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    Mineral lubricating oil compositions containing alkaline earth metal sulfonates and phosphites and process producing same
    3.
    发明授权
    Mineral lubricating oil compositions containing alkaline earth metal sulfonates and phosphites and process producing same 失效
    含有碱金属硫化物和磷酸盐的矿物润滑油组合物及其生产方法

    公开(公告)号：US3655558A

    公开(公告)日：1972-04-11

    申请号：US3655558D

    申请日：1969-04-24

    Applicant: EXXON RESEARCH ENGINEERING CO

    Inventor： GEYER JEROME ,  HU SHIH-EN ,  ROBBINS MAX L

    IPC: C10M159/20 ,  C10M159/24 ,  C10M1/40

    CPC classification number: C10M159/20 ,  C10M159/24 ,  C10M2201/085 ,  C10M2203/06 ,  C10M2205/026 ,  C10M2207/027 ,  C10M2215/04 ,  C10M2215/065 ,  C10M2215/086 ,  C10M2215/26 ,  C10M2215/28 ,  C10M2217/023 ,  C10M2217/046 ,  C10M2217/06 ,  C10M2219/044 ,  C10M2219/046 ,  C10M2219/087 ,  C10M2219/088 ,  C10M2219/089 ,  C10M2223/041 ,  C10M2223/045 ,  C10M2223/12 ,  C10M2225/04 ,  C10M2225/041 ,  C10N2210/02 ,  C10N2220/02 ,  C10N2230/12

    Abstract: Mineral lubricating oil compositions containing oil-soluble overbased alkaline earth metal hydrocarbon sulfonates, employed in internal combustion engines, are improved as to their antirust, sludge inhibiting and/or antiwear properties by incorporating into such compositions, in colloidal form, small amounts, for example 0.01 to 10.0 wt. percent, of the total oil composition, of in situ formed oil-insoluble inorganic alkaline earth metal phosphorus salts derived from the lower oxy or thio acids of phosphorus or from the corresponding oxides or sulfides of phosphorus which, upon hydrolysis, yield the lower oxy or thio acids of phosphorus. The preferred process of preparing such compositions involves the treatment of the neutral or overbased alkaline earth metal sulfonates, either of petroleum origin or of synthetic long chain alkaryl origin, or mineral oil concentrates thereof, and which have been in the past, conventionally employed as oil additives, with up to the stoichiometric amount of the phosphorus acid, thio acid, oxide or sulfide required to at least partially neutralize the free alkalinity of the overbased sulfonate, filtering therefrom any precipitate formed as a result of such treatment of the sulfonate or oil concentrate thereof, and recovering an oil-soluble alkaline earth metal sulfonate product, or oil concentrate thereof, containing colloidal oilinsoluble alkaline earth metal phosphorus compounds of reducing nature formed in situ.

    Abstract translation: 用于内燃机中的含油溶性高碱性碱土金属烃磺酸盐的矿物润滑油组合物通过以少量例如少量的胶体形式掺入到这种组合物中来改善其防锈，污泥抑制和/或抗磨损性能。 0.01〜10.0重量％ 总原油组成的原位形成的油不溶性无机碱土金属磷盐的衍生自磷的低级或硫代酸或相应的磷的氧化物或硫化物，其在水解时产生较低的氧或 磷的硫酸。 制备这种组合物的优选方法包括处理石油源或合成长链烷芳基来源的中性或高碱性碱土金属磺酸盐或其矿物油浓缩物，并且其在过去常规用作油 添加剂，具有至少部分中和高碱性磺酸盐的游离碱度所需的化学计量的磷酸，硫酸，氧化物或硫化物，从而过滤由于这种处理磺酸盐或油浓缩物而形成的任何沉淀物 并回收含有原位形成的具有还原性质的胶体油不溶性碱土金属磷化合物的油溶性碱土金属磺酸盐产物或其油浓缩物。

    Microemulsion separation of organic compounds in liquid state
    5.
    发明授权
    Microemulsion separation of organic compounds in liquid state 失效
    有机化合物在液体状态下的微乳液分离

    公开(公告)号：US3641181A

    公开(公告)日：1972-02-08

    申请号：US3641181D

    申请日：1969-09-10

    Applicant: EXXON RESEARCH ENGINEERING CO

    Inventor： ROBBINS MAX L ,  BROWNAWELL DARRELL W

    IPC: B01D11/04 ,  B01D12/00 ,  C07C7/00 ,  C07C7/10 ,  C07C7/02 ,  C10G

    CPC classification number: B01D11/0492 ,  B01D12/00 ,  C07C7/00

    Abstract: A PROCESS FOR SEPARATING A MIXTURE CONTAINING LIQUID ORGANIC COMPOUNDS, HAVING DIFFERENT INTERFACIAL TENSIONS WHEN MEASURED AGAINST SUBSTANTIALLY HYDROCARBON-INSOLUBLE POLAR LIQUIDS, INTO ITS COMPONENT PARTS COMPRISES THE STEPS OF COMBINING SAID MIXTURE OF ORGANIC LIQUIDS WITH SURFACTANTS AND WITH A POLAR LIQUID SUBSTANTIALLY IMMISCIBLE WITH ANY OF THE COMPONENTS OF THE MIXTURE BEING SEPARATED THEREBY SELECTIVELY FORMING TWO PHASES, ONE BEING A MICROEMULSION RICH IN THE ORGANIC COMPONENTS HAVING THE LOWER INTERFACIAL TENSION, WHWREIN SAID POLAR LIQUID IS THE CONTINUOUS PHASE, AND THE OTHER BEING AN OIL PHASE RICH IN THE COMPONENTS HAVING THE HIGHER INTERFACIAL TENSION WITH RESPECT TO THE POLAR LIQUID. THE TWO PHASES ARE THEN SEPARATED.

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