Mac Murray
IPC: C08F2/50 , B33Y10/00 , B33Y30/00 , B33Y70/00 , B29C64/129 , C08F2/44 , C08F220/18 , C08F290/06 , C08G18/44 , C08G18/67 , C08K5/00 , C08K5/3437
CPC classification number: C08F2/50 , B33Y10/00 , B33Y30/00 , B33Y70/00 , B29C64/129 , C08F2/44 , C08F220/18 , C08F290/06 , C08G18/44 , C08G18/672 , C08K5/0041 , C08K5/3437
Abstract: The present disclosure provides a photopolymerizable composition. The photopolymerizable composition includes a) 40-60 parts by weight of a monofunctional (meth)acrylate monomer, per 100 parts of the total photopolymerizable composition; b) a photoinitiator; and c) a polymerization reaction product of components. A cured homopolymer of the monofunctional (meth)acrylate monomer has a glass transition temperature of 125 degrees Celsius or greater. The polymerization reaction product of components includes i) a diisocyanate; ii) a hydroxy functional methacrylate; iii) a polycarbonate diol; and iv) a catalyst. The polymerization reaction product includes a polyurethane methacrylate polymer. Often, the polycarbonate diol has a number average molecular weight of greater than 1,000 grams per mole (g/mol) or a weighted average of all polycarbonate diols present in the components has a Mn of greater than 1,000 g/mol; alternatively, the polyurethane methacrylate polymer has a weight average molecular weight of 8,000 g/mol or greater. An article is also provided including the photopolymerizable composition reaction product. Further, the present disclosure provides articles and methods of making articles. Methods are additionally provided, including receiving, by a manufacturing device having one or more processors, a digital object comprising data specifying an article; and generating, with the manufacturing device by an additive manufacturing process, the article based on the digital object. A system is also provided, including a display that displays a 3D model of an article; and one or more processors that, in response to the 3D model selected by a user, cause a 3D printer to create a physical object of an article.
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公开(公告)号:US11104758B2
公开(公告)日:2021-08-31
申请号:US17042384
申请日:2019-05-21
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Thomas P. Klun , Zeba Parkar , John M. Riedesel , Richard J. Pokorny , Chad M. Amb , Benjamin R. Coonce , Robert S. Clough , Tianyu Wu , Saswata Chakraborty , Yongshang Lu , Benjamin C. MacMurray , Ian Dailey , David B. Olson
IPC: C08G18/44 , A61C7/08 , A61C13/00 , A61C7/00 , B33Y10/00 , B33Y70/00 , B33Y80/00 , B33Y40/20 , B29C71/00 , B29C71/02 , B29C71/04 , C08G18/22 , C08G18/24 , C08G18/32 , C08G18/67 , C08G64/30 , C08K5/3437 , B33Y30/00
Abstract: The present disclosure provides an orthodontic article including the reaction product of the photopolymerizable composition. The photopolymerizable composition includes i) a monofunctional (meth)acrylate monomer whose cured homopolymer has a glass transition temperature of 90 degrees Celsius or greater; ii) a photoinitiator; and iii) a polymerization reaction product of components. The components include 1) an isocyanate; 2) a (meth)acrylate mono-ol; 3) a polycarbonate diol; and 4) a catalyst. Further, the present disclosure provides a method of making an orthodontic article. The method includes obtaining a photopolymerizable composition and selectively curing the photopolymerizable composition to form an orthodontic article. Further, methods are provided, including receiving, by a manufacturing device having one or more processors, a digital object comprising data specifying an orthodontic article; and generating, with the manufacturing device by an additive manufacturing process, the orthodontic article based on the digital object. A system is also provided, including a display that displays a 3D model of an orthodontic article; and one or more processors that, in response to the 3D model selected by a user, cause a 3D printer to create a physical object of an orthodontic article.
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公开(公告)号:US20210163664A1
公开(公告)日:2021-06-03
申请号:US17042384
申请日:2019-05-21
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Thomas P. Klun , Zeba Parkar , John M. Riedesel , Richard J. Pokorny , Chad M. Amb , Benjamin R. Coonce , Robert S. Clough , Tianyu Wu , Saswata Chakraborty , Yongshang Lu , Benjamin C. Mac Murray , Ian Dailey , David B. Olson
IPC: C08G18/44 , A61C7/08 , A61C13/00 , A61C7/00 , B33Y10/00 , B33Y70/00 , B33Y80/00 , C08G18/32 , C08G64/30 , C08G18/22 , C08G18/24 , B29C71/00 , B29C71/02 , B29C71/04 , C08G18/67 , B33Y40/20 , C08K5/3437
Abstract: The present disclosure provides an orthodontic article including the reaction product of the photopolymerizable composition. The photopolymerizable composition includes i) a monofunctional (meth)acrylate monomer whose cured homopolymer has a glass transition temperature of 90 degrees Celsius or greater; ii) a photoinitiator; and iii) a polymerization reaction product of components. The components include 1) an isocyanate; 2) a (meth)acrylate mono-ol; 3) a polycarbonate diol; and 4) a catalyst. Further, the present disclosure provides a method of making an orthodontic article. The method includes obtaining a photopolymerizable composition and selectively curing the photopolymerizable composition to form an orthodontic article. Further, methods are provided, including receiving, by a manufacturing device having one or more processors, a digital object comprising data specifying an orthodontic article; and generating, with the manufacturing device by an additive manufacturing process, the orthodontic article based on the digital object. A system is also provided, including a display that displays a 3D model of an orthodontic article; and one or more processors that, in response to the 3D model selected by a user, cause a 3D printer to create a physical object of an orthodontic article.
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公开(公告)号:US20210393385A1
公开(公告)日:2021-12-23
申请号:US17292847
申请日:2019-11-19
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Zeba Parkar , Victor Ho , Joel D. Oxman , Jason A. Bender
Abstract: A dental appliance including a polymeric shell with an arrangement of cavities configured to receive one or more teeth and a coating on at least portion of the polymeric shell. The coating can include a polyester with an ion exchange functional group covalently bonded thereto, and the ion exchange functional group can release in an oral environment at least one therapeutically beneficial ion at a surface of a tooth.
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公开(公告)号:US20210361389A1
公开(公告)日:2021-11-25
申请号:US17052536
申请日:2019-06-25
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Benjamin C. Mac Murray , Saswata Chakraborty , John M. Riedesel , Thomas P. Klun , Chad M. Amb , Karl J.L. Geisler , Zeba Parkar , Adrian S. Eckert , Mark T. Gibson , Tianyu Wu
Abstract: The present disclosure provides methods of making a hydrated orthodontic article is provided. One method includes a) providing a photopolymerizable composition; b) selectively curing the photopolymerizable composition using actinic radiation to form an article in the shape of an orthodontic article having a plurality of layers of at least one photopolymerized polymer; and c) exposing the article to water by submersion in water, thereby hydrating the article. A sheet of the at least one photopolymerized polymer has a bending modulus when hydrated of 100 MPa or greater and 2200 MPa or less. Another method includes exposing the orthodontic article to water vapor and hermetically sealing the hydrated orthodontic article in a container. Hydrated orthodontic articles are also provided, including an orthodontic article that is prepared according to one of the methods. The present disclosure further provides kits, including an orthodontic article and instructions for exposing the orthodontic article to water to hydrate the orthodontic article, as well as including a hydrated orthodontic article hermetically sealed in a container.
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公开(公告)号:US20210301042A1
公开(公告)日:2021-09-30
申请号:US17344096
申请日:2021-06-10
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Thomas P. Klun , Zeba Parkar , John M. Riedesel , Richard J. Pokorny , Chad M. Amb , Benjamin R. Coonce , Robert S. Clough , Tianyu Wu , Saswata Chakraborty , Yongshang Lu , Benjamin C. Mac Murray
IPC: C08F2/50 , B33Y10/00 , B33Y30/00 , B33Y70/00 , B29C64/129 , C08F2/44 , C08F220/18 , C08F290/06 , C08G18/44 , C08G18/67 , C08K5/00 , C08K5/3437
Abstract: The present disclosure provides a photopolymerizable composition. The photopolymerizable composition includes a) 40-60 parts by weight of a monofunctional (meth)acrylate monomer, per 100 parts of the total photopolymerizable composition; b) a photoinitiator; and c) a polymerization reaction product of components. A cured homopolymer of the monofunctional (meth)acrylate monomer has a glass transition temperature of 125 degrees Celsius or greater. The polymerization reaction product of components includes i) a diisocyanate; ii) a hydroxy functional methacrylate; iii) a polycarbonate diol; and iv) a catalyst. The polymerization reaction product includes a polyurethane methacrylate polymer. Often, the polycarbonate diol has a number average molecular weight of greater than 1,000 grams per mole (g/mol) or a weighted average of all polycarbonate diols present in the components has a Mn of greater than 1,000 g/mol; alternatively, the polyurethane methacrylate polymer has a weight average molecular weight of 8,000 g/mol or greater. An article is also provided including the photopolymerizable composition reaction product. Further, the present disclosure provides articles and methods of making articles. Methods are additionally provided, including receiving, by a manufacturing device having one or more processors, a digital object comprising data specifying an article; and generating, with the manufacturing device by an additive manufacturing process, the article based on the digital object. A system is also provided, including a display that displays a 3D model of an article; and one or more processors that, in response to the 3D model selected by a user, cause a 3D printer to create a physical object of an article.
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公开(公告)号:US20210292243A1
公开(公告)日:2021-09-23
申请号:US17260344
申请日:2019-08-22
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Gareth A. Hughes , Melissa A. Lackey , Brant U. Kolb , Jerome G. Magnant , Zeba Parkar , Kevin M. Casey , Nicholas S. Wren
IPC: C04B35/584 , C04B35/634 , C04B35/624 , C04B35/626 , C04B35/64 , C04B38/06 , B29C64/124 , B33Y10/00 , B33Y70/10 , B28B1/00
Abstract: The present disclosure provides a method of making a non-oxide ceramic part. The method includes obtaining a photopolymerizable slurry; selectively curing the photopolymerizable slurry to obtain a gelled article; drying the gelled article to form an aerogel article or a xerogel article; heat treating the aerogel article or the xerogel article to form a porous ceramic article; and sintering the porous ceramic article to obtain a sintered ceramic article. The photopolymerizable slurry includes non-oxide ceramic particles; at least one radiation curable monomer; a solvent; a photoinitiator; an inhibitor; and at least one sintering aid. Further, aerogels, xerogels, porous ceramic articles, and non-oxide ceramic articles are provided. In addition, methods are provided, including receiving, by a manufacturing device having one or more processors, a digital object comprising data specifying an article; and generating, with the manufacturing device by an additive manufacturing process, the article based on the digital object. A system is also provided, including a display that displays a 3D model of an article; and one or more processors that, in response to the 3D model selected by a user, cause a 3D printer to create a physical object of an article.
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公开(公告)号:US20210095056A1
公开(公告)日:2021-04-01
申请号:US17042243
申请日:2019-05-21
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor: Thomas P. Klun , Zeba Parkar , John M. Riedesel , Richard J. Pokorny , Chad M. Amb , Benjamin R. Coonce , Robert S. Clough , Tianyu Wu , Saswata Chakraborty , Yongshang Lu , Benjamin C. Mac Murray , Ian Dailey , David B. Olson
IPC: C08F2/50 , C08F220/18 , C08F2/44 , C08F290/06 , C08G18/44 , C08G18/67 , C08K5/00 , C08K5/3437 , B29C64/129 , B33Y10/00 , B33Y30/00 , B33Y70/00
Abstract: The present disclosure provides a photopolymerizable composition. The photopolymerizable composition includes a) 40-60 parts by weight of a monofunctional (meth)acrylate monomer, per 100 parts of the total photopolymerizable composition; b) a photoinitiator; and c) a polymerization reaction product of components. A cured homopolymer of the monofunctional (meth)acrylate monomer has a glass transition temperature of 125 degrees Celsius or greater. The polymerization reaction product of components includes i) a diisocyanate; ii) a hydroxy functional methacrylate; iii) a polycarbonate diol; and iv) a catalyst. The polymerization reaction product includes a polyurethane methacrylate polymer. Often, the polycarbonate diol has a number average molecular weight of greater than 1,000 grams per mole (g/mol) or a weighted average of all polycarbonate diols present in the components has a Mn of greater than 1,000 g/mol; alternatively, the polyurethane methacrylate polymer has a weight average molecular weight of 8,000 g/mol or greater. An article is also provided including the photopolymerizable composition reaction product. Further, the present disclosure provides articles and methods of making articles. Methods are additionally provided, including receiving, by a manufacturing device having one or more processors, a digital object comprising data specifying an article; and generating, with the manufacturing device by an additive manufacturing process, the article based on the digital object. A system is also provided, including a display that displays a 3D model of an article; and one or more processors that, in response to the 3D model selected by a user, cause a 3D printer to create a physical object of an article.
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