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    Solid phosphoric acid catalyst
    1.
    发明授权
    Solid phosphoric acid catalyst 失效
    固体磷酸催化剂

    公开(公告)号：US5081086A

    公开(公告)日：1992-01-14

    申请号：US451978

    申请日：1989-12-18

    申请人： Fiona P. Wilcher ,  Tai-Hsiang Chao

    发明人： Fiona P. Wilcher ,  Tai-Hsiang Chao

    IPC分类号： B01J27/16 ,  B01J35/10 ,  C07C2/70

    CPC分类号： B01J35/10 ,  B01J27/16 ,  C07C2/70 ,  B01J35/1038 ,  B01J35/108 ,  C07C2527/173

    摘要： A novel solid phosphoric acid catalyst composition is disclosed. The composite comprises solid phosphoric acid and a refractory oxide binder. The composite is characterized in that 25.0 volume percent or less of the total catalyst pore volume consists of pores having a diameter of 10,000 .ANG. or greater. An improvement in catalyst activity and stability is observed when such a catalyst is utilized in a hydrocarbon conversion process.

    摘要翻译： 公开了一种新型固体磷酸催化剂组合物。 复合材料包括固体磷酸和难熔氧化物粘合剂。 该复合材料的特征在于，总催化剂孔体积的25.0体积％或更小，由直径为10,000或更大的孔组成。 当在烃转化方法中使用这种催化剂时，观察到催化剂活性和稳定性的改善。

    Catalytic condensation process
    3.
    发明授权
    Catalytic condensation process 失效
    催化冷凝过程

    公开(公告)号：US5059737A

    公开(公告)日：1991-10-22

    申请号：US546971

    申请日：1990-07-02

    申请人： Tai-Hsiang Chao ,  Fiona P. Wilcher ,  Mark R. Ford ,  Andrzej Z. Ringwelski

    发明人： Tai-Hsiang Chao ,  Fiona P. Wilcher ,  Mark R. Ford ,  Andrzej Z. Ringwelski

    IPC分类号： B01J27/16 ,  B01J27/182 ,  B01J29/82 ,  B01J29/85 ,  C07C2/18

    CPC分类号： B01J27/16 ,  B01J29/82 ,  B01J29/85 ,  C07C2/18 ,  B01J2229/36 ,  B01J27/182 ,  C07C2527/173

    摘要： A hydrocarbon conversion process which utilizes a solid phosphoric acid catalyst having a total X-ray intensity of at least 40 percent relative to alpha-alumina. The solid phosphoric acid catalyst is produced by crystallizing an amorphous mixture of an acid oxide of phosphorus and a siliceous material at a temperature of from 350.degree. to 450.degree. C. and in the presence of from 10 to 50 mole percent water vapor based upon the total vapor rate to the crystallizing means. Embodiments of the new hydrocarbon conversion process include alkylation, oligomerization, and hydration, of hydrocarbons and oxygenated hydrocarbons.

    摘要翻译： 烃转化方法，其使用相对于α-氧化铝具有至少40％的总X射线强度的固体磷酸催化剂。 固体磷酸催化剂是通过在350-450℃的温度下和在10-50摩尔％水蒸气存在下，将磷和二氧化硅材料的无定形混合物结晶在基于 与结晶装置的总蒸气速率。 新的烃转化方法的实施方案包括烃和氧化烃的烷基化，低聚和水合。

    Die and method for forming honeycomb structures
    7.
    发明授权
    Die and method for forming honeycomb structures 失效
    用于形成蜂窝结构的模具和方法

    公开(公告)号：US4747986A

    公开(公告)日：1988-05-31

    申请号：US946234

    申请日：1986-12-24

    申请人： Tai-Hsiang Chao

    发明人： Tai-Hsiang Chao

    IPC分类号： B28B3/20 ,  B29C47/20 ,  B29C47/12

    CPC分类号： B29C47/0028 ,  B28B3/269 ,  B29C47/12 ,  B29L2031/60

    摘要： An extrusion die for producing multichanneled structures from an extrudable material. The die is composed of a series of pins that correspond to the shape of the channels in the structure. At one end of the pins, the area between the pins is open to define a discharge zone having the shape of the structure. At their opposite ends, the pins are connected about adjacent corners by a series of webs. Slots bordered by the pins and the webs define a series of feed passages that communicate with the discharge zone at areas of reduced width between adjacent pins.

    摘要翻译： 一种用于从可挤出材料制造多通道结构的挤出模头。 模具由对应于结构中的通道的形状的一系列销组成。 在销的一端，销之间的区域打开以限定具有该结构形状的排放区。 在它们的相对端，销通过一系列网连接在相邻的拐角处。 通过销和腹板限定的槽限定了一系列进料通道，其在相邻销之间的宽度减小的区域处与排出区域连通。

    Platinum group and phosphorus containing catalyst composition for hydrocarbon conversion
    8.
    发明授权
    Platinum group and phosphorus containing catalyst composition for hydrocarbon conversion 失效
    用于烃转化的铂族和含磷催化剂组合物

    公开(公告)号：US4463104A

    公开(公告)日：1984-07-31

    申请号：US408544

    申请日：1982-08-16

    申请人： George J. Antos ,  Tai-Hsiang Chao

    发明人： George J. Antos ,  Tai-Hsiang Chao

    IPC分类号： B01J23/89 ,  B01J27/185 ,  C10G35/09 ,  B01J27/14

    CPC分类号： C10G35/09 ,  B01J23/8966 ,  B01J27/1856

    摘要： A new catalyst composition for converting hydrocarbons is disclosed. Also disclosed is a method for making the catalyst. The catalyst comprises a platinum group component and a phosphorous component with a porous support material. The catalyst is made by compositing a platinum group component with a porous support material and then contacting that composite with phosphorus or a compound of phosphorus. In a preferred embodiment of the invention a catalyst comprising platinum, phosphorus and chlorine with alumina is utilized in the catalytic reforming of hydrocarbons boiling in the gasoline range to produce a high octane reformate suitable for gasoline blending or a high aromatics content reformate suitable as a petrochemical feedstock.

    摘要翻译： 公开了用于转化烃的新的催化剂组合物。 还公开了制备催化剂的方法。 该催化剂包含铂族组分和具有多孔载体材料的磷组分。 催化剂是通过将铂族组分与多孔载体材料合并然后使该复合物与磷或磷化合物接触来制备的。 在本发明的优选实施方案中，在汽油范围内沸腾的烃的催化重整中使用包含铂，磷和氯与氧化铝的催化剂，以产生适用于汽油共混的高辛烷值重整产物或适用作石油化学品的高芳族化合物重整油 原料。

    Preparation of alumina hydrosol from aluminum sulfate solution
    9.
    发明授权
    Preparation of alumina hydrosol from aluminum sulfate solution 失效
    从硫酸铝溶液制备氧化铝水溶胶

    公开(公告)号：US4447351A

    公开(公告)日：1984-05-08

    申请号：US457547

    申请日：1983-01-12

    申请人： Tai-Hsiang Chao

    发明人： Tai-Hsiang Chao

    IPC分类号： B01J21/04 ,  C01F7/02 ,  C01F7/56 ,  B01J13/00

    CPC分类号： C01F7/56 ,  B01J21/04 ,  C01F7/02

    摘要： The present invention relates to a method of preparing an alumina hydrosol from an aluminum sulfate solution. The subject method comprises the steps of admixing a stoichiometric amount of a metal selected from the group consisting of calcium, strontium and/or barium in the form of a mixture of a hydrated chloride metal salt and a metal hydroxide with an aqueous aluminum sulfate solution, filtering the resulting metal sulfate precipitate from the above admixture, recovering a substantially sulfur-free aluminum-containing filtrate solution, admixing aluminum metal with the filtrate solution, and digesting the aluminum metal at digestion conditions with the filtrate solution to form an alumina hydrosol possessing the desired Al:Cl weight ratio.

    摘要翻译： 本发明涉及从硫酸铝溶液制备氧化铝水溶胶的方法。 本发明方法包括以化学计量的量将选自钙，锶和/或钡的金属与水合氯化金属盐和金属氢氧化物的混合物与硫酸铝水溶液混合的步骤， 从上述混合物中过滤得到的金属硫酸盐沉淀物，回收基本上不含硫的含铝滤液，将铝金属与滤液溶液混合，并在消解条件下用滤液消解铝金属，形成具有 所需的Al：Cl重量比。

    Die for extruding and wash coating
    10.
    发明授权
    Die for extruding and wash coating 失效
    用于挤出和洗涤涂层的模具

    公开(公告)号：US4884960A

    公开(公告)日：1989-12-05

    申请号：US190867

    申请日：1988-05-06

    申请人： Tai-Hsiang Chao

    发明人： Tai-Hsiang Chao

    IPC分类号： B01J37/00 ,  B28B3/20 ,  B28B3/26 ,  F01N3/28

    CPC分类号： B28B3/269 ,  B01J37/0009 ,  B28B3/2636 ,  F01N3/2828 ,  F01N2330/06

    摘要： A honeycombed structure is extruded and wash coat applied to the interior channels of the structure before the honeycomb structure is separated from the die in which it is formed. This method produces the honeycombed structure using a die that includes a die body having an inlet and an outlet side, a plurality of parallel pins defined by the body that correspond to the shape of the channels in the honeycombed structure, and a discharge zone that communicates directly with the outlet side of the die and is defined by the open area between the pins. The extrudable material enters the discharge zone from a series of feed passages defined by the pins and a plurality of webs that interconnect the pins. Each pin has an interior duct with an opening at the end of each pin. A series of internal passages in the die body receive fluid from one or more ports on the periphery of the die and distribute the fluid to the ducts. Spraying the wash coat from the ends of the pins eliminates the need for a separate wash coat step after the honeycombed structure has been formed. In addition, wash coat is continually applied to the interior walls of the channel by the duct as the channel passes the end of the pin so that the entire length of the channel is covered with wash coat. This invention can be used in a wide variety of die configurations, but is especially suited for a die having segmented slots for feed passages and square channel forming pins defined in part by the segmented slots.

    摘要翻译： 在蜂窝结构与其形成的模具分离之前，蜂窝结构被挤压和洗涤涂层施加到结构的内部通道。 该方法使用包括具有入口和出口侧的模具体的模具和由本体限定的与蜂窝结构中的通道的形状相对应的多个平行销的模具产生蜂窝结构，以及连通 直接与模具的出口侧并且由销之间的开放区域限定。 可挤压材料从由销钉限定的一系列进给通道和互连销的多个腹板进入排出区。 每个销具有内部导管，每个引脚的末端都有一个开口。 模具体中的一系列内部通道从模具的周边上的一个或多个端口接收流体，并将流体分配到管道。 从针的端部喷涂洗涤涂层，消除了形成蜂窝结构之后需要单独的洗涂步骤。 此外，当通道穿过销的端部时，通过管道将洗衣层连续地施加到通道的内壁，使得通道的整个长度被覆盖着涂层。 本发明可以用于各种模具结构，但是特别适合于具有用于进给通道的分段槽和部分由分段槽限定的方形通道形成销的模具。