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公开(公告)号：US20100055307A1
公开(公告)日：2010-03-04
申请号：US12338692
申请日：2008-12-18
申请人： Jennifer Nam Cha , Geraud Jean-Michel Dubois , James Lupton Hedrick , Ho-Cheol Kim , Victor Yee-Way Lee , Teddie Peregrino Magbitang , Robert Dennis Miller , Willi Volksen
发明人： Jennifer Nam Cha , Geraud Jean-Michel Dubois , James Lupton Hedrick , Ho-Cheol Kim , Victor Yee-Way Lee , Teddie Peregrino Magbitang , Robert Dennis Miller , Willi Volksen
CPC分类号： H01L21/3121 , G03F7/0002 , H01L21/02118 , H01L21/02126 , H01L21/02203 , H01L21/02216 , H01L21/02282 , H01L21/312 , H01L21/31695 , Y10T428/249953 , Y10T428/31663
摘要： A nanoporous material exhibiting a lamellar structure is disclosed. The material comprises three or more substantially parallel sheets of an organosilicate material, separated by highly porous spacer regions. The distance between the centers of the sheets lies between 1 nm and 50 nm. The highly porous spacer regions may be substantially free of condensed material. For the manufacture of such materials, a process is disclosed in which matrix non-amphiphilic polymeric material and templating polymeric material are dispersed in a solvent, where the templating polymeric material includes a polymeric amphiphilic material. The solvent with the polymeric materials is distributed onto a substrate. Organization is induced in the templating polymeric material. The solvent is removed, leaving the polymeric materials in place. The matrix polymeric material is cured, forming a lamellar structure.
摘要翻译： 公开了具有层状结构的纳米多孔材料。 该材料包括由高度多孔的间隔区隔开的三个或更多个基本平行的有机硅酸盐材料片。 片材中心之间的距离介于1nm和50nm之间。 高度多孔的间隔区域可以基本上不含冷凝材料。 为了制造这种材料，公开了一种方法，其中将基质非两亲性聚合物材料和模板聚合物材料分散在溶剂中，其中模板聚合材料包括聚合物两亲性材料。 具有聚合物材料的溶剂分布在基材上。 组织在模板聚合材料中被诱导。 除去溶剂，留下聚合物材料就位。 基体聚合材料固化，形成层状结构。
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公开(公告)号：US07482389B2
公开(公告)日：2009-01-27
申请号：US11111055
申请日：2005-04-20
申请人： Jennifer Nam Cha , Geraud Jean-Michel Dubois , James Lupton Hedrick , Ho-Cheol Kim , Victor Yee-Way Lee , Teddie Peregrino Magbitang , Robert Dennis Miller , Willi Volksen
发明人： Jennifer Nam Cha , Geraud Jean-Michel Dubois , James Lupton Hedrick , Ho-Cheol Kim , Victor Yee-Way Lee , Teddie Peregrino Magbitang , Robert Dennis Miller , Willi Volksen
IPC分类号： B32B3/26
CPC分类号： H01L21/3121 , G03F7/0002 , H01L21/02118 , H01L21/02126 , H01L21/02203 , H01L21/02216 , H01L21/02282 , H01L21/312 , H01L21/31695 , Y10T428/249953 , Y10T428/31663
摘要： A nanoporous material exhibiting a lamellar structure is disclosed. The material comprises three or more substantially parallel sheets of an organosilicate material, separated by highly porous spacer regions. The distance between the centers of the sheets lies between 1 nm and 50 nm. The highly porous spacer regions may be substantially free of condensed material. For the manufacture of such materials, a process is disclosed in which matrix non-amphiphilic polymeric material and templating polymeric material are dispersed in a solvent, where the templating polymeric material includes a polymeric amphiphilic material. The solvent with the polymeric materials is distributed onto a substrate. Organization is induced in the templating polymeric material. The solvent is removed, leaving the polymeric materials in place. The matrix polymeric material is cured, forming a lamellar structure.
摘要翻译： 公开了具有层状结构的纳米多孔材料。 该材料包括由高度多孔的间隔区隔开的三个或更多个基本平行的有机硅酸盐材料片。 片材中心之间的距离介于1nm和50nm之间。 高度多孔的间隔区域可以基本上不含冷凝材料。 为了制造这种材料，公开了一种方法，其中将基质非两亲性聚合物材料和模板聚合物材料分散在溶剂中，其中模板聚合材料包括聚合物两亲性材料。 具有聚合物材料的溶剂分布在基材上。 组织在模板聚合材料中被诱导。 除去溶剂，留下聚合物材料就位。 基体聚合材料固化，形成层状结构。
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3.发明授权公开(公告)号：US08481164B2
公开(公告)日：2013-07-09
申请号：US12061283
申请日：2008-04-02
CPC分类号： C08L101/12 , C08L53/00 , G03F7/0002 , Y10T428/24 , Y10T428/2495 , Y10T428/24975 , Y10T428/249921 , Y10T428/249953 , Y10T428/249958 , Y10T428/249975 , Y10T428/249978 , Y10T428/249979 , Y10T428/24998 , Y10T428/25 , Y10T428/26 , Y10T428/31504 , Y10T428/31511 , Y10T428/31612 , Y10T428/31663 , Y10T428/31931 , Y10T428/31935 , Y10T428/31938
摘要： A material and an associated method of formation. A self-assembling block copolymer that includes a first block species and a second block species respectively characterized by a volume fraction of F1 and F2 with respect to the self-assembling block copolymer is provided. At least one crosslinkable polymer that is miscible with the second block species is provided. The self-assembling block copolymer and the at least one crosslinkable polymer are combined to form a mixture. The mixture having a volume fraction, F3, of the crosslinkable polymer, a volume fraction, F1A, of the first block species, and a volume fraction, F2A, of the second block species is formed. A material having a predefined morphology where the sum of F2A and F3 were preselected is formed.
摘要翻译： 一种材料和相关的形成方法。 提供了一种自组装嵌段共聚物，其包括分别以相对于自组装嵌段共聚物的F1和F2的体积分数表征的第一嵌段和第二嵌段。 提供了与第二嵌段物质混溶的至少一种可交联聚合物。 自组装嵌段共聚物和至少一种可交联聚合物组合形成混合物。 形成具有可交联聚合物的体积分数F3，第一嵌段物质的体积分数F1A和第二嵌段物质的体积分数F2A的混合物。 形成具有预定形态的材料，其中预先选择F2A和F3的总和。
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公开(公告)号：US08784966B2
公开(公告)日：2014-07-22
申请号：US11950453
申请日：2007-12-05
CPC分类号： C08L101/12 , C08L53/00 , G03F7/0002 , Y10T428/24 , Y10T428/2495 , Y10T428/24975 , Y10T428/249921 , Y10T428/249953 , Y10T428/249958 , Y10T428/249975 , Y10T428/249978 , Y10T428/249979 , Y10T428/24998 , Y10T428/25 , Y10T428/26 , Y10T428/31504 , Y10T428/31511 , Y10T428/31612 , Y10T428/31663 , Y10T428/31931 , Y10T428/31935 , Y10T428/31938
摘要： A method of forming a material. A self-assembling block copolymer that includes a first block species and a second block species respectively characterized by a volume fraction of F1 and F2 with respect to the self-assembling block copolymer is provided. At least one crosslinkable polymer that is miscible with the second block species is provided. The self-assembling block copolymer and the at least one crosslinkable polymer are combined to form a mixture. The mixture having a volume fraction, F3, of the crosslinkable polymer, a volume fraction, F1A, of the first block species, and a volume fraction, F2A, of the second block species is formed. A material having a predefined morphology where the sum of F2A and F3 were preselected is formed.
摘要翻译： 一种形成材料的方法。 提供了一种自组装嵌段共聚物，其包括分别以相对于自组装嵌段共聚物的F1和F2的体积分数表征的第一嵌段和第二嵌段。 提供了与第二嵌段物质混溶的至少一种可交联聚合物。 自组装嵌段共聚物和至少一种可交联聚合物组合形成混合物。 形成具有可交联聚合物的体积分数F3，第一嵌段物质的体积分数F1A和第二嵌段物质的体积分数F2A的混合物。 形成具有预定形态的材料，其中预先选择F2A和F3的总和。
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公开(公告)号：US08389589B2
公开(公告)日：2013-03-05
申请号：US12338692
申请日：2008-12-18
申请人： Jennifer Nam Cha , Geraud Jean-Michel Dubois , James Lupton Hedrick , Ho-Cheol Kim , Victor Yee-Way Lee , Teddie Peregrino Magbitang , Robert Dennis Miller , Willi Volksen
发明人： Jennifer Nam Cha , Geraud Jean-Michel Dubois , James Lupton Hedrick , Ho-Cheol Kim , Victor Yee-Way Lee , Teddie Peregrino Magbitang , Robert Dennis Miller , Willi Volksen
CPC分类号： H01L21/3121 , G03F7/0002 , H01L21/02118 , H01L21/02126 , H01L21/02203 , H01L21/02216 , H01L21/02282 , H01L21/312 , H01L21/31695 , Y10T428/249953 , Y10T428/31663
摘要： A nanoporous material exhibiting a lamellar structure is disclosed. The material comprises three or more substantially parallel sheets of an organosilicate material, separated by highly porous spacer regions. The distance between the centers of the sheets lies between 1 nm and 50 nm. The highly porous spacer regions may be substantially free of condensed material. For the manufacture of such materials, a process is disclosed in which matrix non-amphiphilic polymeric material and templating polymeric material are dispersed in a solvent, where the templating polymeric material includes a polymeric amphiphilic material. The solvent with the polymeric materials is distributed onto a substrate. Organization is induced in the templating polymeric material. The solvent is removed, leaving the polymeric materials in place. The matrix polymeric material is cured, forming a lamellar structure.
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公开(公告)号：US20080213556A1
公开(公告)日：2008-09-04
申请号：US12061283
申请日：2008-04-02
CPC分类号： C08L101/12 , C08L53/00 , G03F7/0002 , Y10T428/24 , Y10T428/2495 , Y10T428/24975 , Y10T428/249921 , Y10T428/249953 , Y10T428/249958 , Y10T428/249975 , Y10T428/249978 , Y10T428/249979 , Y10T428/24998 , Y10T428/25 , Y10T428/26 , Y10T428/31504 , Y10T428/31511 , Y10T428/31612 , Y10T428/31663 , Y10T428/31931 , Y10T428/31935 , Y10T428/31938
摘要： A material and an associated method of formation. A self-assembling block copolymer that includes a first block species and a second block species respectively characterized by a volume fraction of F1 and F2 with respect to the self-assembling block copolymer is provided. At least one crosslinkable polymer that is miscible with the second block species is provided. The self-assembling block copolymer and the at least one crosslinkable polymer are combined to form a mixture. The mixture having a volume fraction, F3, of the crosslinkable polymer, a volume fraction, F1A, of the first block species, and a volume fraction, F2A, of the second block species is formed. A material having a predefined morphology where the sum of F2A and F3 were preselected is formed.
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公开(公告)号：US08436062B2
公开(公告)日：2013-05-07
申请号：US13101017
申请日：2011-05-04
申请人： Jennifer Nam Cha , James Lupton Hedrick , Ho-Cheol Kim , Victor Yee-Way Lee , Teddie Peregrino Magbitang , Robert Dennis Miller , Willi Volksen
发明人： Jennifer Nam Cha , James Lupton Hedrick , Ho-Cheol Kim , Victor Yee-Way Lee , Teddie Peregrino Magbitang , Robert Dennis Miller , Willi Volksen
摘要： Substantially or roughly spherical micellar structures useful in the formation of nanoporous materials by templating are disclosed. A roughly spherical micellar structure is formed by organization of one or more spatially unsymmetric organic amphiphilic molecules. Each of those molecules comprises a branched moiety and a second moiety. The branched moiety can form part of either the core or the surface of the spherical micellar structure, depending on the polarity of the environment. The roughly spherical micellar structures form in a thermosetting polymer matrix. They are employed in a templating process whereby the amphiphilic molecules are dispersed in the polymer matrix, the matrix is cured, and the porogens are then removed, leaving nanoscale pores.
摘要翻译： 公开了用于通过模板形成纳米多孔材料的基本或大致球形的胶束结构。 通过组织一个或多个空间上不对称的有机两亲分子形成大致球形的胶束结构。 这些分子中的每一个包括支链部分和第二部分。 取决于环境的极性，支化部分可以形成球形胶束结构的芯或表面的一部分。 大致球形的胶束结构在热固性聚合物基体中形成。 它们用于模板化过程，由此将两亲分子分散在聚合物基质中，使基质固化，然后去除孔隙原，留下纳米孔。
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公开(公告)号：US20110245433A1
公开(公告)日：2011-10-06
申请号：US13101017
申请日：2011-05-04
申请人： Jennifer Nam Cha , James Lupton Hedrick , Ho-Cheol Kim , Victor Yee-Way Lee , Teddie Peregrino Magbitang , Robert Dennis Miller , Willi Volksen
发明人： Jennifer Nam Cha , James Lupton Hedrick , Ho-Cheol Kim , Victor Yee-Way Lee , Teddie Peregrino Magbitang , Robert Dennis Miller , Willi Volksen
摘要： Substantially or roughly spherical micellar structures useful in the formation of nanoporous materials by templating are disclosed. A roughly spherical micellar structure is formed by organization of one or more spatially unsymmetric organic amphiphilic molecules. Each of those molecules comprises a branched moiety and a second moiety. The branched moiety can form part of either the core or the surface of the spherical micellar structure, depending on the polarity of the environment. The roughly spherical micellar structures form in a thermosetting polymer matrix. They are employed in a templating process whereby the amphiphilic molecules are dispersed in the polymer matrix, the matrix is cured, and the porogens are then removed, leaving nanoscale pores.
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公开(公告)号：US07960442B2
公开(公告)日：2011-06-14
申请号：US11111343
申请日：2005-04-20
申请人： Jennifer Nam Cha , Geraud Jean-Michel Dubois , James Lupton Hedrick , Ho-Cheol Kim , Victor Yee-Way Lee , Teddie Peregrino Magbitang , Robert Dennis Miller , Willi Volksen
发明人： Jennifer Nam Cha , Geraud Jean-Michel Dubois , James Lupton Hedrick , Ho-Cheol Kim , Victor Yee-Way Lee , Teddie Peregrino Magbitang , Robert Dennis Miller , Willi Volksen
IPC分类号： C08J9/00
摘要： Substantially or roughly spherical micellar structures useful in the formation of nanoporous materials by templating are disclosed. A roughly spherical micellar structure is formed by organization of one or more spatially unsymmetric organic amphiphilic molecules. Each of those molecules comprises a branched moiety and a second moiety. The branched moiety can form part of either the core or the surface of the spherical micellar structure, depending on the polarity of the environment. The roughly spherical micellar structures form in a thermosetting polymer matrix. They are employed in a templating process whereby the amphiphilic molecules are dispersed in the polymer matrix, the matrix is cured, and the porogens are then removed, leaving nanoscale pores.
摘要翻译： 公开了用于通过模板形成纳米多孔材料的基本或大致球形的胶束结构。 通过组织一个或多个空间上不对称的有机两亲分子形成大致球形的胶束结构。 这些分子中的每一个包括支链部分和第二部分。 取决于环境的极性，支化部分可以形成球形胶束结构的芯或表面的一部分。 大致球形的胶束结构在热固性聚合物基体中形成。 它们用于模板化过程，由此将两亲分子分散在聚合物基质中，使基质固化，然后去除孔隙原，留下纳米孔。
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10.发明授权公开(公告)号：US07341788B2
公开(公告)日：2008-03-11
申请号：US11077804
申请日：2005-03-11
IPC分类号： B32B27/30
CPC分类号： C08L101/12 , C08L53/00 , G03F7/0002 , Y10T428/24 , Y10T428/2495 , Y10T428/24975 , Y10T428/249921 , Y10T428/249953 , Y10T428/249958 , Y10T428/249975 , Y10T428/249978 , Y10T428/249979 , Y10T428/24998 , Y10T428/25 , Y10T428/26 , Y10T428/31504 , Y10T428/31511 , Y10T428/31612 , Y10T428/31663 , Y10T428/31931 , Y10T428/31935 , Y10T428/31938
摘要： A material and an associated method of formation. A self-assembling block copolymer that includes a first block species and a second block species respectively characterized by a volume fraction of F1 and F2 with respect to the self-assembling block copolymer is provided. At least one crosslinkable polymer that is miscible with the second block species is provided. The self-assembling block copolymer and the at least one crosslinkable polymer are combined to form a mixture. The mixture having a volume fraction, F3, of the crosslinkable polymer, a volume fraction, F1A, of the first block species, and a volume fraction, F2A, of the second block species is formed. A material having a predefined morphology where the sum of F2A and F3 were preselected is formed.
摘要翻译： 一种材料和相关的形成方法。 一种自组装嵌段共聚物，其包括分别以相对于自组装的F 1和F 2的体积分数表征的第一嵌段物质和第二嵌段物质 嵌段共聚物。 提供了与第二嵌段物质混溶的至少一种可交联聚合物。 自组装嵌段共聚物和至少一种可交联聚合物组合形成混合物。 具有第一嵌段物质的可交联聚合物的体积分数F 3 N 3，体积分数F 1 A 1，以及体积分数F 2A 。 预先选择具有预定形态的材料，其中预先选择F 2 A 2和F 3 3之和。
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