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公开(公告)号：US4904704A
公开(公告)日：1990-02-27
申请号：US289082
申请日：1988-12-22
IPC分类号： C07C263/18 , C07C263/20 , C07C265/14 , C08G18/00 , C08G18/58 , C08G18/70 , C08G18/72 , C08G18/76 , C08G101/00
CPC分类号： C08G18/58 , C07C263/20 , C08G18/003 , C08G18/4018 , C08G18/4213 , C08G18/4816 , C08G18/4829 , C08G18/727 , C08G18/7621 , C08G18/7664 , C08G2101/0025 , C08G2105/02
摘要： A method of treating toluene diisocyanate distillation residues comprising reacting the residues with at least about 0.5 equivalents, based on hydrolyzable chloride concentration of the residues, of an epoxy compound at a temperature of from about 155 to about 220.degree. C. to produce a treated distillation residue having a hydrolyzable chloride level of less than about 800 parts per million (ppm) is taught. The product of the method is useful, for instance, in producing rigid foams with low K Factors.
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2.发明授权Flexible polyurethane rebond foam having improved tear resistance and method for the preparation thereof 失效具有改善的抗撕裂性的柔性聚氨酯泡沫泡沫塑料及其制备方法
公开(公告)号：US5290818A
公开(公告)日：1994-03-01
申请号：US989256
申请日：1992-12-11
CPC分类号： C08J9/33 , C08G18/10 , C08G18/727 , C08J2375/04 , C08J2475/00 , Y10S264/07
摘要： Rebond polyurethane foams can be prepared by coating shredded polyurethane foam with a prepolymer binder formulation which includes toluene diisocyanate distillation bottoms, compressing the binder coated foam, and the curing the binder with steam. The toluene diisocyanate distillation bottoms can be used in place of more expensive prepolymer formulation components such as toluene diisocyanate or methylene diphenyldiisocyanate. The toluene diisocyanate distillation bottoms can also improve elongation and tear resistance properties of the resultant rebond foams prepared therewith.
摘要翻译： 可以通过用包含甲苯二异氰酸酯蒸馏塔底物，压缩粘合剂涂覆的泡沫和用蒸汽固化粘合剂的预聚物粘合剂制剂涂布切碎的聚氨酯泡沫来制备再粘合聚氨酯泡沫。 可以使用甲苯二异氰酸酯蒸馏塔底代替更昂贵的预聚物配制组分如甲苯二异氰酸酯或亚甲基二苯基二异氰酸酯。 甲苯二异氰酸酯蒸馏塔底还可以改善由此制备的所得到的泡沫泡沫的伸长率和抗撕裂性能。
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公开(公告)号：US5312888A
公开(公告)日：1994-05-17
申请号：US148471
申请日：1993-11-08
CPC分类号： C08J9/33 , C08G18/10 , C08G18/727 , C08J2375/04 , C08J2475/00 , Y10S264/07
摘要： Rebond polyurethane foams can be prepared by coating shredded polyurethane foam with a prepolymer binder formulation which includes toluene diisocyanate distillation bottoms, compressing the binder coated foam, and the curing the binder with steam. The toluene diisocyanate distillation bottoms can be used in place of more expensive prepolymer formulation components such as toluene diisocyanate or methylene diphenyldiisocyanate. The toluene diisocyanate distillation bottoms can also improve elongation and tear resistance properties of the resultant rebond foams prepared therewith.
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4.发明授权Polyol-fluorocarbon-aminetriol blend and polyisocyanurate foams therefore 失效因此，多元醇 - 氟烃 - 二胺混合物和聚异氰尿酸酯泡沫
公开(公告)号：US4289858A
公开(公告)日：1981-09-15
申请号：US117436
申请日：1980-02-01
CPC分类号： C08G18/4018 , C08G18/5021 , C08G18/667 , C08G2105/02 , C08G2350/00 , Y10S521/902
摘要： Disclosed are novel polyol blends comprising from about 20 percent to about 85 percent by weight of said blend of an amine triol, or mixture of amine triols selected from the formula ##STR1## wherein R is an aliphatic radical having from 8 to 18 carbon atoms, inclusive, each R.sub.1 is independently selected from the group consisting of hydrogen or methyl, x, y, and z each independently have an average value from about 1 to about 5 inclusive, n is 2 or 3; and from about 15 percent to about 80 percent by weight of a primary hydroxyl polyol characterized by a molecular weight of from about 60 to about 1000.The polyol blends are miscible with fluorocarbon blowing agents and water and other adjuvants including trimerization catalysts.The novel blends are particularly useful in an improved process for the preparation of polyisocyanurate foams. The foams are characterized by high reaction exotherms making such foams particularly suited to the preparation of polyisocyanurate foam laminates.
摘要翻译： 公开了新型多元醇共混物，其包含约20重量％至约85重量％的所述三元醇混合物或选自下式的胺三醇的混合物其中R为具有8至18个碳原子的脂族基团， 每个R 1独立地选自氢或甲基，x，y和z各自独立地具有约1至约5的平均值，其中n为2或3; 和约15％至约80％重量的伯羟基多元醇，其特征在于分子量为约60至约1000.多元醇共混物可与氟碳发泡剂和水以及其它助剂（包括三聚催化剂）混溶。 新颖的共混物在制备聚异氰脲酸酯泡沫体的改进方法中特别有用。 泡沫的特征在于高反应放热，使得这种泡沫特别适用于制备聚异氰脲酸酯泡沫层压材料。
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公开(公告)号：US4246364A
公开(公告)日：1981-01-20
申请号：US122029
申请日：1980-02-19
CPC分类号： C08G18/5039 , C08G18/3825 , C08G2105/02
摘要： Disclosed are novel polyol blends comprising from about 20 percent to about 85 percent by weight of said blend of an amide diol, or mixture of amide diols selected from the formula ##STR1## wherein R is an aliphatic radical having from 7 to 17 carbon atoms, inclusive, each R.sub.1 is independently selected from the group consisting of hydrogen or methyl, x and y each independently have an average value from about 1 to about 3 inclusive; and from about 15 percent to about 80 percent by weight of a primary hydroxyl polyol characterized by a molecular weight of from about 60 to about 1000.The polyol blends are miscible with fluorocarbon blowing agents and water and other adjuvants including trimerization catalysts.The novel blends are particularly useful in an improved process for the preparation of polyisocyanurate foams. The foams are characterized by high reaction exotherms making such foams particularly suited to the preparation of polyisocyanurate foam laminates.
摘要翻译： 公开了新型多元醇共混物，其包含约20重量％至约85重量％的所述酰胺二醇或选自下式的酰胺二醇的混合物：其中R是具有7至17个碳原子的脂族基团， 每个R 1独立地选自氢或甲基，x和y各自独立地具有约1至约3的平均值; 和约15％至约80％重量的伯羟基多元醇，其特征在于分子量为约60至约1000.多元醇共混物可与氟碳发泡剂和水以及其它助剂（包括三聚催化剂）混溶。 新颖的共混物在制备聚异氰脲酸酯泡沫体的改进方法中特别有用。 泡沫的特征在于高反应放热，使得这种泡沫特别适用于制备聚异氰脲酸酯泡沫层压材料。
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6.发明授权Portable, expandable mold for fabricating substantially isotropic isocyanate based polymer foam buns 失效用于制造基本上各向同性异氰酸酯的聚合物泡沫小圆面包的便携式可扩展模具
公开(公告)号：US4179094A
公开(公告)日：1979-12-18
申请号：US910077
申请日：1978-05-26
CPC分类号： B29C44/586 , B29C33/30 , B29K2075/00 , Y10S264/84
摘要： A mold is described for the molding of substantially isotropic isocyanate-based polymer foam buns. The mold is a box mold which has sidewalls of which at least one pair disposed in parallel relationship is adapted to move outwardly when subjected to pressure exerted by the expanding foam during the molding operation. The outward movement of the sidewalls is controlled by stops provided on the periphery of the mold floor, said sidewalls being free to slide over the surface of the floor. The lid of the mold is supported in sliding engagement with the upper edges of the sidewalls. The mold and the process of fabricating foam buns therewith is particularly suitable for use in situations (e.g. operation in the field) in which it is not possible or practicable to employ continuous bunstock machines. The mold is relatively inexpensive and readily dismantled for transportation to a fabrication site.
摘要翻译： 描述了用于模制基本上各向同性的异氰酸酯基聚合物泡沫小圆面包的模具。 模具是具有侧壁的盒模具，其中至少一对平行关系设置成在模制操作期间受膨胀泡沫施加的压力时向外移动。 侧壁的向外运动由设置在模具地板的周边上的挡块控制，所述侧壁可自由地在地板的表面上滑动。 模具的盖子被支撑成与侧壁的上边缘滑动接合。 模具和其中制造泡沫块的方法特别适用于不可能或可行地使用连续坯料机器的情况（例如在现场操作中）。 模具相对便宜并易于拆卸以便运输到制造现场。
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7.发明授权Process for molding a substantially isotropic isocyanate-based polymer foam bun 失效用于模制基本上各向同性的异氰酸酯基聚合物泡沫块的方法
公开(公告)号：US4104346A
公开(公告)日：1978-08-01
申请号：US709777
申请日：1976-07-29
IPC分类号： B29B7/00 , B29C39/00 , B29C39/26 , B29C39/32 , B29C39/40 , B29C44/58 , B29C67/20 , B29K105/04 , B29D27/04
CPC分类号： B29C44/586 , Y10S264/84
摘要： A mold is described for the molding of substantially isotropic isocyanate-based polymer foam buns. The mold is a box mold which has sidewalls of which at least one pair disposed in parallel relationship is adapted to move outwardly when subjected to pressure exerted by the expanding foam during the molding operation. The outward movement of the sidewalls is controlled by stops provided on the periphery of the mold floor, said sidewalls being free to slide over the surface of the floor. The lid of the mold is supported in sliding engagement with the upper edges of the sidewalls. The mold and the process of fabricating foam buns therewith is particularly suitable for use in situations (e.g. operation in the field) in which it is not possible or practicable to employ continuous bunstock machines. The mold is relatively inexpensive and readily dismantled for transportation to a fabrication site.
摘要翻译： 描述了用于模制基本上各向同性的异氰酸酯基聚合物泡沫小圆面包的模具。 模具是具有侧壁的盒模具，其中至少一对平行关系设置成在模制操作期间受膨胀泡沫施加的压力时向外移动。 侧壁的向外运动由设置在模具地板的周边上的挡块控制，所述侧壁可自由地在地板的表面上滑动。 模具的盖子被支撑成与侧壁的上边缘滑动接合。 模具和其中制造泡沫块的方法特别适用于不可能或可行地使用连续坯料机器的情况（例如在现场操作中）。 模具相对便宜并易于拆卸以便运输到制造现场。
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公开(公告)号：US4339343A
公开(公告)日：1982-07-13
申请号：US204243
申请日：1980-11-03
CPC分类号： C08G18/667 , C08G18/4018 , C08G18/5021 , C08G2105/02 , C08G2350/00 , Y10S521/902
摘要： Disclosed are novel polyol blends comprising from about 20 percent to about 85 percent by weight of said blend of an amine diol, or mixture of amine diols selected from the formula ##STR1## wherein R is an aliphatic radical having from 8 to 18 carbon atoms, inclusive, each R.sub.1 is independently selected from the group consisting of hydrogen or methyl, x and y each independently have an average value from about 4 to about 15 inclusive; and from about 15 percent to about 80 percent by weight of a primary hydroxyl polyol characterized by a molecular weight of from about 60 to about 1000.The polyol blends are miscible with fluorocarbon blowing agents and water and other adjuvants including trimerization catalysts.The novel blends are particularly useful in an improved process for the preparation of polyisocyanurate foams. The foams are characterized by high reaction exotherms making such foams particularly suited to the preparation of polyisocyanurate foam laminates.
摘要翻译： 公开了新型多元醇共混物，其包含约20重量％至约85重量％的所述胺二醇或选自下式的胺二醇的混合物：其中R是具有8至18个碳原子的脂族基团， 每个R 1独立地选自氢或甲基，x和y各自独立地具有约4至约15的平均值; 和约15％至约80％重量的伯羟基多元醇，其特征在于分子量为约60至约1000.多元醇共混物可与氟碳发泡剂和水以及其它助剂（包括三聚催化剂）混溶。 新颖的共混物在制备聚异氰脲酸酯泡沫体的改进方法中特别有用。 泡沫的特征在于高反应放热，使得这种泡沫特别适用于制备聚异氰脲酸酯泡沫层压材料。
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公开(公告)号：US4256802A
公开(公告)日：1981-03-17
申请号：US127478
申请日：1980-03-05
IPC分类号： C08G18/38 , C08G18/40 , C08G18/50 , C08G18/66 , B32B5/18 , C08G18/14 , C08G18/30 , C08G18/48
CPC分类号： C08G18/5021 , C08G18/3825 , C08G18/4018 , C08G18/6666 , C08G2350/00 , Y10S521/902 , Y10T428/249953 , Y10T428/31547
摘要： Disclosed are novel polyol blends comprising from about 20 percent to about 85 percent by weight of said blend of an amine diol, or mixture of amine diols selected from the formula ##STR1## wherein R is an aliphatic radical having from 8 to 18 carbon atoms, inclusive, each R.sub.1 is independently selected from the group consisting of hydrogen or methyl, x and y each independently have an average value from about 4 to about 15 inclusive; and from about 15 percent to about 80 percent by weight of a primary hydroxyl polyol characterized by a molecular weight of from about 60 to about 1000.The polyol blends are miscible with fluorocarbon blowing agents and water and other adjuvants including trimerization catalysts.The novel blends are particularly useful in an improved process for the preparation of polyisocyanurate foams. The foams are characterized by high reaction exotherms making such foams particularly suited to the preparation of polyisocyanurate foam laminates.
摘要翻译： 公开了新型多元醇共混物，其包含约20重量％至约85重量％的所述胺二醇或选自下式的胺二醇的混合物的混合物，其中R是具有8至18个碳原子的脂族基团， 每个R 1独立地选自氢或甲基，x和y各自独立地具有约4至约15的平均值; 和约15％至约80％重量的伯羟基多元醇，其特征在于分子量为约60至约1000.多元醇共混物可与氟碳发泡剂和水以及其它助剂（包括三聚催化剂）混溶。 新颖的共混物在制备聚异氰脲酸酯泡沫体的改进方法中特别有用。 泡沫的特征在于高反应放热，使得这种泡沫特别适用于制备聚异氰脲酸酯泡沫层压材料。
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