摘要:
A method for manufacturing β-sialon, including: a mixing process wherein at least one of aluminum oxide and silicon oxide, silicon nitride, aluminum nitride, and europium compound are mixed; a burning process wherein the mixture having undergone the mixing process is heated at the temperature hither than 1950° C. but not exceeding 2200° C. for 10 hours or longer; and a heat treatment process wherein heat treatment is conducted after the burning process at the temperature from 1300° C. to 1600° C. in an atmosphere of inert gas other than nitrogen at the partial pressure of 10 kPa or lower.
摘要:
A method of manufacturing β-SiAlON represented by a general formula Si6-zAlzOzN8-z:Eu, including a baking step for baking a powdered material that contains Al content from 0.3 to 1.2 mass %, O content from 0.15 to 1 mass %, O/Al molar ratio from 0.9 to 1.3, Si content from 58 to 60 mass %, N content from 37 to 40 mass %, N/Si molar ratio from 1.25 to 1.45, and Eu content from 0.3 to 0.7 mass %. The baking step is a step of baking the powdered material in a nitrogen atmosphere at temperatures from 1850° C. to 2050° C., and the manufactured β-SiAlON satisfies 0.280≦x≦0.340 and 0.630≦y≦0.675 on the CIExy chromaticity coordinate.
摘要翻译:一种制造由通式Si 6-z Al z O z N 8 -z:Eu表示的-SiAlON的方法,包括用于焙烧含有0.3至1.2质量%的Al含量的粉末材料,O含量为0.15至1质量%的烘烤步骤, O / Al摩尔比为0.9〜1.3,Si含量为58〜60质量%,N含量为37〜40质量%,N / Si摩尔比为1.25〜1.45,Eu含量为0.3〜0.7质量%。 烘烤步骤是在氮气气氛中在1850℃至2050℃的温度下烘烤粉末材料的步骤,并且所制造的-SiAlON满足0.280≦̸ x< l1; 0.340和0.630≦̸ y≦̸ 0.675 on CIExy色度坐标。
摘要:
β-SiAlON represented by a general formula Si6-zAlzOzN8-z with Eu dissolved therein, whose spin density corresponding to absorption g=2.00±0.02 at 25° C. obtained by the electron spin resonance method is equal to or lower than 6.0×1016 spins/g. A method of manufacturing the β-SiAlON includes: a mixing step of mixing β-SiAlON materials; a baking step of baking the β-SiAlON having undergone the mixing step; a heating step of increasing the ambient temperature of the materials having undergone the mixing step from 1500° C. to a baking temperature of the baking step at a rate equal to or lower than 2° C/min.; an annealing step of annealing the β-SiAlON having undergone the baking step; and an acid treatment step of acid-treating the β-SiAlON having undergone the annealing step. The objective of the present invention is to provide β-SiAlON capable of achieving high luminescent efficiency, a method of manufacturing the β-SiAlON, and a light-emitting device using the β-SiAlON.
摘要:
β-SiAlON represented by a general formula Si6-zAlzOzN8-z with Eu dissolved therein, whose spin density corresponding to absorption g=2.00±0.02 at 25° C. obtained by the electron spin resonance method is equal to or lower than 6.0×1016 spins/g. A method of manufacturing the β-SiAlON includes: a mixing step of mixing β-SiAlON materials; a baking step of baking the β-SiAlON having undergone the mixing step; a heating step of increasing the ambient temperature of the materials having undergone the mixing step from 1500° C. to a baking temperature of the baking step at a rate equal to or lower than 2° C./min.; an annealing step of annealing the β-SiAlON having undergone the baking step; and an acid treatment step of acid-treating the β-SiAlON having undergone the annealing step. The objective of the present invention is to provide β-SiAlON capable of achieving high luminescent efficiency, a method of manufacturing the β-SiAlON, and a light-emitting device using the β-SiAlON.
摘要翻译:由通式Si 6-z Al z O z N 8-z表示的-SiAlON,其中Eu被溶解,其通过电子自旋共振法获得的在25℃下对应于吸收g = 2.00±0.02的自旋密度等于或低于6.0× 1016旋/克。 一种制造-SiAlON的方法包括:混合-SiAlON材料的混合步骤; 焙烧步骤,烘焙已经经历混合步骤的&bgr; -SiAlON; 将经过混合步骤的材料的环境温度从1500℃提高至烘烤步骤的烘烤温度的加热步骤,其速度等于或低于2℃/分钟; 退火步骤,退火已经经过烘烤步骤的SiAlON; 以及酸处理已经经过退火步骤的SiAlON的酸处理步骤。 本发明的目的是提供能够实现高发光效率的SiAlON,制造-SiAlON的方法和使用该-SiAlON的发光器件。
摘要:
Provided is a production method of a β-sialon phosphor that europium ions are solid-solved in β-sialon, including a mixing process for mixing raw materials of the β-sialon phosphor; a burning process for burning the raw materials after the mixing process to form the β-sialon phosphor; a HIP treatment process in which the β-sialon phosphor after the burning process is subjected to a HIP treatment; an annealing process in which the β-sialon phosphor after the HIP treatment process is subjected to an annealing treatment; and an acid treatment process in which the β-sialon phosphor after the annealing process is subjected to an acid treatment. According to the production method of a β-sialon phosphor, a β-sialon phosphor excellent in luminescence intensity is obtained.
摘要:
Provided is a production method of a β-sialon phosphor that europium ions are solid-solved in β-sialon, including a mixing process for mixing raw materials of the β-sialon phosphor; a burning process for burning the raw materials after the mixing process to form the β-sialon phosphor; a HIP treatment process in which the β-sialon phosphor after the burning process is subjected to a HIP treatment; an annealing process in which the β-sialon phosphor after the HIP treatment process is subjected to an annealing treatment; and an acid treatment process in which the β-sialon phosphor after the annealing process is subjected to an acid treatment. According to the production method of a β-sialon phosphor, a β-sialon phosphor excellent in luminescence intensity is obtained.
摘要:
A spacer fitted inside a water jacket of a cylinder block in an internal combustion engine is set so that a space formed between an inner peripheral surface of the spacer and an inner wall surface of the water jacket is smaller than a space formed between an outer peripheral surface of the spacer and an outer wall surface of the water jacket. Accordingly, even if a position of the spacer is shifted in a radial direction, the inner peripheral surface of the spacer comes into abutment on the inner wall surface of the water jacket at first. Thereby, the abutment of the outer peripheral surface of the spacer on the outer wall surface of the water jacket is prevented completely. Therefore, hitting sounds of pistons can be blocked by the space between the outer peripheral surface of the spacer and the outer wall surface of the water jacket.
摘要:
A balancer housing of a balancer device disposed to face an oil pan below a crankshaft of an engine, includes oil discharge bores for discharging an oil accumulated in the balancer housing with the rotation of balancer weights. The oil discharge bores are covered by baffle plates for inhibiting the turbulence of a surface of the oil stored in the oil pan. Thus, it is possible to inhibit the entrance of the oil into the balancer housing through the oil discharge bores without provision of a special cover member for covering the oil discharge bores.
摘要:
A relief valve assembly, comprises: a relief valve; a valve housing including a valve path along which the relief valve can slide; a relief inflow portion formed on one end of the valve housing; and relief discharge portions formed at an intermediate location of the valve path of the valve housing and provided with small aperture portions axed large aperture portions formed in communication with one another. A side wherein the relief discharge portions are provided with the small aperture portions is the side near the relief inflow portion.
摘要:
A composite piezoelectric component includes a plurality of piezoelectric resonant elements. Each of the plurality of piezoelectric resonant elements includes a substrate having a first major surface and a second major surface disposed opposite to each other. A pair of vibrating electrodes is disposed on the first and second major surfaces, respectively, so as to oppose each other with the substrate disposed therebetween. A ground electrode which is connected to ground is disposed on at least one of the first and second major surfaces. The plurality of piezoelectric resonant elements are stacked on each other so that the major surface of one substrate opposes the major surface of another substrate. A conductive joining member electrically connects at least two of the vibrating electrodes and the ground electrode of the plurality of piezoelectric resonant elements and mechanically bonds the stacked piezoelectric resonant elements. Each of the substrates of the of the piezoelectric resonant elements other than the piezoelectric resonant element located on the top portion includes a plurality of piezoelectric substrate portions, a conductive material portion arranged between the plurality of piezoelectric substrate portions, with the ground electrodes being provided on the first and second major surfaces of the substrate in the conductive material portion. The plurality of ground electrodes of the piezoelectric resonant elements are electrically connected to one another via the conductive material portions and the conductive joining members.