Polyester concentrates having high stability in solution and having a greying-inhibiting effect
    2.
    发明授权
    Polyester concentrates having high stability in solution and having a greying-inhibiting effect 有权
    聚酯浓缩物在溶液中具有高稳定性并具有防灰白效果

    公开(公告)号:US08871703B2

    公开(公告)日:2014-10-28

    申请号:US13512260

    申请日:2010-11-24

    摘要: The invention relates to an aqueous polyester concentrate having a proportion by weight of polyesters of 12 to 60%, wherein the polyesters are obtainable by means of polymerization of the components selected from a) one or more sulfo group-free aromatic dicarboxylic acids and/or salts thereof and/or anhydrides thereof and/or esters thereof, b) optionally one or more sulfo group-containing dicarboxylic acids, salts thereof and/or anhydrides thereof and/or esters thereof, c) 1,2-propylene glycol, d) ethylene glycol, e) one or more compounds of the formula (1) R1O(CHR2CHR3O)nH (1), where R1 is a linear or branched, saturated or unsaturated alkyl group having from 1 to 22 C atoms, R2 and R3, independently of one another, are hydrogen or an alkyl group having from 1 to 4 carbon atoms, and n is an integer of from 1 to 50, f) optionally one or more compounds of the formula (2) H—(OCH2CH2)m—SO3X (2), where m is an integer of from 1 to 10 and X is hydrogen or an alkali metal ion, and g) optionally one or more cross-linking polyfunctional compounds, provided that at least one of the components b) or f) is present, and provided further that the molar ratio of the components c) 1,2-propylene glycol to d) ethylene glycol is greater than or equal to 1.60.

    摘要翻译: 本发明涉及一种聚酯重量百分比为12至60%的聚酯水性聚酯浓缩物,其中聚酯可通过选自以下成分的聚合获得:a)一种或多种不含无磺基的芳族二羧酸和/或 其盐和/或其酸酐和/或其酯,b)任选的一种或多种含磺基的二羧酸,其盐和/或其酸酐和/或其酯,c)1,2-丙二醇,d) 乙二醇,e)一种或多种式(1)化合物R 1 O(CHR 2 CHR 3 O)n H(1),其中R 1是具有1至22个C原子的直链或支链饱和或不饱和的烷基,R2和R3独立地 是氢或具有1至4个碳原子的烷基,n是1至50的整数,f)任选的一种或多种式(2)的化合物,H(OCH 2 CH 2)m -SO 3 X (2)中,m为1〜10的整数,X为氢或碱金属离子,g)选择 条件是存在至少一种组分b)或f)的一种或多种交联多官能化合物,并进一步提供组分c)1,2-丙二醇与d)乙二醇的摩尔比为 大于或等于1.60。

    System and Method for Providing Insurance Data
    3.
    发明申请
    System and Method for Providing Insurance Data 审中-公开
    提供保险数据的制度和方法

    公开(公告)号:US20070276704A1

    公开(公告)日:2007-11-29

    申请号:US11567115

    申请日:2006-12-05

    IPC分类号: G06Q40/00

    CPC分类号: G06Q40/08

    摘要: A method for providing insurance data includes storing one or more service events, where each service event is associated with one or more medical encounters and with enrollee responsibility data, receiving medical encounter data from a user, identifying the service event associated with the medical encounter data received from the user, and providing to the user the enrollee responsibility data associated with the identified service event. A system for providing insurance data includes a database configured for storing one or more service events, where each service event is associated with one or more medical encounters and with enrollee responsibility data, a processor configured for retrieving data associated with the one or more service events; and a plurality of user terminals for receiving the retrieved data.

    摘要翻译: 用于提供保险数据的方法包括存储一个或多个服务事件,其中每个服务事件与一个或多个医疗遭遇相关联,以及与登记者责任数据相关联,从用户接收医疗遭遇数据,识别与医疗遭遇数据相关联的服务事件 从用户接收,并向用户提供与所标识的服务事件相关联的登记者责任数据。 用于提供保险数据的系统包括配置用于存储一个或多个服务事件的数据库,其中每个服务事件与一个或多个医疗遭遇相关联,以及与登记者责任数据相关联;处理器,被配置为检索与一个或多个服务事件相关联的数据 ; 以及用于接收检索的数据的多个用户终端。

    Method for isolating concentrated paraffin sulfonic acids
    4.
    发明授权
    Method for isolating concentrated paraffin sulfonic acids 有权
    浓缩石蜡磺酸分离方法

    公开(公告)号:US08426642B2

    公开(公告)日:2013-04-23

    申请号:US12598229

    申请日:2008-04-29

    IPC分类号: C07C309/04

    摘要: The invention relates to a method for isolating concentrated paraffin sulfonic acids from reaction mixtures that are produced during the sulfoxidation of n-paraffins, from which a major part of the sulfuric acid and the paraffin was removed by phase separation and which contain, in addition to the free paraffin sulfonic acids, n-paraffins, water and optionally minor amounts of sulfuric acids. The method according to the invention is characterized by removing paraffin and optionally residual water by vacuum distillation. The paraffin sulfonic acids obtained by distillation have a content of more than 85% by weight of the active substance. The material is pale, odorless and low in sulfuric acid and paraffin.

    摘要翻译: 本发明涉及一种从正链烷烃的亚磺氧化反应中产生的反应混合物中分离浓缩的链烷磺酸的方法,其中大部分硫酸和石蜡通过相分离除去,并且除了含有 游离的链烷烃磺酸,正链烷烃,水和任选的少量硫酸。 根据本发明的方法的特征在于通过真空蒸馏除去石蜡和任选的残余水。 通过蒸馏获得的链烷磺酸含量大于活性物质的85重量%。 该材料为浅灰色,无臭,硫酸和石蜡含量低。

    Method For Producing 3,7-Diaza-Bicyclo[3.3.1] Nonane Compounds
    6.
    发明申请
    Method For Producing 3,7-Diaza-Bicyclo[3.3.1] Nonane Compounds 有权
    制备3,7-二氮杂双环[3.3.1]壬烷化合物的方法

    公开(公告)号:US20110152528A1

    公开(公告)日:2011-06-23

    申请号:US13059470

    申请日:2009-08-17

    IPC分类号: C07D471/08

    CPC分类号: C07D471/08

    摘要: The invention relates to a one-pot reaction for the production of 3,7-diaza-bicyclo[3.3.1]nonane compounds, wherein in a first step a dicarboxylic acid ester is reacted with a pyridine aldehyde and a primary amine. The piperidone created in this manner is reacted with formaldehyde and a further primary amine in a second step. It is essential to the invention that both reaction steps are carried out in a one-pot variation in a C1-C4 alcohol as the solvent, and that the reaction water created is removed by means of distillation.

    摘要翻译: 本发明涉及一种用于制备3,7-二氮杂双环[3.3.1]壬烷化合物的一锅反应,其中在第一步中,二羧酸酯与吡啶醛和伯胺反应。 在第二步骤中以这种方式产生的哌啶酮与甲醛和另外的伯胺反应。 本发明重要的是,两个反应步骤都是以C1-C4醇作为溶剂的一锅变化进行的,所产生的反应水通过蒸馏除去。

    Process for the preparation of ureidoperoxycarboxylic acids
    9.
    发明授权
    Process for the preparation of ureidoperoxycarboxylic acids 失效
    制备尿嘧啶羧酸的方法

    公开(公告)号:US5235099A

    公开(公告)日:1993-08-10

    申请号:US793815

    申请日:1991-11-18

    摘要: A process for the preparation of ureidoperoxycarboxylic acids of the formula ##STR1## in which x is the number 1 or 2,A,if x is 1,is hydrogen, C.sub.1 -C.sub.20 -alkyl, aryl, preferably phenyl, or haloaryl, preferably chlorophenyl, orif x is 2,is C.sub.1 -C.sub.20 -alkylene or arylene, preferably phenylene,B is a group of the formula ##STR2## in which n is a number from 1 to 20,m is the number 0, 1 or 2,R.sup.1 is C.sub.1 -C.sub.20 -alkyl andR.sup.2 is in each case hydrogen or C.sub.1 -C.sub.20 -alkyl, which comprises dissolving carbamoyllactams of the formula ##STR3## in which x, A and B have the abovementioned meanings, in a one- to six-fold, preferably a one- to three-fold, amount by weight of a strong catalyst acid, by then adding water in a one- to ten-fold molar excess, relative to the carbamoyllactam, to the solution of the carbamoyllactam in the catalyst acid and by heating the reaction mixture to form the ureidocarboxylic acid, by then adding to the reaction mixture an aqueous hydrogen peroxide solution in a one- to ten-fold, preferably a two- to four fold, molar excess per oxidizable carboxyl group of the ureidocarboxylic acid formed in the preceding reaction step, and by then precipitating the resulting ureidoperoxycarboxylic acid from the reaction mixture.These compounds are suitable as bleaches, oxidants and disinfectants.

    摘要翻译: 制备式A [NHCONHBCOOOH] x的脲基过氧羧酸的方法,其中x为数1或2,如果x为1,则为A,为C 1 -C 20烷基,芳基,优选苯基或卤代芳基 ,优选氯苯基,或如果x为2,则为C 1 -C 20亚烷基或亚芳基,优选亚苯基,B为下式的基团:其中n为1至20的数,m为数 0,1或2,R 1是C 1 -C 20烷基,R 2在各自的情况下是氢或C 1 -C 20 - 烷基,其包括将式(ⅩⅧ)的氨基甲酰基内酰胺溶解在其中x,A和B具有上述含义, 以强的催化剂酸的重量比为1至6倍,优选1至3倍,然后将相对于氨基甲酰基内酰胺的1至10倍摩尔过量的水加入到 催化剂中的氨基甲酰基内酰胺,并加热反应混合物形成脲基羧酸,然后向反应混合物中加入过氧化氢水溶液 在上述反应步骤中形成的脲基羧酸的每个可氧化羧基的摩尔过量为十倍,优选为二至四倍,然后从反应混合物中沉淀所得的脲基过氧羧酸。 这些化合物适合作为漂白剂,氧化剂和消毒剂。

    Method for producing 3,7-diaza-bicyclo[3.3.1]nonane compounds
    10.
    发明授权
    Method for producing 3,7-diaza-bicyclo[3.3.1]nonane compounds 有权
    制备3,7-二氮杂双环[3.3.1]壬烷化合物的方法

    公开(公告)号:US08293910B2

    公开(公告)日:2012-10-23

    申请号:US13059470

    申请日:2009-08-17

    IPC分类号: C07D471/08

    CPC分类号: C07D471/08

    摘要: The invention relates to a one-pot reaction for the production of 3,7-diaza-bicyclo[3.3.1]nonane compounds, wherein in a first step a dicarboxylic acid ester is reacted with a pyridine aldehyde and a primary amine. The piperidone created in this manner is reacted with formaldehyde and a further primary amine in a second step. It is essential to the invention that both reaction steps are carried out in a one-pot variation in a C1-C4 alcohol as the solvent, and that the reaction water created is removed by means of distillation.

    摘要翻译: 本发明涉及一种用于制备3,7-二氮杂双环[3.3.1]壬烷化合物的一锅反应,其中在第一步中,二羧酸酯与吡啶醛和伯胺反应。 在第二步骤中以这种方式产生的哌啶酮与甲醛和另外的伯胺反应。 本发明重要的是,两个反应步骤都是以C1-C4醇作为溶剂的一锅变化进行的,所产生的反应水通过蒸馏除去。