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公开(公告)号：US5304363A
公开(公告)日：1994-04-19
申请号：US907941
申请日：1992-07-02
IPC分类号： B01D53/86 , B01J20/02 , B01J29/03 , B01J29/04 , B01J29/40 , B01J29/70 , B01J29/82 , B01J29/83 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , C10G47/16 , C01B33/26
CPC分类号： C10G47/16 , B01D53/8628 , B01J20/041 , B01J20/06 , B01J20/08 , B01J20/103 , B01J20/3078 , B01J29/0308 , B01J29/041 , B01J29/40 , B01J29/70 , B01J29/82 , B01J29/83 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , B01J2229/26 , B01J2229/32 , B01J2229/34 , B01J2229/36 , B01J2229/40 , B01J2229/42
摘要： There is provided a porous material. A process for preparing this material involves adding an amphiphilic compound to the reaction mixture for preparing a crystalline oxide. The amphiphilic compound may be a quaternary ammonium cationic surfactant. These surfactants may be in the form of lamellar liquid crystals, and may function as templates for the formation of the present mesoporous oxide materials.
摘要翻译： 提供多孔材料。 制备该材料的方法包括向反应混合物中加入两亲性化合物以制备结晶氧化物。 两亲性化合物可以是季铵阳离子表面活性剂。 这些表面活性剂可以是层状液晶的形式，并且可以用作形成本中介氧化物材料的模板。
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公开(公告)号：US5370785A
公开(公告)日：1994-12-06
申请号：US189773
申请日：1994-02-01
IPC分类号： B01D53/86 , B01J20/02 , B01J29/03 , B01J29/04 , B01J29/40 , B01J29/70 , B01J29/82 , B01J29/83 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , C10G47/16
CPC分类号： C10G47/16 , B01D53/8628 , B01J20/06 , B01J20/08 , B01J20/103 , B01J20/12 , B01J20/18 , B01J29/0308 , B01J29/041 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , B01J2229/26 , B01J2229/32 , B01J2229/34 , B01J2229/36 , B01J2229/40 , B01J2229/42
摘要： There is provided a hydrocarbon conversion process and a process for sorbing a sorbate wherein said conversion and sorption process each comprises the use of a porous material. A process for preparing this material involves adding an amphiphilic compound to the reaction mixture for preparing a crystalline oxide. The amphiphilic compound may be a quaternary ammonium cationic surfactant. These surfactants may be in the form of lamellar liquid crystals, and may function as templates for the formation of the present mesoporous oxide materials.
摘要翻译： 提供烃转化方法和用于吸附山梨酸盐的方法，其中所述转化和吸附方法各自包括使用多孔材料。 制备该材料的方法包括向反应混合物中加入两亲性化合物以制备结晶氧化物。 两亲性化合物可以是季铵阳离子表面活性剂。 这些表面活性剂可以是层状液晶的形式，并且可以用作形成本中介氧化物材料的模板。
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公开(公告)号：US5108725A
公开(公告)日：1992-04-28
申请号：US625238
申请日：1990-12-10
申请人： Jeffrey S. Beck , Cynthia T. Chu , Ivy D. Johnson , Charles T. Kresge , Michael E. Leonowicz , Wieslaw J. Roth , James C. Vartuli
发明人： Jeffrey S. Beck , Cynthia T. Chu , Ivy D. Johnson , Charles T. Kresge , Michael E. Leonowicz , Wieslaw J. Roth , James C. Vartuli
IPC分类号： B01D53/86 , B01J20/02 , B01J29/03 , B01J29/04 , B01J29/40 , B01J29/70 , B01J29/82 , B01J29/83 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , C10G47/16
CPC分类号： B01J29/0308 , B01D53/8628 , B01J20/041 , B01J20/06 , B01J20/08 , B01J20/103 , B01J20/12 , B01J20/18 , B01J29/04 , B01J29/041 , B01J29/40 , B01J29/70 , B01J29/82 , B01J29/83 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , C10G47/16 , B01J2229/26 , B01J2229/32 , B01J2229/34 , B01J2229/36 , B01J2229/40 , B01J2229/42 , Y10S423/30
摘要： This invention relates to a method for synthesizing a new synthetic composition of ultra-large pore crystalline material which can be used as a sorbent or catalyst component for conversion of organic and inorganic compounds. The crystalline material product of this method exhibits unusually large sorption capacity demonstrated by its benzene adsorption capacity of greater than about 15 grams benzene/100 grams at 50 torr and 25.degree. C., a hexagonal electron diffraction pattern that can be indexed with a d.sub.100 value greater than about 18 Angstrom Units and a hexagonal arrangement of uniformly sized pores with a maximum perpendicular cross section of at least about 13 Angstrom units.
摘要翻译： 本发明涉及一种用于合成可用作有机和无机化合物转化的吸附剂或催化剂组分的超大孔结晶材料的新合成组合物的方法。 该方法的结晶材料产品显示出异常大的吸附能力，其吸附能力在50托和25℃时苯吸附量大于约15克苯/ 100克，可以用d100值指数的六方电子衍射图 大于约18埃单位和具有至少约13埃单位的最大垂直截面的均匀尺寸孔的六边形排列。
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公开(公告)号：US5264203A
公开(公告)日：1993-11-23
申请号：US735224
申请日：1991-07-24
申请人： Jeffrey S. Beck , Charles T. Kresge , Michael E. Leonowicz , Wieslaw J. Roth , James C. Vartuli
发明人： Jeffrey S. Beck , Charles T. Kresge , Michael E. Leonowicz , Wieslaw J. Roth , James C. Vartuli
IPC分类号： B01D53/86 , B01J20/02 , B01J29/03 , B01J29/04 , B01J29/40 , B01J29/70 , B01J29/82 , B01J29/83 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , C10G47/16 , C01B33/34
CPC分类号： B01J29/04 , B01D53/8628 , B01J20/041 , B01J20/06 , B01J20/08 , B01J20/103 , B01J20/12 , B01J20/18 , B01J29/0308 , B01J29/041 , B01J29/40 , B01J29/70 , B01J29/82 , B01J29/83 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , C10G47/16 , B01J2229/26 , B01J2229/32 , B01J2229/34 , B01J2229/36 , B01J2229/40 , B01J2229/42
摘要： This invention relates to a new synthetic composition of ultra-large pore crystalline material, e.g., [metallo]silicoaluminophosphate, having a composition, expressed on an anhydrous basis as follows:M.sub.n/q (W.sub.a X.sub.b Y.sub.c Z.sub.d O.sub.h)wherein M is one or more ions; n is the charge of the composition excluding M expressed as oxides; q is the weighted molar average valence of M; n/q is the number of moles or mole fraction of M; W is one or more divalent elements; X is one or more trivalent elements; Y is one or more tetravalent elements; Z is one or more pentavalent elements; a, b, c, and d are mole fractions of W, X, Y, and Z, respectively; (a+b+c+d)=1; a .gtoreq. 0; b, c, and d are each>0; and h is a number of from 1 to 2.5. The crystalline material is prepared by i) crystallizing a reaction mixture comprising sources of W, X, Z and an organic directing agent; ii) contacting the product of i) with a reaction mixture comprising sources of Y and organic directing agent; and iii) maintaining the mixture of ii) under conditions sufficient to form said composition of matter. The composition is suited to use for catalytic conversion of organic compounds.
摘要翻译： 本发明涉及具有如下无水基础的组成的[金属]硅铝磷酸盐的超大孔结晶材料的新合成组合物：Mn / q（WaXbYcZdOh）其中M是一个或多个离子; n是不含M表示为氧化物的组成的电荷; q是M的加权摩尔平均化合价; n / q是M的摩尔数或摩尔分数; W是一个或多个二价元素; X是一个或多个三价元素; Y是一种或多种四价元素; Z是一种或多种五价元素; a，b，c和d分别为W，X，Y和Z的摩尔分数; （a + b + c + d）= 1; a> / = 0; b，c和d各自> 0; h为1〜2.5的数。 晶体材料通过i）使含有W，X，Z和有机导向剂的反应混合物结晶来制备; ii）使i）的产物与包含Y和有机导向剂的反应混合物接触; 和iii）保持ii）的混合物在足以形成所述组合物的条件下。 该组合物适用于有机化合物的催化转化。
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公开(公告)号：US5246689A
公开(公告)日：1993-09-21
申请号：US735240
申请日：1991-07-24
申请人： Jeffrey S. Beck , William S. Borghard , Charles T. Kresge , Michael E. Leonowicz , Wieslaw J. Roth , James C. Vartuli
发明人： Jeffrey S. Beck , William S. Borghard , Charles T. Kresge , Michael E. Leonowicz , Wieslaw J. Roth , James C. Vartuli
IPC分类号： B01D53/86 , B01J20/02 , B01J29/03 , B01J29/04 , B01J29/40 , B01J29/70 , B01J29/82 , B01J29/83 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , C10G47/16
CPC分类号： C10G11/05 , B01D53/8628 , B01J20/041 , B01J20/06 , B01J20/08 , B01J20/103 , B01J29/0308 , B01J29/04 , B01J29/041 , B01J29/40 , B01J29/70 , B01J29/82 , B01J29/83 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G47/16 , B01J2229/26 , B01J2229/32 , B01J2229/34 , B01J2229/36 , B01J2229/40 , B01J2229/42
摘要： This invention relates to a composition of matter, e.g., silicoaluminate or metalloaluminosilicate, comprising an inorganic, porous crystalline phase material exhibiting, after calcination, an X-ray diffraction pattern with at least one peak at a d-spacing greater than 1.8 nm and having a benzene adsorption capacity of greater than 15 grams benzene per 100 grams of said material at 6.7 kPa (50 torr) and 25.degree. C. wherein said crystalline phase has a composition expressed as follows:M.sub.n/q (W.sub.a X.sub.b Y.sub.c O.sub.h)wherein M is one or more ions; n is the charge of the composition excluding M expressed as oxides; q is the weighted molar average valence of M; n/q is the number of moles or mole fraction of M; W is one or more divalent elements; X is one or more trivalent elements; Y is one or more tetravalent elements; a, b, and c are mole fractions of W, X, and Y, respectively; h is a number of from 1 to 2.5; (a+b+c)=1; and a, b, and c, are each >0.
摘要翻译： 本发明涉及一种物质的组合物，例如硅铝酸盐或金属铝硅酸盐，其包含无机多孔结晶相材料，其在煅烧后表现出具有至少一个d值大于1.8nm的峰的X射线衍射图，并且具有 在6.7kPa（50托）和25℃下每100克所述材料苯吸附量大于15克苯。其中所述结晶相的组成如下表示：Mn / q（WaXbYcOh）其中M是一个或 更多离子 n是不含M表示为氧化物的组成的电荷; q是M的加权摩尔平均化合价; n / q是M的摩尔数或摩尔分数; W是一个或多个二价元素; X是一个或多个三价元素; Y是一种或多种四价元素; a，b和c分别是W，X和Y的摩尔分数; h是从1到2.5的数字; （a + b + c）= 1; 和a，b和c分别为> 0。
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公开(公告)号：US5145816A
公开(公告)日：1992-09-08
申请号：US718056
申请日：1991-06-20
申请人： Jeffrey S. Beck , David C. Calabro , Sharon B. McCullen , Bruce P. Pelrine , Kirk D. Schmitt , James C. Vartuli
发明人： Jeffrey S. Beck , David C. Calabro , Sharon B. McCullen , Bruce P. Pelrine , Kirk D. Schmitt , James C. Vartuli
IPC分类号： B01J20/10 , B01D53/86 , B01J20/02 , B01J29/03 , B01J29/04 , B01J29/06 , B01J29/40 , B01J29/70 , B01J29/82 , B01J29/83 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C01B39/04 , C01B39/06 , C01B39/48 , C10G11/05 , C10G47/16
CPC分类号： B01D53/8628 , B01J20/041 , B01J20/06 , B01J20/08 , B01J20/103 , B01J20/12 , B01J20/18 , B01J20/3078 , B01J29/0308 , B01J29/04 , B01J29/041 , B01J29/045 , B01J29/40 , B01J29/82 , B01J29/83 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , C10G47/16 , B01J2229/12 , B01J2229/14 , B01J2229/26 , B01J2229/32 , B01J2229/34 , B01J2229/40 , B01J2229/42
摘要： A method is described for modifying an ultra-large pore crystalline material by contacting with a treatment composition M'X'Y'.sub.n wherein M' is an element of Groups IIA, IVA, VA, VIA, VIIA, IB, IIB, IVB, VB or VIB; X' is halide, hydride, alkoxide of C.sub.1-6', or acetate; Y' is X or phosphine, sulfide, carbonyl or cyano; and N=1-5. The contacted crystalline material becomes functionalized. The functionalized material is also described and can be used as a sorbent or catalyst component.
摘要翻译： 描述了通过与处理组合物M'X'Y'n接触来改性超大孔结晶材料的方法，其中M'是IIA，IVA，VA，VIA，VIIA，IB，IIB，IVB，IVB族的元素， VB或VIB; X'是卤化物，氢化物，C1-6'的醇盐或乙酸盐; Y'是X或膦，硫化物，羰基或氰基; N = 1-5。 接触的结晶材料变得官能化。 还描述了官能化材料并且可以用作吸附剂或催化剂组分。
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7.发明授权
公开(公告)号：US5220101A
公开(公告)日：1993-06-15
申请号：US918322
申请日：1992-07-22
申请人： Jeffrey S. Beck , David C. Calabro , Sharon B. McCullen , Bruce P. Pelrine , Kirk D. Schmitt , James C. Vartuli
发明人： Jeffrey S. Beck , David C. Calabro , Sharon B. McCullen , Bruce P. Pelrine , Kirk D. Schmitt , James C. Vartuli
IPC分类号： B01D53/86 , B01J20/02 , B01J29/03 , B01J29/04 , B01J29/40 , B01J29/70 , B01J29/82 , B01J29/83 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , C10G47/16
CPC分类号： C10G47/16 , B01D53/8628 , B01J20/041 , B01J20/06 , B01J20/08 , B01J20/103 , B01J20/12 , B01J20/18 , B01J20/3078 , B01J29/0308 , B01J29/04 , B01J29/041 , B01J29/40 , B01J29/70 , B01J29/82 , B01J29/83 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , B01J2229/12 , B01J2229/14 , B01J2229/26 , B01J2229/32 , B01J2229/34 , B01J2229/36 , B01J2229/40 , B01J2229/42
摘要： A process is provided for separating at least one component from a mixture of components which comprises contacting the mixture with a composition comprising a functionalized inorganic, porous, non-layered crystalline phase having uniformly sized pores of at least about 13, e.g., at least about 15, Angstrom Units in diameter.
摘要翻译： 提供了用于从组分混合物中分离至少一种组分的方法，其包括使混合物与包含官能化无机，多孔，非层状结晶相的组合物接触，该组合物具有至少约13，例如至少约 15，直径单位。
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8.发明授权
公开(公告)号：US5200058A
公开(公告)日：1993-04-06
申请号：US895283
申请日：1992-06-08
申请人： Jeffrey S. Beck , David C. Calabro , Sharon B. McCullen , Bruce P. Pelrine , Kirk D. Schmitt , James C. Vartuli
发明人： Jeffrey S. Beck , David C. Calabro , Sharon B. McCullen , Bruce P. Pelrine , Kirk D. Schmitt , James C. Vartuli
IPC分类号： B01D53/86 , B01J20/02 , B01J29/03 , B01J29/04 , B01J29/40 , B01J29/70 , B01J29/82 , B01J29/83 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , C10G47/16
CPC分类号： B01J29/045 , B01D53/8628 , B01J20/041 , B01J20/06 , B01J20/08 , B01J20/103 , B01J20/12 , B01J20/3078 , B01J29/0308 , B01J29/04 , B01J29/041 , B01J29/82 , B01J29/83 , B01J29/85 , C01B37/00 , C01B37/02 , C01B37/08 , C01B39/00 , C10G11/05 , C10G47/16 , B01J2229/12 , B01J2229/14 , B01J2229/26 , B01J2229/32 , B01J2229/34 , B01J2229/36 , B01J2229/40 , B01J2229/42
摘要： A process is provided for effecting catalytic conversion of an organic compound-containing feedstock to conversion product which comprises contacting said feedstock under catalytic conversion conditions with a catalyst comprising an active form of a functionalized inorganic, porous, non-layered crystalline phase having uniformly sized pores of at least about 13, e.g., at least about 15, Angstrom Units in diameter.
摘要翻译： 提供了一种用于将含有机化合物的原料催化转化成转化产物的方法，其包括在催化转化条件下使所述原料与包含具有均匀尺寸的孔的官能化无机，多孔，非层状结晶相的活性形式的催化剂接触 至少约13，例如至少约15埃，直径单位。
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9.发明授权
公开(公告)号：US5689025A
公开(公告)日：1997-11-18
申请号：US382103
申请日：1995-02-01
CPC分类号： C07C6/123 , B01J29/40 , B01J37/086 , C07C2/66 , C07C2/864 , B01J2229/12 , B01J2229/32 , B01J2229/42 , C07C2529/06 , C07C2529/40 , C07C2529/65 , C07C2529/70
摘要： A process for ethylbenzene production that involves contacting a hydrocarbon feedstream including benzene and ethylene, under alkylation conditions, with a catalytic molecular sieve which has been modified by being ex situ selectivated with a silicon compound. The ex situ selectivation involves exposing the molecular sieve to at least two selectivation sequences, each selectivation sequence comprising contacting the catalyst with a silicon compound followed by calcination. The modified catalyst used in the process may also be steamed. Optionally, the modified catalyst may be trim-selectivated.
摘要翻译： 一种乙苯生产方法，其涉及在烷基化条件下使含有苯和乙烯的烃进料流与通过用硅化合物进行原位选择性修饰的催化分子筛接触。 异位选择包括将分子筛暴露于至少两个选择性序列，每个选择活性序列包括使催化剂与硅化合物接触，随后煅烧。 在该方法中使用的改性催化剂也可以蒸。 任选地，修饰的催化剂可以是修剪选择的。
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10.发明授权Selective ethylbenzene disproportionation process (SEBDP) with ex situ selectivated zeolite catalysts 失效选择性乙苯歧化过程（SEBDP）与非原位选择性沸石催化剂
公开(公告)号：US5382737A
公开(公告)日：1995-01-17
申请号：US69257
申请日：1993-05-28
CPC分类号： B01J37/086 , B01J29/40 , C07C6/123 , B01J2229/12 , B01J2229/32 , B01J2229/42 , C07C2529/40
摘要： A process for shape selective hydrocarbon conversion that involves contacting a hydrocarbon feedsteam, including ethylbenzene, under conversion conditions with a catalytic molecular sieve which has been modified by being ex situ selectivated with a silicon compound. The ex situ selectivation involves exposing the molecular sieve to at least two silicon impregnation sequences, each sequence comprising an impregnation with a silicon compound followed by calcination. The modified catalyst used in the process may also be steamed. Optionally, the modified catalyst may be trim-selectivated.
摘要翻译： 一种用于形状选择性烃转化的方法，其包括在转化条件下将烃类原料（包括乙苯）与通过用硅化合物进行非原位选择性修饰的催化分子筛接触。 异位选择包括将分子筛暴露于至少两个硅浸渍序列，每个序列包含用硅化合物浸渍，然后煅烧。 在该方法中使用的改性催化剂也可以蒸。 任选地，修饰的催化剂可以是修剪选择的。
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