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公开(公告)号：US07015354B2
公开(公告)日：2006-03-21
申请号：US10917414
申请日：2004-08-13
申请人： Jochen Petzoldt , Signe Unverricht , Heiko Arnold , Klaus Joachim Müller-Engel , Martin Dieterle
发明人： Jochen Petzoldt , Signe Unverricht , Heiko Arnold , Klaus Joachim Müller-Engel , Martin Dieterle
CPC分类号： C07C45/35 , C07C51/252 , C07C47/22 , C07C57/04
摘要： A process for preparing (meth)acrolein and/or (meth)acrylic acid by heterogeneously catalyzed gas phase partial oxidation of an organic precursor compound over a fresh fixed catalyst bed, in which the process is started up at a reduced hourly space velocity of charging gas mixture on the fixed catalyst bed.
摘要翻译： 通过在新鲜的固定催化剂床上的有机前体化合物的非均相催化气相部分氧化制备（甲基）丙烯醛和/或（甲基）丙烯酸的方法，其中该方法以减小的小时空速充电开始 固定催化剂床上的气体混合物。
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2.发明授权Heterogeneously catalyzed partial gas phase oxidation of acrolein to acrylic acid 有权丙烯醛的异相催化部分气相氧化成丙烯酸公开(公告)号：US06982347B2
公开(公告)日：2006-01-03
申请号：US10806460
申请日：2004-03-23
IPC分类号： C07C51/235
CPC分类号： C07C51/252 , C07C57/04
摘要： In a process for partially oxidizing acrolein to acrylic acid in the gas phase under heterogeneous catalysis, the starting reaction gas mixture is oxidized at an acrolein loading of ≦145 and ≧70 l (STP) of acrolein/l of fixed catalyst bed·h over a fixed catalyst bed which is accommodated in two successive reaction zones A, B, the highest temperature of the reaction gas mixture within reaction zone A being above the highest temperature of the reaction gas mixture within reaction zone B.
摘要翻译： 在非均相催化下在气相中将丙烯醛部分氧化为丙烯酸的方法中，起始反应气体混合物以丙烯醛负载<= 145和> = 70l（STP）的丙烯醛/ l固定催化剂床进行氧化。 h在固定的催化剂床上，其被容纳在两个连续的反应区A，B中，反应区A内的反应气体混合物的最高温度高于反应区B内的反应气体混合物的最高温度。
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3.发明授权Heterogeneously catalyzed partial gas phase oxidation of propene to acrylic acid 有权将丙烯非均相催化部分气相氧化成丙烯酸公开(公告)号：US06888024B2
公开(公告)日：2005-05-03
申请号：US10799754
申请日：2004-03-15
CPC分类号： B01J23/002 , B01J23/8876 , B01J23/8877 , B01J35/0006 , B01J37/0221 , B01J2523/00 , C07C51/252 , C07C57/04 , B01J2523/17 , B01J2523/55 , B01J2523/68 , B01J2523/69 , B01J2523/13 , B01J2523/41 , B01J2523/54 , B01J2523/842 , B01J2523/845
摘要： In a process for heterogeneously catalyzed partial gas phase oxidation of propene to acrylic acid, the starting reaction gas mixture is oxidized at a propene loading of
摘要翻译： 在将丙烯非均相催化的部分气相氧化成丙烯酸的过程中，起始反应气体混合物在第一反应阶段中以<160l（STP）/ 1h的丙烯负载量在被容纳的固定催化剂床1上被氧化 在两个连续的反应区A，B和第一反应阶段的含丙烯醛的产物气体混合物随后在第二反应阶段中在固定的催化剂床2上氧化，固定的催化剂床2容纳在两个连续的反应区C，D中， 反应区A内的反应气体混合物的最高温度高于反应区B内反应气体混合物的最高温度，反应区C内的反应气体混合物的最高温度高于反应气体混合物的最高温度 区D.
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公开(公告)号：US20050038291A1
公开(公告)日：2005-02-17
申请号：US10917414
申请日：2004-08-13
CPC分类号： C07C45/35 , C07C51/252 , C07C47/22 , C07C57/04
摘要： A process for preparing (meth)acrolein and/or (meth)acrylic acid by heterogeneously catalyzed gas phase partial oxidation of an organic precursor compound over a fresh fixed catalyst bed, in which the process is started up at a reduced hourly space velocity of charging gas mixture on the fixed catalyst bed.
摘要翻译： 通过在新鲜的固定催化剂床上的有机前体化合物的非均相催化气相部分氧化制备（甲基）丙烯醛和/或（甲基）丙烯酸的方法，其中该方法以减小的小时空速充电开始 固定催化剂床上的气体混合物。
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5.发明授权Method for producing a multi metal oxide catalyst, method for producing unsaturated aldehydes and/or carboxylic acids and band calcination device 有权多金属氧化物催化剂的制造方法，不饱和醛和/或羧酸的制造方法以及带烧结装置公开(公告)号：US06881702B2
公开(公告)日：2005-04-19
申请号：US10363856
申请日：2001-09-20
IPC分类号： B01J6/00 , B01J19/18 , B01J19/22 , B01J23/88 , B01J23/888 , B01J35/00 , B01J37/08 , C07B61/00 , C07C27/14 , C07C45/33 , C07C45/34 , C07C45/35 , C07C45/38 , C07C47/22 , C07C51/215 , C07C51/25 , C07C57/05 , B01J23/00 , B01J21/08 , B01J21/12 , B01J21/14 , B01J27/192
CPC分类号： C07C51/215 , B01J6/004 , B01J19/1862 , B01J19/22 , B01J23/002 , B01J23/88 , B01J23/8885 , B01J35/0006 , B01J37/08 , B01J2219/00132 , B01J2219/00157 , B01J2219/182 , B01J2523/00 , C07C45/33 , C07C45/34 , C07C45/35 , C07C45/38 , C07C51/252 , C07C47/22 , C07C57/04 , B01J2523/13 , B01J2523/41 , B01J2523/54 , B01J2523/68 , B01J2523/69 , B01J2523/842 , B01J2523/845
摘要： A catalyst suitable for the gas-phase oxidation of organic compounds to α,β-unsaturated aldehydes and/or carboxylic acids and having an active phase comprising a multimetal oxide material is prepared by a process in which a particulate catalyst precursor which contains oxides and/or compounds of the elements other than oxygen which constitute the multimetal oxide material, which compounds can be converted into oxides, is prepared and said catalyst precursor is converted by calcination into a catalytically active form, wherein a stream of the particulate catalyst precursor is passed at substantially constant speed through at least one calcination zone at constant temperature for calcination.
摘要翻译： 适合于将有机化合物气相氧化成α，β-不饱和醛和/或羧酸并且具有包含多金属氧化物材料的活性相的催化剂通过以下方法制备，其中含有氧化物和/ 或构成多金属氧化物材料的氧以外的元素的化合物，该化合物可以转化为氧化物，并且将所述催化剂前体通过煅烧转化为催化活性形式，其中将颗粒状催化剂前体的流通过 通过至少一个煅烧区在恒定温度下用于煅烧的基本上恒定的速度。
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6.发明申请Heterogeneously catalyzed gas-phase partial oxidation of precursor compounds of (meth)acrylic acid 审中-公开（甲基）丙烯酸前体化合物的非均相催化气相部分氧化公开(公告)号：US20070032680A1
公开(公告)日：2007-02-08
申请号：US11443135
申请日：2006-05-31
IPC分类号： C07C51/16 , C07C51/235
CPC分类号： C07C51/235 , B01J19/30 , B01J23/28 , B01J23/31 , B01J23/8876 , B01J23/8877 , B01J35/002 , B01J35/026 , B01J2219/30223 , B01J2219/30242 , B01J2219/30475 , C07C45/35 , C07C51/252 , C07C47/22 , C07C57/04
摘要： In a process for the heterogeneously catalyzed gas-phase partial oxidation of precursor compounds of (meth)acrylic acid over a fixed catalyst bed which contains, as a catalyst, a mixed oxide active material shaped into a geometric body, the geometric body is a geometric base body into whose surface a cavity has been introduced.
摘要翻译： 在（甲基）丙烯酸前体化合物在固定催化剂床上的非均相催化气相部分氧化的方法中，该固定催化剂床含有形成几何体的混合氧化物活性物质作为催化剂，几何体是几何体 基体已经被引入其表面。
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公开(公告)号：US06794539B2
公开(公告)日：2004-09-21
申请号：US10380159
申请日：2003-03-17
IPC分类号： C07C5116
CPC分类号： B01J37/00 , B01J23/002 , B01J23/887 , B01J35/0006 , B01J2523/00 , C07C51/252 , C07C57/04 , B01J2523/17 , B01J2523/55 , B01J2523/68 , B01J2523/69
摘要： In a process for preparing a multiplephase multimetal oxide composition comprising Mo, V, Cu and, if desired, further elements, at least one phase is preformed separately and dispersed in a plastically deformable precursor composition of a further phase. The mixture is dried and calcined. The multimetal oxide composition is suitable as active composition of catalysts for the catalytically oxidation of organic compounds in the gas phase, in particular for the oxidation of acrolein to acrylic acid.
摘要翻译： 在制备包含Mo，V，Cu的多相多金属氧化物组合物的方法中，并且如果需要，另外的元素，至少一个相分别预成型并分散在另一相的可塑变形的前体组合物中。 将混合物干燥并煅烧。 多金属氧化物组合物适合用作气相中有机化合物催化氧化的催化剂的活性组合物，特别是用于将丙烯醛氧化成丙烯酸。
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公开(公告)号：US07122707B2
公开(公告)日：2006-10-17
申请号：US10398287
申请日：2001-10-09
申请人： Jochen Petzoldt , Signe Unverricht , Heiko Arnold
发明人： Jochen Petzoldt , Signe Unverricht , Heiko Arnold
CPC分类号： B01J37/0221 , B01J23/002 , B01J23/8876 , B01J2523/00 , C07C45/35 , C07C47/22 , B01J2523/13 , B01J2523/41 , B01J2523/54 , B01J2523/68 , B01J2523/842 , B01J2523/845
摘要： Coated catalysts which are suitable for the gas-phase catalytic oxidation of propene to acrolein are prepared by a process in which rings are used as supports and water is used as a binder.
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9.发明授权Heterogenically catalysed gas-phase partial oxidation method for precursor compounds of (meth)acrylic acid 失效（甲基）丙烯酸前体化合物的异相催化气相部分氧化法公开(公告)号：US07129195B2
公开(公告)日：2006-10-31
申请号：US10466244
申请日：2002-01-12
CPC分类号： C07C51/235 , B01J19/30 , B01J23/28 , B01J23/31 , B01J23/8876 , B01J23/8877 , B01J35/002 , B01J35/026 , B01J2219/30223 , B01J2219/30242 , B01J2219/30475 , C07C45/35 , C07C51/252 , C07C47/22 , C07C57/04
摘要： The invention relates to a method for the heterogenically catalyed gas-phase partial oxidation of precursor compounds of (meth)acrylic acid in a fixed catalyst bed, containing as the catalyst an activated mass of mixed oxide, shaped to form a geometric body. Said geometric body is a geometric base body, into whose surface a cavity is incorporated.
摘要翻译： 本发明涉及在固定催化剂床中异构催化气相部分氧化前体化合物（甲基）丙烯酸的方法，该方法含有形成几何体的成形为混合氧化物的活化物质作为催化剂。 所述几何体是几何基体，其表面中并入有空腔。
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10.发明授权公开(公告)号：US07211691B2
公开(公告)日：2007-05-01
申请号：US10784825
申请日：2004-02-24
申请人： Jochen Petzoldt , Martin Dieterle , Heiko Arnold , Wilhelm Ruppel , Klaus-Joachim Mueller-Engel
发明人： Jochen Petzoldt , Martin Dieterle , Heiko Arnold , Wilhelm Ruppel , Klaus-Joachim Mueller-Engel
IPC分类号： C07C51/16
CPC分类号： C07C45/35 , C07C51/252 , C07C47/22 , C07C57/04
摘要： In a process for heterogeneously catalyzed partial gas phase oxidation of propene to acrolein, the starting reaction gas mixture is oxidized over a fixed catalyst bed which consists of at least two fixed catalyst bed zones and is accommodated in two successive temperature zones A, B, and the transition from temperature zone A to temperature zone B does not spatially coincide with a transition from one fixed catalyst bed zone to another fixed catalyst bed zone.
摘要翻译： 在将丙烯非均相催化的部分气相氧化成丙烯醛的过程中，起始反应气体混合物在由至少两个固定的催化剂床区组成的固定催化剂床上被氧化，并被容纳在两个连续的温度区A，B和 从温度区A到温度区B的过渡在空间上与从一个固定的催化剂床区到另一个固定催化剂床区的过渡不一致。
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