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1.发明授权
公开(公告)号：US5401393A
公开(公告)日：1995-03-28
申请号：US120505
申请日：1993-09-14
Applicant: Darrell D. Whitehurst , Tsoung Y. Yan
Inventor： Darrell D. Whitehurst , Tsoung Y. Yan
CPC classification number: B01J20/264 , B01J20/0266 , B01J20/265 , B01J20/267 , B01J20/28004 , B01J20/28016 , B01J20/28057 , B01J20/3078 , B01J20/321 , B01J20/3234 , C10G25/02 , B01J2220/46
Abstract: A method is disclosed for synthesizing a reactive sulfur-containing adsorbent material for removing metals, preferably mercury, from hydrocarbon fluids. The method includes impregnating a porous polystyrene resin with elemental sulfur, and heating the impregnated resin/sulfur mixture to chemically fix the sulfur to the resin. The elemental sulfur may be in solid, liquid, or vapor phase under conditions of contact with the resin. Also disclosed is the reactive adsorbent synthesized by this method. Also, a process is disclosed for removing mercury from hydrocarbon fluids by using a reactive adsorbent of the invention.
Abstract translation: 公开了一种合成用于从烃流体中除去金属（优选汞）的反应性含硫吸附剂材料的方法。 该方法包括用元素硫浸渍多孔聚苯乙烯树脂，并加热浸渍的树脂/硫混合物以将硫化学固定在树脂上。 在与树脂接触的条件下，元素硫可以是固体，液体或气相。 还公开了通过该方法合成的反应性吸附剂。 此外，公开了通过使用本发明的反应性吸附剂从烃流体中除去汞的方法。
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公开(公告)号：US4247384A
公开(公告)日：1981-01-27
申请号：US20601
申请日：1979-03-15
Applicant: Nai Y. Chen , Dennis E. Walsh , Tsoung Y. Yan , Darrell D. Whitehurst
Inventor： Nai Y. Chen , Dennis E. Walsh , Tsoung Y. Yan , Darrell D. Whitehurst
CPC classification number: C10G1/083
Abstract: Improved method for solubilizing solid carbonaceous materials, e.g., wood and/or coal in an aromatic petroleum or coal-derived solvent in the presence of alkali and hydrogen transfer agent at elevated temperatures. The liquid products can be used as fuels or further processed into desirable products.
Abstract translation: 在碱和氢转移剂存在下，在升高的温度下，在芳香族石油或来自煤的溶剂中溶解固体碳质材料（例如木材和/或煤）的改进方法。 液体产品可用作燃料或进一步加工成所需产品。
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3.发明授权Continuous coking of residual oil and production of gaseous fuel and smokeless solid fuels from coal 失效剩余油的持续焦化以及来自煤的气态燃料和无烟固体燃料的生产
公开(公告)号：US4533463A
公开(公告)日：1985-08-06
申请号：US512505
申请日：1983-07-11
Applicant: Tsoung Y. Yan , Darrell D. Whitehurst
Inventor： Tsoung Y. Yan , Darrell D. Whitehurst
IPC: B01J8/20 , C01B39/04 , C08F2/06 , C08F10/00 , C10B55/10 , C10G1/04 , C10G1/06 , C10G9/00 , C10G9/28 , C10G9/38 , C10G9/32
CPC classification number: C10G9/38 , B01J8/20 , C01B39/04 , C08F10/00 , C10B55/10 , C10G1/042 , C10G1/045 , C10G1/065 , C10G9/005 , C10G9/28 , B01J2219/1946 , Y02P20/582
Abstract: Coal and residual oil are simultaneously processed in a reactor with a combustion zone at the bottom and a fluidized bed on top of it. The residual oil is injected into heat exchange relationship with the top of the fluidized bed where it is cracked with heat generated by the combustion.
Abstract translation: 煤和残油在反应器中同时被处理，其中底部具有燃烧区，并在其顶部具有流化床。 将残留的油与流化床的顶部注入与燃烧产生的热量破裂的热交换关系。
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公开(公告)号：US4470254A
公开(公告)日：1984-09-11
申请号：US378160
申请日：1982-05-14
Applicant: Nai Y. Chen , Darrell D. Whitehurst , Tsoung Y. Yan
Inventor： Nai Y. Chen , Darrell D. Whitehurst , Tsoung Y. Yan
Abstract: The present invention provides two-stage and three-stage fluidized bed process embodiments for burning carbonaceous solids for the generation of heat to produce motive fluids for application in combined cycle power plant systems.The finely-divided refractory solids employed in the fluidized beds may contain sorbent material to neutralize noxious gas constituents and yield a clean flue gas for venting.
Abstract translation: 本发明提供两阶段和三阶段流化床方法实施例，用于燃烧碳质固体以产生热量以产生用于联合循环发电厂系统的运动流体。 在流化床中使用的细碎耐火材料固体可能含有吸附剂材料以中和有害气体成分，并产生用于排气的干净烟道气。
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公开(公告)号：US4385042A
公开(公告)日：1983-05-24
申请号：US296763
申请日：1981-08-27
Applicant: Darrell D. Whitehurst , Tsoung Y. Yan
Inventor： Darrell D. Whitehurst , Tsoung Y. Yan
IPC: B01J8/20 , C01B39/02 , C01B39/04 , C08F10/00 , C10B55/00 , C10G1/04 , C10G1/06 , C10G9/00 , C01B33/28
CPC classification number: C10G9/005 , B01J8/20 , C01B39/02 , C01B39/04 , C08F10/00 , C10B55/00 , C10G1/042 , C10G1/045 , C10G1/065 , B01J2219/1946 , Y02P20/582 , Y10S423/09
Abstract: A solid product resulting from the nucleated growth of the product on solid material of either the same or different composition and having a density higher than the reaction medium is formed from one or more liquid phase reactants by a method which comprises tangentially introducing the liquid phase reaction medium into the lower, smaller end of an inverted, frusto-conical reactor-separator, thereby imparting an upward swirling motion to the reaction medium in the reactor-separator, the horizontal velocity at the bottom of the reactor-separator being sufficiently large to cause fluidization of larger, solid product particles and concentration of them in the central lower portion of the reactor-separator and the vertical velocity at the top of the reactor-separator being sufficiently small to avoid carry-over of the smaller solid particles but sufficiently large to concentrate them in the upper portion of the reactor-separator; at least periodically recovering the larger, solid product particles in spherical form from the bottom of the reactor-separator; and recovering fluid products from the top of the reactor-separator. The method described is useful in a variety of reactions wherein a solid product forms by a nucleated growth mechanism. Examples of such reactions include thermal upgrading of petroleum derived feedstocks and coal liquids, synthesis of zeolites and Ziegler-Natta polymerization of olefins.
Abstract translation: 由相同或不同组成的固体材料产生的具有比反应介质高的密度产生的固体产物由一种或多种液相反应物形成，该方法包括切向引入液相反应 介质进入倒立的截头圆锥形反应器分离器的较小的较小端，从而向反应器分离器中的反应介质施加向上旋转运动，反应器分离器底部的水平速度足够大以致 更大的固体产物颗粒的流化和它们在反应器分离器的中心下部的浓度以及反应器分离器顶部的垂直速度足够小以避免较小固体颗粒的滞留，但足够大以至 将它们集中在反应器分离器的上部; 从反应器分离器的底部至少周期性地回收球形的更大的固体产物颗粒; 并从反应器分离器的顶部回收流体产物。 所描述的方法可用于通过有核生长机制形成固体产物的各种反应。 这种反应的实例包括石油衍生的原料和煤液体的热升级，沸石的合成和烯烃的齐格勒 - 纳塔聚合。
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Patent Agency Ranking6.发明授权
公开(公告)号：US4383094A
公开(公告)日：1983-05-10
申请号：US296765
申请日：1981-08-27
Applicant: Darrell D. Whitehurst , Tsoung Y. Yan
Inventor： Darrell D. Whitehurst , Tsoung Y. Yan
CPC classification number: C10G9/005 , B01J8/20 , C01B39/04 , C08F10/00 , C10G1/042 , C10G1/045 , C10G1/065 , B01J2219/1946 , Y02P20/582
Abstract: A solid product resulting from the nucleated growth of the product on solid material of either the same or different composition and having a density higher than the reaction medium is formed from one or more liquid phase reactants by a method which comprises tangentially introducing the liquid phase reaction medium into the lower, smaller end of an inverted, frusto-conical reactor-separator, thereby imparting an upward swirling motion to the reaction medium in the reactor-separator, the horizontal velocity at the bottom of the reactor-separator being sufficiently large to cause fluidization of larger, solid product particles and concentration of them in the central lower portion of the reactor-separator and the vertical velocity at the top of the reactor-separator being sufficiently small to avoid carry-over of the smaller solid particles but sufficiently large to concentrate them in the upper portion of the reactor-separator; at least periodically recovering the larger, solid product particles in spherical form from the bottom of the reactor-separator; and recovering fluid products from the top of the reactor-separator. The method described is useful in a variety of reactions wherein a solid product forms by a nucleated growth mechanism. Examples of such reactions include thermal upgrading of petroleum derived feedstocks and coal liquids, synthesis of zeolites and Ziegler-Natta polymerization of olefins.
Abstract translation: 由相同或不同组成的固体材料产生的具有比反应介质高的密度产生的固体产物由一种或多种液相反应物形成，该方法包括切向引入液相反应 介质进入倒立的截头圆锥形反应器分离器的较小的较小端，从而向反应器分离器中的反应介质施加向上旋转运动，反应器分离器底部的水平速度足够大以致 更大的固体产物颗粒的流化和它们在反应器分离器的中心下部的浓度以及反应器分离器顶部的垂直速度足够小以避免较小固体颗粒的滞留，但足够大以至 将它们集中在反应器分离器的上部; 从反应器分离器的底部至少周期性地回收球形的更大的固体产物颗粒; 以及从反应器分离器的顶部回收流体产物。 所描述的方法可用于通过有核生长机制形成固体产物的各种反应。 这种反应的实例包括石油衍生的原料和煤液体的热升级，沸石的合成和烯烃的齐格勒 - 纳塔聚合。
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公开(公告)号：US4303494A
公开(公告)日：1981-12-01
申请号：US64142
申请日：1979-08-06
Applicant: Darrell D. Whitehurst , Tsoung Y. Yan
Inventor： Darrell D. Whitehurst , Tsoung Y. Yan
IPC: B01J8/20 , C01B39/04 , C08F2/06 , C08F10/00 , C10B55/10 , C10G1/04 , C10G1/06 , C10G9/00 , C10G9/28 , C10G9/38 , C10G1/00
CPC classification number: C10G9/38 , B01J8/20 , C01B39/04 , C08F10/00 , C10B55/10 , C10G1/042 , C10G1/045 , C10G1/065 , C10G9/005 , C10G9/28 , B01J2219/1946 , Y02P20/582
Abstract: A solid product resulting from the nucleated growth of the product on solid material of either the same or different composition and having a density higher than the reaction medium is formed from one or more liquid phase reactants by a method which comprises tangentially introducing the liquid phase reaction medium into the lower, smaller end of an inverted, frusto-conical reactor-separator, thereby imparting an upward swirling motion to the reaction medium in the reactor-separator, the horizontal velocity at the bottom of the reactor-separator being sufficiently large to cause fluidization of larger, solid product particles and concentration of them in the central lower portion of the reactor-separator and the vertical velocity at the top of the reactor-separator being sufficiently small to avoid carry-over of the smaller solid particles but sufficiently large to concentrate them in the upper portion of the reactor-separator; at least periodically recovering the larger, solid product particles in spherical form from the bottom of the reactor-separator; and recovering fluid products from the top of the reactor-separator. The method described is useful in a variety of reactions wherein a solid product forms by a nucleated growth mechanism. Examples of such reactions include thermal upgrading of petroleum derived feedstocks and coal liquids, synthesis of zeolites and Ziegler-Natta polymerization of olefins.
Abstract translation: 由相同或不同组成的固体材料产生的具有比反应介质高的密度产生的固体产物由一种或多种液相反应物形成，该方法包括切向引入液相反应 介质进入倒立的截头圆锥形反应器分离器的较小的较小端，从而向反应器分离器中的反应介质施加向上旋转运动，反应器分离器底部的水平速度足够大以致 更大的固体产物颗粒的流化和它们在反应器分离器的中心下部的浓度以及反应器分离器顶部的垂直速度足够小以避免较小固体颗粒的滞留，但足够大以至 将它们集中在反应器分离器的上部; 从反应器分离器的底部至少周期性地回收球形的更大的固体产物颗粒; 并从反应器分离器的顶部回收流体产物。 所描述的方法可用于通过有核生长机制形成固体产物的各种反应。 这种反应的实例包括石油衍生的原料和煤液体的热升级，沸石的合成和烯烃的齐格勒 - 纳塔聚合。
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公开(公告)号：US20120228231A1
公开(公告)日：2012-09-13
申请号：US13470340
申请日：2012-05-13
Applicant: Ping-Wen Yen , Yuh-Sheve Ho , Hung-Tzu Chiu , Chung-Jong Hwu , June-Cheng Chang , Tzong-Bin Lin , Tsoung Y. Yan , Cheng-Tsung Hong , Hung-Chung Shen , Jeng-Cheng Lee , Fu-Ming Lee
Inventor： Ping-Wen Yen , Yuh-Sheve Ho , Hung-Tzu Chiu , Chung-Jong Hwu , June-Cheng Chang , Tzong-Bin Lin , Tsoung Y. Yan , Cheng-Tsung Hong , Hung-Chung Shen , Jeng-Cheng Lee , Fu-Ming Lee
IPC: B03C1/30
CPC classification number: C10G21/28 , B01D29/23 , B01D35/06 , B03C1/0332 , B03C1/286 , B03C1/30 , B03C2201/18 , B03C2201/20 , B03C2201/28 , C10G25/003 , C10G31/09 , C10G32/02
Abstract: A novel design of filters for removing iron rust particulates and other polymeric sludge from refinery and chemical process streams that are paramagnetic in nature is provided. The performance of these filters is greatly enhanced by the presence of the magnetic field induced by magnets. Basically, the filter comprises a high-pressure vessel with means to support the plurality of magnets in the form of bars or plates that are encased in stainless steel tubes or columns. Filters with various configurations are disclosed for accommodating the removal of contaminants from the process streams of different industries, with high efficiency for contaminants removal, simple construction, low operational and maintenance costs, and low hazardous operation.
Abstract translation: 提供了一种用于从炼油厂和化学工艺流中去除铁锈微粒和其他聚合污泥的过滤器的新颖设计，其性质是顺磁性的。 这些滤波器的性能由磁铁引起的磁场的存在而大大增强。 基本上，过滤器包括高压容器，该高压容器具有用于将多个以棒或板形式的磁体支撑在不锈钢管或列中的装置。 公开了具有各种结构的过滤器，用于容纳从不同行业的工艺流中去除污染物，高效率地去除污染物，简单的结构，低操作和维护成本以及低危险操作。
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公开(公告)号：US20100065504A1
公开(公告)日：2010-03-18
申请号：US12589314
申请日：2009-10-21
Applicant: Ping-Wen Yen , Yuh-Sheve Ho , Hung-Tzu Chiu , Chung-Jong Hwu , June-Cheng Chang , Tzong-Bin Lin , Tsoung Y. Yan , Cheng-Tsung Hong , Hung-Chung Shen , Jeng-Cheng Lee , Fu-Ming Lee
Inventor： Ping-Wen Yen , Yuh-Sheve Ho , Hung-Tzu Chiu , Chung-Jong Hwu , June-Cheng Chang , Tzong-Bin Lin , Tsoung Y. Yan , Cheng-Tsung Hong , Hung-Chung Shen , Jeng-Cheng Lee , Fu-Ming Lee
IPC: B03C1/02
CPC classification number: C10G21/28 , B01D29/23 , B01D35/06 , B03C1/0332 , B03C1/286 , B03C1/30 , B03C2201/18 , B03C2201/20 , B03C2201/28 , C10G25/003 , C10G31/09 , C10G32/02
Abstract: A novel design of filters for removing iron rust particulates and other polymeric sludge from refinery and chemical process streams that are paramagnetic in nature is provided. The performance of these filters is greatly enhanced by the presence of the magnetic field induced by magnets. Basically, the filter comprises a high-pressure vessel with means to support the plurality of magnets in the form of bars or plates that are encased in stainless steel tubes or columns. Filters with various configurations are disclosed for accommodating the removal of contaminants from the process streams of different industries, with high efficiency for contaminants removal, simple construction, low operational and maintenance costs, and low hazardous operation.
Abstract translation: 提供了一种用于从炼油厂和化学工艺流中去除铁锈微粒和其他聚合污泥的过滤器的新颖设计，其性质是顺磁性的。 这些滤波器的性能由磁铁引起的磁场的存在而大大增强。 基本上，过滤器包括高压容器，该高压容器具有用于将多个以棒或板形式的磁体支撑在不锈钢管或列中的装置。 公开了具有各种结构的过滤器，用于容纳从不同行业的工艺流中去除污染物，高效率地去除污染物，简单的结构，低操作和维护成本以及低危险操作。
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10.发明申请PROCESS AND APPARATUS FOR ONLINE REJUVENATION OF CONTAMINATED SULFOLANE SOLVENT 审中-公开污染磺化溶剂在线重新使用的工艺和装置公开(公告)号：US20090272702A1
公开(公告)日：2009-11-05
申请号：US12112623
申请日：2008-04-30
Applicant: Ping-Wen Yen , Yuh-Sheve Ho , Hung-Tzu Chiu , Chung-Jong Hwu , June-Cheng Chang , Tzong-Bin Lin , Tsoung Y. Yan , Cheng-Tsung Hong , Hung-Chung Shen
Inventor： Ping-Wen Yen , Yuh-Sheve Ho , Hung-Tzu Chiu , Chung-Jong Hwu , June-Cheng Chang , Tzong-Bin Lin , Tsoung Y. Yan , Cheng-Tsung Hong , Hung-Chung Shen
Abstract: A continuous online process for rejuvenating whole stream of contaminated lean sulfolane in an extraction system is provided. In particular, a rejuvenator is installed in the solvent circulation loop to remove the contaminants continuously to keep the solvent clean, effective and less corrosive. Specifically, the rejuvenator comprises a high pressure vessel with a removable cover and a round rack with vertical stainless steel tubes fitted in the high pressure vessel. A magnetic bar is placed in each stainless steel tube. A screen cylinder is installed inside the ring of stainless steel tubes. As the contaminated sulfolane is passed through the rejuvenator, the rejuvenator picks up its contaminants. The rejuvenator can be dissembled to remove the contaminants periodically. The rejuvenator is characterized by simple in construction, reliable in operation, and low in operation and maintenance costs. With this rejuvenator, the extraction system can be operated at high efficiency and high capacity without the dreaded corrosion.
Abstract translation: 提供了一个连续的在线过程，用于在提取系统中恢复受污染的贫环烷砜的全流。 特别地，在溶剂循环回路中安装一个振动器，以连续地去除污染物，以保持溶剂清洁，有效和较少的腐蚀性。 具体来说，复原器包括具有可拆卸盖的高压容器和安装在高压容器中的垂直不锈钢管的圆形架。 在每个不锈钢管中放置一个磁棒。 丝网筒安装在不锈钢管的环内。 当受污染的环丁砜通过振动器时，复原器会吸收其污染物。 可以拆除复原器以定期去除污染物。 振兴器的特点是施工简单，运行可靠，运行维护成本低。 通过这种振兴器，提取系统可以高效率和高容量地运行，而不会产生可怕的腐蚀。
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