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    Process for producing anionic clay using boehmite which has been peptized with an acid
    1.
    发明授权
    Process for producing anionic clay using boehmite which has been peptized with an acid 失效
    使用已经用酸胶溶的勃姆石生产阴离子粘土的方法

    公开(公告)号：US06800578B2

    公开(公告)日：2004-10-05

    申请号：US10271920

    申请日：2002-10-15

    申请人： Dennis Stamires ,  Paul O'Connor ,  William Jones ,  Michael Brady

    发明人： Dennis Stamires ,  Paul O'Connor ,  William Jones ,  Michael Brady

    IPC分类号： B01J2116

    CPC分类号： C01F7/005 ,  B01J23/007 ,  C01F7/162 ,  C01P2002/22 ,  C01P2002/72

    摘要： This patent describes economical and environment-friendly processes for the synthesis of anionic clays. It involves reacting a slurry comprising boehmite, which has been peptized with acid with a divalent metal source followed by addition of source of base. The slurry is then hydrothermally aged. There is no necessity to wash or filter the product and it can be spray dried directly to form microspheres, or can be extruded to form shaped bodies. The product can be combined with other ingredients in the manufacture of catalysts, absorbents, pharmaceuticals, cosmetics, detergents, polymeric nanocomposites and other commodity products that contain anionic clays.

    摘要翻译： 该专利描述了用于合成阴离子粘土的经济和环境友好的方法。 其包括将已经与酸缔合的勃姆石与二价金属源反应，然后加入碱源。 然后将该浆液水热老化。 没有必要洗涤或过滤产品，并且可以直接喷雾干燥以形成微球体，或者可以挤出以形成成形体。 该产品可以与催化剂，吸收剂，药物，化妆品，洗涤剂，聚合物纳米复合材料和其它含有阴离子粘土的商品产品的制造中的其他成分组合。

    Process for the preparation of anionic clay and boehmite-containing compositions
    2.
    发明授权
    Process for the preparation of anionic clay and boehmite-containing compositions 失效
    用于制备阴离子粘土和勃姆石组合物的方法

    公开(公告)号：US06710004B2

    公开(公告)日：2004-03-23

    申请号：US10071386

    申请日：2002-02-07

    申请人： Dennis Stamires ,  William Jones ,  Paul O'Connor

    发明人： Dennis Stamires ,  William Jones ,  Paul O'Connor

    IPC分类号： B01J2116

    CPC分类号： B01J21/04 ,  B01J21/16 ,  B01J23/007 ,  C01B13/363 ,  C01B13/366 ,  C01F7/005 ,  C01F7/162 ,  C01G9/006 ,  C01P2002/22 ,  C01P2002/32 ,  C01P2002/72

    摘要： This invention relates to a process for the preparation of anionic clay and boehmite-containing compositions. These compositions may also contain unreacted trivalent metal source and/or divalent metal source. The process involves subjecting a precursor mixture comprising a divalent metal source and a trivalent metal source to at least two aging steps, wherein at least once between two aging steps an aluminum source is added. An advantage of the invention is that the crystallinity of the boehmite in the composition can be tuned.

    摘要翻译： 本发明涉及一种制备阴离子粘土和勃姆石组合物的方法。 这些组合物还可以含有未反应的三价金属源和/或二价金属源。 该方法包括将包含二价金属源和三价金属源的前体混合物经历至少两个老化步骤，其中在两个老化步骤之间至少一次加入铝源。 本发明的一个优点是可以调节组合物中勃姆石的结晶度。

    Process for making, and use of, anionic clay materials
    3.
    发明授权
    Process for making, and use of, anionic clay materials 有权
    制造和使用阴离子粘土材料的方法

    公开(公告)号：US06479421B1

    公开(公告)日：2002-11-12

    申请号：US09457802

    申请日：1999-12-09

    申请人： Albert A. Vierheilig

    发明人： Albert A. Vierheilig

    IPC分类号： B01J2116

    CPC分类号： C01F7/005 ,  B01J21/10 ,  B01J21/16 ,  B01J23/002 ,  B01J23/007 ,  B01J2523/00 ,  C01B13/14 ,  C01P2002/22 ,  C01P2002/32 ,  C01P2002/72 ,  C01P2006/10 ,  C01P2006/21 ,  C10G11/02 ,  B01J2523/22 ,  B01J2523/31 ,  B01J2523/3712 ,  B01J2523/55

    摘要： Anionic clay compounds such as hydrotalcite-like compounds can be made by a process wherein a non-hydrotalcite-like compound (or a hydrotalcite-like compound) are heat treated and then hydrated to form hydrotalcite-like compounds having properties (e.g.., increased hardness and/or density) that differ from those of hydrotalcite-like compounds made by prior art methods wherein non-hydrotalcite-like compounds (or hydrotalcite-like compounds) are not similarly heat treated and hydrated to form such hydrotalcite-like compounds.

    摘要翻译： 阴离子粘土化合物如类水滑石化合物可以通过其中非水滑石类化合物（或类水滑石样化合物）进行热处理然后水合以形成具有（例如增加的）的类水滑石化合物的方法 硬度和/或密度）与通过现有技术方法制备的类水滑石化合物不同，其中非水滑石样化合物（或水滑石样化合物）不类似地热处理和水合以形成这种类水滑石化合物。

    Vanadia catalyst impregnated on titania-pillared clay for the removal of nitrogen oxide
    4.
    发明授权
    Vanadia catalyst impregnated on titania-pillared clay for the removal of nitrogen oxide 有权
    浸渍在二氧化钛柱状粘土上的Vanadia催化剂用于除去氮氧化物

    公开(公告)号：US06475944B1

    公开(公告)日：2002-11-05

    申请号：US09535747

    申请日：2000-03-27

    申请人： Hee-Sung Yang ,  Seok-Lyong Song ,  Hyun-Chul Choi ,  In-Sik Nam ,  Ho-Jeong Chae

    发明人： Hee-Sung Yang ,  Seok-Lyong Song ,  Hyun-Chul Choi ,  In-Sik Nam ,  Ho-Jeong Chae

    IPC分类号： B01J2116

    CPC分类号： F01N3/2066 ,  B01D53/8628 ,  B01D53/9418 ,  B01D2251/2062 ,  B01D2255/2063 ,  B01D2255/20707 ,  B01D2255/20723 ,  B01D2255/20738 ,  B01D2255/20761 ,  B01J29/049 ,  F01N2610/02 ,  Y02T10/24

    摘要： A catalyst for effectively removing NOx by using NH3 as a reducing agent is disclosed. Particularly, a vanadia impregnated onto Ti-PILC (titania-pillared interlayer clay) is disclosed, which is prepared by the generally known technology. More specifically, a V2O5/Ti-PILC catalyst is disclosed, in which NOx contained in the flue gas from an electric power plant and the like (an excessive amount of SO2 being present in the flue gas stream) is reacted with NH3 (which is injected as a reducing agent) over a vanadia impregnated onto a Ti-PILC, so that they can be converted into harmless nitrogen and water. The V2O5/Ti-PILC catalyst is employed for reducing NOx contained in the exhaust gas stream as well as the large amounts of SO2 into nitrogen and water. The catalyst is prepared by pillaring a titania to a clay by a pillaring method. The V2O5/Ti-PILC catalyst prepared in the present invention reveals a superior NO removal activity under dry and wet conditions compared with the commercial V2O5—WO3/TiO2 catalyst.

    摘要翻译： 公开了一种通过使用NH 3作为还原剂有效地除去NOx的催化剂。 特别地，公开了通过通常已知的技术制备的浸渍在Ti-PILC（二氧化钛柱状夹层粘土）上的氧化钒。 更具体地，公开了一种V2O5 / Ti-PILC催化剂，其中来自发电厂的烟道气中所含的NOx（烟道气中存在过量的SO 2）与NH 3（其是 作为还原剂注入）浸渍在Ti-PILC上的钒氧化物，使得它们可以转化成无害的氮和水。 V2O5 / Ti-PILC催化剂用于将废气流中所含的NOx以及大量的SO2还原成氮和水。 通过柱状法将二氧化钛作为粘土制成催化剂。 本发明制备的V2O5 / Ti-PILC催化剂与商业V2O5-WO3 / TiO2催化剂相比，在干湿条件下显示出优异的NO去除活性。

    Processes for producing a bleaching clay product
    5.
    发明授权
    Processes for producing a bleaching clay product 失效
    用于生产漂白粘土产品的方法

    公开(公告)号：US06288003B1

    公开(公告)日：2001-09-11

    申请号：US09337170

    申请日：1999-06-21

    申请人： Christian P. Fabry ,  Franz K. Kleindl

    发明人： Christian P. Fabry ,  Franz K. Kleindl

    IPC分类号： B01J2116

    CPC分类号： B01J21/16 ,  B01J20/12

    摘要： A process for the production of a bleaching clay product which includes the steps of selecting a naturally occurring hormite clay product, cleaning and crushing the clay product to form clay clumps less than 2 in. in diameter, aging the crushed hormite clay and activating the clay with extremely small amounts of acid, in the range of less than 1 percent, by weight. The process may also be conducted without an aging step. Also, an acceptable bleaching clay product can be produced without the addition of any acid to the aged hormite clay.

    摘要翻译： 一种用于生产漂白粘土产品的方法，其包括选择天然存在的激素粘土产品，清洁和破碎粘土产品以形成直径小于2英寸的粘土块，使粉碎的激素粘土老化并活化粘土 极少量的酸在小于1重量％的范围内。 该方法也可以在没有老化步骤的情况下进行。 此外，可以生产可接受的漂白粘土产品，而不向老化的激素粘土添加任何酸。

    Polymerization catalysts for olefinic and styrenic monomer and polymer production method
    6.
    发明授权
    Polymerization catalysts for olefinic and styrenic monomer and polymer production method 失效
    烯烃和苯乙烯单体的聚合催化剂和聚合物的制备方法

    公开(公告)号：US06255244B1

    公开(公告)日：2001-07-03

    申请号：US09391343

    申请日：1999-09-08

    申请人： Nobuhiro Yabunouchi

    发明人： Nobuhiro Yabunouchi

    IPC分类号： B01J2116

    CPC分类号： C08F12/08 ,  B01J21/16 ,  B01J31/143 ,  B01J31/146 ,  B01J31/2295 ,  B01J31/38 ,  B01J2531/46 ,  C08F4/025 ,  C08F4/65908 ,  C08F4/65912 ,  C08F4/65916 ,  C08F4/65922 ,  C08F10/00 ,  C08F4/6592

    摘要： A catalyst for polymerization of olefins or styrenes, which is prepared by contacting (A) a transition metal compound, (B) at least one material selected from the group consisting of oxygen-containing compounds and compounds which react with a transition metal compound to form an ionic complex, and optionally (C) an alkylating agent with each other, and contacting these materials (A), (B) and (C) with an adsorbing substance (D), during or after the contact of materials (A), (B) and (C) with each other, followed by removing the adsorbing substance (D) from the contacted materials (A), (B) and (C).

    摘要翻译： 一种用于烯烃或苯乙烯聚合的催化剂，其通过使（A）过渡金属化合物，（B）至少一种选自含氧化合物和与过渡金属化合物反应的化合物中的至少一种材料与（A）过渡金属化合物反应形成 离子络合物和任选的（C）烷基化试剂，并且在材料（A）的接触期间或之后使这些材料（A），（B）和（C）与吸附物质（D）接触， （B）和（C），然后从接触材料（A），（B）和（C）中除去吸附物质（D）。

    Clay-titanium tetrachloride catalyst and the preparation thereof
    10.
    发明授权
    Clay-titanium tetrachloride catalyst and the preparation thereof 有权
    四氯化钛催化剂及其制备方法

    公开(公告)号：US06613711B2

    公开(公告)日：2003-09-02

    申请号：US10066417

    申请日：2002-01-31

    申请人： Xuequan Zhang ,  Feng Yang ,  Haichao Zhao

    发明人： Xuequan Zhang ,  Feng Yang ,  Haichao Zhao

    IPC分类号： B01J2116

    CPC分类号： C08F10/00 ,  B01J21/063 ,  B01J21/16 ,  B01J27/135 ,  C08F110/02 ,  C08F4/025 ,  C08F4/6555 ,  C08F4/654

    摘要： The present invention provides a clay-titanium tetrachloride catalyst used for the preparation of polyolefine/clay composite materials, comprising: 1) a phyllosilicate; 2) a magnesium compound selected from the group consisting of MgCl2, Mg(OR)2 and MgR2, wherein R is an alkyl group having 1-8 carbon atoms; 3) an aliphatic alcohol which is capable of dissolving the magnesium compound; 4) titanium tetrachloride TiCl4; and optionally 5) an electron-donor reagent selected from the group consisting of an aromatic ester and an aromatic group substituted or cycloalkyl group substituted alkoxy silane. The present invention also provide a method for the prepare of the catalyst. The nanocomposite materials obtained by using the catalyst have tensile strength of 32-50 MPa and Vicat temperature of 131-220° C.

    摘要翻译： 本发明提供用于制备聚烯烃/粘土复合材料的粘土四氯化钛催化剂，其包括：1）页硅酸盐; 2）选自MgCl 2，Mg（OR）2和MgR 2的镁化合物，其中R是具有1-8个碳原子的烷基; 3）能够溶解镁化合物的脂族醇; 4）四氯化钛TiCl4; 和任选的5）选自芳族酯和芳族取代或环烷基取代的烷氧基硅烷的电子给体试剂。 本发明还提供了制备催化剂的方法。 使用催化剂得到的纳米复合材料的拉伸强度为32-50MPa，维卡温度为131-220℃。