摘要:
A cephalosporin compound represented by the formula (I) or (I') ##STR1## wherein R.sup.1 represents a phenyl group, a 2-thienyl group or a phenoxy group; R.sup.2 represents a hydrogen atom, an alkyl group having 1 to 4 carbon atoms which may be substituted with a phenyl group, an alkoxy group having 1 to 4 carbon atoms or a halogen atom, or a phenyl group which may be substituted with one or two groups selected from the group consisting of a halogen atom, a nitro group, an alkyl group having 1 to 4 carbon atoms and an alkoxy group having 1 to 4 carbon atoms; R.sup.3 represents a hydrogen atom or an alkyl group having 1 to 4 carbon atoms which may be substituted with a monoalkylamino group having 1 to 4 carbon atoms in the alkyl moiety thereof, a dialkylamino group having 1 to 4 carbon atoms in each alkyl moiety thereof, a halogen atom or a phenyl group which may be substituted with one to three groups selected from the group consisting of a halogen atom, a nitro group, an alkyl group having 1 to 4 carbon atoms and an alkoxy group having 1 to 4 carbon atoms; R.sup.4 represents an alkyl group having 1 to 4 carbon atoms; A has up to 15 carbon atoms and represents a straight or branched chain alkylene group, a straight or branched chain alkenylene group, a straight or branched chain alkadienylene group or a phenylene group, and n is 0 or 1; or the salt thereof; and a process for preparing the same.
摘要:
A process for preparing a cephalosporanic acid derivative or a 7-acylaminocephalosporanic acid derivative which comprises subjecting an esterifying agent to reaction in liquid sulfur dioxide in the presence of a base with an N-protected-cephalosporin C to obtain a diester, subjecting the diester to reaction in an inert solvent with an iminohalide forming agent to produce an iminohalide, subjecting the iminohalide with a lower alcohol to produce an iminoether, subjecting the product produced, after subjecting the iminoether to reaction with a reactive derivative of an organic acid, to hydrolysis and further eliminating the ester group of the carboxylic acid.
摘要:
A novel ester of a cephem compound having a carboxyl group at the 4-position in the nucleus; a process for preparing the same by reacting a cephem carboxylic acid or its salt with a halogenide; and a method for removing the protective group for the carboxyl group in the nucleus of a cephem compound by contacting it with an alcohol, or with an organic solvent in the presence of a Lewis acid.
摘要:
A process for preparing a cephalosporin ester which comprises subjecting an organic halide or an alcohol to reaction with a cephalosporin acid, a cephalosporin acid halide or a salt thereof in the presence of liquid sulfur dioxide.
摘要:
An exhaust valve for a supercritical fluid chromatography apparatus. The exhaust valve is a constant-pressure release valve which maintains the pressure inside the flow passage system of the apparatus constant. Eluates are discharged via the valve. An organic solvent effective at atmospheric pressures, such as toluene, dichloromethane, or benzene, which readily dissolves the analyzed sample at ordinary temperature, is introduced either in the flow passage on the upstream side of the valve or in the flow passage in the valve to prevent the flow passage in the valve from clogging.
摘要:
A battery pack includes: a battery having a main surface; and a resin layer capable of being integrated with an armor member armoring the battery so that at least a part of the main surface of the battery is exposed and covering the main surface of the battery, wherein the resin layer is formed by curing a reaction curable resin having a viscosity of not less than 80 mPa·second to less than 1000 mPa·second and a thickness of the resin layer on the main surface of the battery ranges from 0.05 mm to smaller than 0.4 mm.
摘要:
A battery pack includes a battery and a casing covering the battery and formed of a shape-memory resin. A portion or the entirety of the casing is deformed by heating at a predetermined temperature. The deformed casing returns to an original shape at the predetermined temperature or higher.
摘要:
An accurately controllable two-stage pump assembly comprising two plunger pumps connected in series. The suction port of the outlet pump A is connected to the discharge port of the inlet pump B, so that the discharge port of the outlet pump A and the suction port of the inlet pump B act as the discharge port and the suction port, respectively, of the whole pump assembly. While the inlet pump B is delivering fluid from the whole pump assembly, the outlet pump A completes the filling stroke of the whole pump assembly and fully increases the pressure inside the chamber of the outlet pump A. While the inlet pump B is filling, the outlet pump A is in the stage of displacement stroke and delivers fluid from the whole pump assembly. The plungers of the pumps are moved via cams by stepper motors which swing or rotate back and forth within a certain angular range.
摘要:
A battery pack includes: a battery having a main surface; and a resin layer capable of being integrated with an armor member armoring the battery so that at least a part of the main surface of the battery is exposed and covering the main surface of the battery, wherein the resin layer is formed by curing a reaction curable resin having a viscosity of not less than 80 mPa·second to less than 1000 mPa·second and a thickness of the resin layer on the main surface of the battery ranges from 0.05 mm to smaller than 0.4 mm.
摘要:
There are provided a method for imparting a high-durability function to a polymer formed article, which can efficiently impart various function-imparting agents to the polymer formed article, can decrease processing waste liquid as much as possible and recover the waste liquid and the function-imparting agents, can also reuse them as needed, and moreover, can impart the function-imparting agents to the polymer formed article by a continuous system, not by a batch system; and an apparatus thereof.A method for imparting a function to a polymer formed article, which comprises spraying a supercritical fluid to the polymer formed article to firmly fix a function-imparting agent to the polymer formed article.