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    Catalysts and method for the production of amines
    6.
    发明授权
    Catalysts and method for the production of amines 有权
    用于生产胺的催化剂和方法

    公开(公告)号：US07183438B2

    公开(公告)日：2007-02-27

    申请号：US10507602

    申请日：2003-03-07

    申请人： Till Gerlach ,  Frank Funke ,  Johann-Peter Melder ,  Stefan Iselborn ,  Martin Rudloff ,  Michael Hüllmann

    发明人： Till Gerlach ,  Frank Funke ,  Johann-Peter Melder ,  Stefan Iselborn ,  Martin Rudloff ,  Michael Hüllmann

    IPC分类号： C07C209/16 ,  C07C209/18 ,  C07C209/29 ,  B01J23/40 ,  B01J23/42

    CPC分类号： C07C213/02 ,  B01J23/70 ,  B01J23/755 ,  B01J37/03 ,  B01J37/06 ,  C07C209/16 ,  C07C209/26 ,  C07D295/023 ,  C07C211/03 ,  C07C217/08

    摘要： Disclosed are catalysts, the catalytically active mass of which contains 22 to 40 percent by weight of oxygen-containing compounds of zirconium, calculated as ZrO2, 1 to 30 percent by weight of oxygen-containing compounds of copper, calculated as CuO, 15 to 50 percent by weight of oxygen-containing compounds of nickel, calculated as NiO, the molar ratio between nickel and copper being greater than 1, 15 to 50 percent by weight of oxygen-containing compounds of cobalt, calculated as CoO, and less than 1 percent by weight of an alkali metal, calculated as alkali metal oxide, prior to being treated with hydrogen. Also disclosed is a method for the production of amines by reacting primary and secondary alcohols, aldehydes, or ketones with hydrogen and nitrogen compounds selected from the group ammonia, primary and secondary amines, in the presence of said catalysts at an elevated temperature and an elevated pressure.

    摘要翻译： 公开了催化剂，其催化活性物质含有22至40重量％的以ZrO 2计算的含氧化合物的锆，1至30重量％的含氧化合物的铜 ，以CuO计，15至50重量％的含氧化合物的镍，以NiO计算，镍和铜之间的摩尔比大于15重量％，含氧化合物的化合物为15至50重量％ 作为CoO，并且在用氢处理之前少于1重量％的碱金属（以碱金属氧化物计）。 还公开了一种通过使伯醇和仲醇，醛或酮与选自氨，伯胺和仲胺的氢和氮化合物在所述催化剂存在下在升高的温度和升高的温度下生产胺的方法 压力。

    Method for Preparing Aminodiglycol (Adg) and Morpholine
    9.
    发明申请
    Method for Preparing Aminodiglycol (Adg) and Morpholine 审中-公开
    制备氨基二甘醇（Adg）和吗啉的方法

    公开(公告)号：US20080255351A1

    公开(公告)日：2008-10-16

    申请号：US12088718

    申请日：2006-09-25

    申请人： Bram Willem Hoffer ,  Holger Evers ,  Petr Kubanek ,  Till Gerlach ,  Johann-Peter Melder ,  Frank Funke ,  Matthias Frauenkron ,  Helmut Schmidtke

    发明人： Bram Willem Hoffer ,  Holger Evers ,  Petr Kubanek ,  Till Gerlach ,  Johann-Peter Melder ,  Frank Funke ,  Matthias Frauenkron ,  Helmut Schmidtke

    IPC分类号： C07D265/30

    CPC分类号： C07D295/023 ,  C07C213/02 ,  C07C217/08

    摘要： Processes comprising: providing a starting material comprising diethylene glycol; and reacting the starting material with ammonia in the presence of a heterogeneous transition metal catalyst to form a reaction product comprising aminodiglycol and morpholine; wherein the catalyst comprises a catalytically active composition, which prior to treatment with hydrogen, comprises a mixture of oxygen-containing compounds of copper, nickel, cobalt and at least one of aluminum and zirconium; and wherein the catalyst is present as one or more shaped catalyst particles selected from spheres, extrudates, pellets and other geometries, wherein the sphere or extradate has a diameter of

    摘要翻译： 方法包括：提供包含二甘醇的原料; 并在非均相过渡金属催化剂存在下使原料与氨反应形成包含氨基二甘醇和吗啉的反应产物; 其中所述催化剂包含催化活性组合物，其在用氢处理之前包含铜，镍，钴和铝和锆中的至少一种的含氧化合物的混合物; 并且其中所述催化剂作为选自球体，挤出物，丸粒和其它几何形状的一种或多种成型催化剂颗粒存在，其中所述球体或引体具有<3mm的直径，所述颗粒具有<3mm的高度，而另一个 几何形状具有等效直径L = 1 / a'<0.70mm，其中a'是每单位体积的外表面积（mm×s×2 / 由 定义的 3 MI> a = A / MSUB> V p 其中A < SUB>是催化剂颗粒的外表面积（mm 2），V p是催化剂颗粒的体积（mm 3） 3＆lt; 3＆gt; 3＆lt; 3＆gt;）。