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    Process for the preparation of anionic clay
    1.
    发明授权
    Process for the preparation of anionic clay 失效
    阴离子粘土的制备方法

    公开(公告)号：US06593265B2

    公开(公告)日：2003-07-15

    申请号：US10071385

    申请日：2002-02-07

    申请人： Dennis Stamires ,  William Jones ,  Sjoerd Daamen

    发明人： Dennis Stamires ,  William Jones ,  Sjoerd Daamen

    IPC分类号： B01J2100

    CPC分类号： C04B35/6261 ,  B01J21/16 ,  B01J23/005 ,  B01J23/007 ,  B01J37/0036 ,  B01J37/0045 ,  C01F7/005 ,  C01P2002/22 ,  C01P2002/50 ,  C01P2002/72 ,  C01P2002/78 ,  C01P2006/10 ,  C01P2006/21 ,  C04B35/62645 ,  C04B35/62805 ,  C04B35/62815 ,  C04B2235/3206 ,  C04B2235/3222

    摘要： A process for preparing a 3R1-type crystalline anionic clay comprising the steps of: a) preparing an aqueous precursor mixture comprising aluminum trihydrate or a thermally treated form thereof and a magnesium source, the magnesium source is milled before use or when present in the precursor mixture, b) aging the precursor mixture at temperatures in the range 30°-100° C. to obtain the crystalline clay product, and c) optionally shaping the product of step b). Milling of the magnesium source, either alone or in combination with the (thermally treated) aluminum trihydrate, results in a faster reaction and higher conversion to anionic clay. The resulting anionic clay can be obtained by simply drying the slurry retrieved from the reactor. There is no need for washing or filtering, and a wide range of ratios of Mg/Al in the reaction product is possible.

    摘要翻译： 一种制备3R1型结晶阴离子粘土的方法，包括以下步骤：a）制备包含三水合铝或其热处理形式和镁源的含水前体混合物，镁源在使用前或当存在于前体中时被研磨 混合物，b）在30°-100℃的温度下老化前体混合物以获得结晶粘土产品，和c）任选地使步骤b）的产物成型。单独或组合的镁源的加工 与（热处理）三水合铝相比，导致反应速度更快，对阴离子粘土的转化率更高。 所得到的阴离子粘土可以通过简单地干燥从反应器中回收的浆料来获得。 不需要洗涤或过滤，反应产物中Mg / Al的比例范围很宽。

    Process for the Preparation of an Additive-Containing Anionic Clay
    2.
    发明申请
    Process for the Preparation of an Additive-Containing Anionic Clay 审中-公开
    制备含添加剂的阴离子粘土的方法

    公开(公告)号：US20080032884A1

    公开(公告)日：2008-02-07

    申请号：US11587395

    申请日：2005-04-26

    申请人： William Jones ,  Dennis Stamires ,  Paul O'Connor ,  Michael Brady

    发明人： William Jones ,  Dennis Stamires ,  Paul O'Connor ,  Michael Brady

    IPC分类号： B01J21/16

    CPC分类号： B01J21/16 ,  B01J23/007 ,  B01J23/10 ,  B01J37/0036

    摘要： Process for the preparation of an additive-containing anionic clay comprising the steps of (a) milling a physical mixture of a divalent metal compound and a trivalent metal compound, (b) calcining the physical mixture at a temperature in the range 200-800° C., and (c) rehydrating the calcined mixture in aqueous suspension, wherein an additive is present in the physical mixture and/or the aqueous suspension of step (c). With this process additive-containing anionic clays with a homogeneous additive distribution can be prepared.

    摘要翻译： 制备含添加剂的阴离子粘土的方法包括以下步骤：（a）研磨二价金属化合物和三价金属化合物的物理混合物，（b）在200-800℃的温度下煅烧该物理混合物 和（c）在水悬浮液中再水化煅烧的混合物，其中添加剂存在于步骤（c）的物理混合物和/或水悬浮液中。 使用该方法可以制备具有均匀添加剂分布的含添加剂的阴离子粘土。

    Process for producing anionic clay using non-peptized boemite and compositions produced therefrom
    4.
    发明授权
    Process for producing anionic clay using non-peptized boemite and compositions produced therefrom 有权
    使用非胶溶的波希米特生产阴离子粘土的方法和由其生产的组合物

    公开(公告)号：US06541409B1

    公开(公告)日：2003-04-01

    申请号：US09491263

    申请日：2000-01-26

    申请人： William Jones ,  Dennis Stamires ,  Michael Brady

    发明人： William Jones ,  Dennis Stamires ,  Michael Brady

    IPC分类号： B01J2116

    CPC分类号： B01J23/007 ,  C01F7/005 ,  C01F7/162 ,  C01P2002/22 ,  C01P2002/70 ,  C01P2004/32

    摘要： An economical and environment-friendly processes for the synthesis of anionic clays and the products made therefrom. It involves reacting a slurry comprising non-peptized boehmite with a magnesium source. There is no necessity to wash or filter the product. It can be spray dried directly to form microspheres or can be extruded to form shaped bodies. The product can be combined with other ingredients in the manufacture of catalysts, absorbents, pharmaceuticals, cosmetics, detergents, and other commodity products that contain anionic clays.

    摘要翻译： 用于合成阴离子粘土和由其制备的产品的经济和环境友好的方法。 它包括使包含非胶溶勃姆石的浆料与镁源反应。 没有必要洗涤或过滤产品。 它可以直接喷雾干燥以形成微球体，或者可以挤出形成成型体。 该产品可以与制造催化剂，吸收剂，药物，化妆品，洗涤剂和其他含有阴离子粘土的商品一起制成其他成分。

    Catalyst composition comprising anionic clay and rare earth metals, its preparation and use in FCC
    5.
    发明授权
    Catalyst composition comprising anionic clay and rare earth metals, its preparation and use in FCC 有权
    包含阴离子粘土和稀土金属的催化剂组合物，其制备和用于FCC

    公开(公告)号：US07576024B2

    公开(公告)日：2009-08-18

    申请号：US10582177

    申请日：2004-12-06

    申请人： William Jones ,  Dennis Stamires ,  Paul O'Connor ,  Michael F. Brady

    发明人： William Jones ,  Dennis Stamires ,  Paul O'Connor ,  Michael F. Brady

    IPC分类号： B01J29/06

    CPC分类号： B01J21/16 ,  B01J23/10 ,  B01J37/03 ,  C10G11/04 ,  C10G11/18

    摘要： The invention relates to a composition comprising anionic clay and rare earth metal hydroxy carbonate. This composition can suitably be used in FCC for the reduction of NOx and/or SOx emissions, the reduction of the S and/or N-content in fuels, and as a metal trap.The composition can be prepared by precipitating a divalent metal salt, a trivalent metal salt, and a rare earth metal salt to form a precipitate, calcining the precipitate at 200-800° C., and rehydrating the precipitate in the presence of a carbonate source to form a composition comprising anionic clay and a rare earth metal hydroxy carbonate.

    摘要翻译： 本发明涉及包含阴离子粘土和稀土金属羟基碳酸酯的组合物。 该组合物可以适当地用于FCC中用于还原NOx和/或SO x排放，降低燃料中的S和/或N含量，以及作为金属阱。 该组合物可以通过沉淀二价金属盐，三价金属盐和稀土金属盐来制备，以形成沉淀物，在200-800℃下煅烧沉淀物，并在碳酸盐源存在下再沉淀沉淀物 以形成包含阴离子粘土和稀土金属羟基碳酸酯的组合物。

    Process for producing anionic clay using two types of alumina compounds
    7.
    发明授权
    Process for producing anionic clay using two types of alumina compounds 失效
    使用两种氧化铝化合物生产阴离子粘土的方法

    公开(公告)号：US06815389B2

    公开(公告)日：2004-11-09

    申请号：US10042730

    申请日：2002-03-15

    申请人： Dennis Stamires ,  Michael F. Brady ,  William Jones ,  Fathi Kooli

    发明人： Dennis Stamires ,  Michael F. Brady ,  William Jones ,  Fathi Kooli

    IPC分类号： B01J2116

    CPC分类号： C01F7/005 ,  B01J21/005 ,  B01J21/16 ,  B01J23/007 ,  B01J29/049 ,  C01F7/00 ,  C01F7/162 ,  C01P2002/22 ,  C01P2002/54 ,  C01P2002/72 ,  C01P2004/32

    摘要： An economical and environment-friendly process for the synthesis of anionic clays with carbonate and/or hydroxide anions as the charge-balancing interlayer species is disclosed. The process involves reacting a slurry comprising an aluminum source and a magnesium source, the aluminum source comprising two types of aluminum-containing compounds, preferably aluminum trihydrate and/or thermally treated calcined aluminum trihydrate. There is no necessity to wash or filter the product. It can be spray dried directly to form microspheres or can be extruded to form shaped bodies. The product can be combined with other ingredients in the manufacture of catalysts, absorbents, pharmaceuticals, cosmetics, detergents, and other commodity products.

    摘要翻译： 公开了一种用于合成具有碳酸盐和/或氢氧根阴离子作为电荷平衡层间物质的阴离子粘土的经济和环境友好的方法。 该方法包括使包含铝源和镁源的浆料反应，铝源包含两种类型的含铝化合物，优选三水合铝和/或经热处理的煅烧铝三水合物。 没有必要洗涤或过滤产品。 它可以直接喷雾干燥以形成微球体，或者可以挤出形成成型体。 该产品可以与催化剂，吸收剂，药物，化妆品，洗涤剂和其他商品的制造中的其他成分组合。

    Process for the preparation of quasi-crystalline boehmites
    8.
    发明授权
    Process for the preparation of quasi-crystalline boehmites 失效
    制备准晶体勃艮第的方法

    公开(公告)号：US06506358B1

    公开(公告)日：2003-01-14

    申请号：US09636694

    申请日：2000-08-11

    申请人： Dennis Stamires ,  Paul O'Connor ,  Gregory Pearson ,  William Jones

    发明人： Dennis Stamires ,  Paul O'Connor ,  Gregory Pearson ,  William Jones

    IPC分类号： C01F700

    CPC分类号： C01F7/448 ,  B01J21/04 ,  C01F7/34 ,  C01F7/36 ,  C01P2002/04 ,  C01P2002/72

    摘要： The present invention pertains to an improved process for the preparation of quasi-crystalline boehmite. In this improved process a quasi-crystalline boehmite precursor is aged at a pH below 7, prefereably under hydrothermal conditions. It was found that when conducting the preparation processes for quasi-crystalline aluminas described in the prior art at a pH below 7 and under hydrothermal conditions instead of the high pH and thermal aging used in the prior art, QCBs with higher crystallinity are obtained. In the process according to the invention additives may be added to the quasi-crystalline boehmite precursor. This results in a high quality QCB with additives in a homogeneously dispersed state. Suitable additives are compounds containing elements selected from the group of rare earth metals alkaline earth metals, transition metals, actinides, silicon, gallium, boron, and phosphorus.

    摘要翻译： 本发明涉及制备准晶状勃姆石的改进方法。 在这种改进的方法中，准结晶勃姆石前体在pH低于7的条件下老化，优选在水热条件下。 发现在现有技术中描述的准晶体氧化铝的制备方法在pH低于7且在水热条件下代替现有技术中使用的高pH和热老化，获得具有较高结晶度的QCB。 在根据本发明的方法中，可以将添加剂加入到准结晶勃姆石前体中。 这导致具有均匀分散状态的添加剂的高质量QCB。 合适的添加剂是含有选自稀土金属碱土金属，过渡金属，锕系元素，硅，镓，硼和磷的元素的化合物。

    Process for the Preparation of a Metal-Containing Composition
    10.
    发明申请
    Process for the Preparation of a Metal-Containing Composition 审中-公开
    含金属组合物的制备方法

    公开(公告)号：US20080039313A1

    公开(公告)日：2008-02-14

    申请号：US11578806

    申请日：2005-04-26

    申请人： William Jones ,  Dennis Stamires ,  Paul O'Connor ,  Michael Brady

    发明人： William Jones ,  Dennis Stamires ,  Paul O'Connor ,  Michael Brady

    IPC分类号： B01J20/08

    CPC分类号： B01J21/16 ,  B01J37/06 ,  B01J37/08

    摘要： Process for the preparation of a metal-containing composition, which process comprises the steps of (a) calcining a physical mixture of an anionic clay and a metal additive at a temperature between 200 and 800° C., and (b) rehydrating the calcined product of step a). This process allows the use of insoluble metal additives. It does not require the use of soluble metal additives, which has economic and environmental advantages.

    摘要翻译： 制备含金属组合物的方法，该方法包括以下步骤：（a）在200-800℃的温度下煅烧阴离子粘土和金属添加剂的物理混合物，和（b）将煅烧过的 步骤a）的产物。 该方法允许使用不溶性金属添加剂。 它不需要使用具有经济和环境优点的可溶性金属添加剂。