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    2- and 3-Cyclotetradecen-1-ones as bitterness depressants
    2.
    发明授权
    2- and 3-Cyclotetradecen-1-ones as bitterness depressants 失效
    2-和3-环十四碳烯-1-酮作为苦味抑制剂

    公开(公告)号：US4183965A

    公开(公告)日：1980-01-15

    申请号：US973093

    申请日：1978-12-26

    申请人： Braja D. Mookherjee ,  Robert W. Trenkle ,  Manfred H. Vock ,  Domenick Luccarelli, Jr. ,  Frederick L. Schmitt ,  Gilbert Stork ,  Timothy MacDonald ,  Arthur L. Liberman

    发明人： Braja D. Mookherjee ,  Robert W. Trenkle ,  Manfred H. Vock ,  Domenick Luccarelli, Jr. ,  Frederick L. Schmitt ,  Gilbert Stork ,  Timothy MacDonald ,  Arthur L. Liberman

    IPC分类号： A23F5/46 ,  A23G3/00 ,  A23G3/36 ,  A23L27/20 ,  A23L27/30 ,  C07C45/56 ,  C07C49/587 ,  C11B9/00 ,  A23F1/04 ,  A23L1/22 ,  A23L1/226 ,  C12C3/00

    CPC分类号： A23G3/36 ,  A23F5/465 ,  A23L27/203 ,  A23L27/30 ,  C07C45/562 ,  C07C49/587 ,  C11B9/0038

    摘要： Processes and compositions are described for the use in foodstuff flavor and aroma and perfume and perfumed article aroma augmenting, modifying, altering and enhancing compositions and as foodstuffs, chewing gum, toothpaste, medicinal product, perfume and perfumed article aroma imparting materials of specific isomer and isomer mixtures of 2- and 3-cyclotetradecen-1-ones having the structures: ##STR1## or mixtures of same or mixtures of such 2- and 3-cyclotetradecen-1-ones with cyclotetradecanone having the structure: ##STR2## or cyclododecanone having the structure: ##STR3## Addition of said 2- and 3-cyclotetradecen-1-ones or mixtures is indicated to produce:(a) In food flavorings, a sweet, brown sugar and musky aroma and sweet and musky flavor characteristics (useful for flavor augmentation or enhancement in pear, blackberry, apricot and peach flavors and as a bitterness depressant for such foodstuffs, flavor adjuvants and beverages as black coffee; and(b) In perfumes and perfumed articles, a sweet, musk aroma and exaltone-like, scorched linen, waxy and rooty nuances.

    摘要翻译： 描述了用于食品香料和香料和香料和香料制品香气增强，改性，改变和增强组合物以及作为食品，口香糖，牙膏，药用产品，香料和香料赋予特定异构体的芳香赋予材料的方法和组合物， 具有以下结构的2-和3-环十四碳烯-1-酮的异构体混合物：或其混合物或这些2-和3-环十四碳烯-1-酮与环十四烷酮的混合物，其具有以下结构：具有以下结构： 结构：所述2-和3-环十四碳烯-1-酮或其混合物的添加表明产生：（a）在食品香料中，甜味，红糖和麝香的香气和甜味和麝香风味特征（可用于 梨，黑莓，杏子和桃子香味的香味增强或增强，以及作为黑咖啡的这类食品，风味佐剂和饮料的苦味抑制剂;和（b）在香水和香料中 一种甜美的麝香，麝香香气和高雅的香味，烧焦的亚麻，蜡质和根深蒂固的细微差别。

    Composition of matter comprising more than 50% trans, trans-.DELTA.-damascone for augmenting or enhancing the aroma and taste of a smoking tobacco
    7.
    发明授权
    Composition of matter comprising more than 50% trans, trans-.DELTA.-damascone for augmenting or enhancing the aroma and taste of a smoking tobacco 失效
    包含超过50％反式，反式 - DELTA-马斯克酮用于增强或增强吸烟烟草的香气和味道的物质组成

    公开(公告)号：US4211242A

    公开(公告)日：1980-07-08

    申请号：US851727

    申请日：1977-11-15

    申请人： Braja D. Mookherjee ,  Robert W. Trenkle ,  Richard A. Wilson ,  Frederick L. Schmitt ,  Manfred H. Vock ,  Edward J. Granda ,  Joacquin Vinals ,  Jacob Kiwala ,  William L. Schreiber

    发明人： Braja D. Mookherjee ,  Robert W. Trenkle ,  Richard A. Wilson ,  Frederick L. Schmitt ,  Manfred H. Vock ,  Edward J. Granda ,  Joacquin Vinals ,  Jacob Kiwala ,  William L. Schreiber

    IPC分类号： A23L27/20 ,  A23L27/29 ,  A24B3/12 ,  A24B15/34 ,  A61K8/00 ,  A61K8/35 ,  A61Q11/00 ,  A61Q13/00 ,  C07C45/67 ,  C07C45/69 ,  C07C45/72 ,  C07C49/543 ,  C07C49/573 ,  C07C67/00 ,  C07C401/00 ,  C07C403/00 ,  C07C403/16 ,  C11B9/00

    CPC分类号： C11D3/0084 ,  A24B15/34 ,  C07C403/16 ,  C07C45/67 ,  C07C45/69 ,  C07C45/72 ,  C07C49/543 ,  C07C49/573 ,  C11B9/0034 ,  C07B2200/09 ,  C07C2101/16

    摘要： Described is a process for augmenting or enhancing the aroma and taste of a smoking tobacco comprising adding to said smoking tobacco an organoleptic property modifying quantity of a composition of matter comprising more than 50% trans,trans-.DELTA.-damascone and in addition a process for augmenting or enhancing the aroma and taste of a smoking tobacco comprising adding to said smoking tobacco in an organoleptic property modifying quantity a product produced according to the process of (i) reacting 1-alpha-acetyl-2-alpha,6,6-trimethyl-3-cyclohexene with strong base in aqueous ethanol at reflux thereby producing 1-alpha-acetyl-2-beta,6,6-trimethyl-3-cyclohexene; (ii) reacting the 1-alpha-acetyl-2-beta,6,6-trimethyl-3-cyclohexene with n-methyl aniline Grignard thereby forming a first organometallic compound; (iii) reacting said first organometallic compound with acetaldehyde thereby forming a second organometallic compound; (iv) reacting said second organometallic compound with acid in order to hydrolyze said second organometallic compound thereby forming a hydroxy ketone having the structure: ##STR1## in admixture with other compounds; (v) dehydrating said hydroxy ketone in admixture with other compounds thereby forming a mixture having a major proportion of trans, trans-.DELTA.-damascone having the structure: ##STR2## in admixture with cis, trans-.DELTA.-damascone having the structure: ##STR3## and in admixture with other compounds; and in addition smoking tobacco products containing same.

    摘要翻译： 描述了一种用于增强或增强吸烟烟草的香气和味道的方法，包括向所述吸烟烟草中添加包含超过50％反式，反式 - △ - 马斯酮酮的物质组合物的感官特性改性量，另外还包括 增加或增强烟草的香气和味道，其包括向所述吸烟烟草中加入感官特性调节量，根据以下方法生产的产物：（i）使1-α-乙酰基-2-α，6,6-三甲基 -3-环己烯与强碱在乙醇水溶液中反应，从而产生1-α-乙酰基-2-β，6,6-三甲基-3-环己烯; （ii）使1-α-乙酰基-2-β6,6-三甲基-3-环己烯与正甲基苯胺格氏试剂反应，从而形成第一有机金属化合物; （iii）使所述第一有机金属化合物与乙醛反应，从而形成第二有机金属化合物; （iv）使所述第二有机金属化合物与酸反应以水解所述第二有机金属化合物，从而形成具有以下结构的羟基酮：与其它化合物混合; （v）使所述羟基酮与其它化合物混合，从而形成具有以下结构的具有以下结构的具有以下结构的反式，反式 - 三氯乙酸 - 马来酰肼的主要比例的混合物：＆lt; IMAGE＆gt;与具有以下结构的顺式，反式 - IMAGE>并与其他化合物混合; 以及含有相同烟草制品的烟草制品。