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    Tire tread compound made with strain crystallizable 3,4-polyisoprene
    3.
    发明授权
    Tire tread compound made with strain crystallizable 3,4-polyisoprene 失效
    用应变结晶的3,4-聚异戊二烯制成的轮胎胎面复合材料

    公开(公告)号：US5356997A

    公开(公告)日：1994-10-18

    申请号：US968916

    申请日：1992-10-30

    申请人： Johnny D. Massie, II ,  Wen-Liang Hsu ,  Adel F. Halasa ,  Paul H. Sandstrom

    发明人： Johnny D. Massie, II ,  Wen-Liang Hsu ,  Adel F. Halasa ,  Paul H. Sandstrom

    IPC分类号： C08F4/60 ,  C08F4/70 ,  C08F36/08 ,  C08F136/08 ,  C08L9/00

    CPC分类号： C08F136/08 ,  C08F2410/01 ,  Y10S152/905

    摘要： Strain crystallizable 3,4-polyisoprene having a 3,4-microstructure content which is within the range of about 65% to about 85%, a cis-1,4-microstructure content which is within the range of about 15% to about 35%, and essentially no trans-1,4-microstructure or 1,2-microstructure can be synthesized in organic solvents to quantitative yields after short polymerization times by utilizing the catalyst systems of this invention. This invention specifically discloses a process for the synthesis of 3,4-polyisoprene which comprises polymerizing isoprene monomer in an organic solvent at a temperatIre which is within the range of about -10.degree. C. to about 100.degree. C. in the presence of a catalyst system which is comprised of (a) an organoiron compound which is soluble in the organic solvent, wherein the iron in the organoiron compound is in the +3 oxidation state, (b) a partially hydrolyzed organoaluminum compound which was prepared by adding a protonic compound selected from the group consisting of water, alcohols and carboxylic acids to the organoaluminum compound, and (c) a chelating aromatic amine; wherein the molar ratio of the chelating amine to the organoiron compound is within the range of about 0.1:1 to about 1:1, wherein the molar ratio of the organoaluminum compound to the organoiron compound is within the range of about 5:1 to about 200:1, and wherein the molar ratio of the protonic compound to the organoaluminum compound is within the range of about 0,001:1 to about 0.2:1.

    摘要翻译： 具有3,4-微结构含量在约65％至约85％范围内的应变可结晶的3,4-聚异戊二烯，顺式-1,4-微结构含量在约15％至约35的范围内 通过利用本发明的催化剂体系，在短时间聚合时间之后，可以在有机溶剂中基本上没有反式-1,4-微结构或1,2-微结构合成定量产率。 本发明具体公开了一种合成3,4-聚异戊二烯的方法，该方法包括在有机溶剂中将异戊二烯单体在约-10℃至约100℃范围内的温度下聚合， 催化剂体系，其由（a）可溶于有机溶剂的有机铁化合物组成，其中有机铁化合物中的铁处于+3氧化态，（b）部分水解的有机铝化合物，其通过加入质子 选自水，醇和羧酸的化合物的有机铝化合物的化合物，和（c）螯合芳族胺; 其中螯合胺与有机铁化合物的摩尔比在约0.1:1至约1:1的范围内，其中有机铝化合物与有机铁化合物的摩尔比在约5:1至约 200：1，其中质子化合物与有机铝化合物的摩尔比在约0.001:1至约0.2:1的范围内。

    Polyurethane rolls and methods of manufacturing
    4.
    发明授权
    Polyurethane rolls and methods of manufacturing 有权
    聚氨酯辊及其制造方法

    公开(公告)号：US07347808B2

    公开(公告)日：2008-03-25

    申请号：US10755904

    申请日：2004-01-13

    申请人： Bradley L. Beach ,  Bhaskar Gopalanarayanan ,  Johnny D. Massie, II

    发明人： Bradley L. Beach ,  Bhaskar Gopalanarayanan ,  Johnny D. Massie, II

    IPC分类号： G03G15/04

    CPC分类号： C08G18/4277 ,  C08G18/10 ,  C08G18/61 ,  C08G18/69 ,  C08G18/40 ,  C08G18/48

    摘要： Rolls having a polyurethane elastomer formed from a polyurethane mixture, wherein the polyurethane mixture comprises polydiene, tri-functional polyol curative, an additional graft polymer curative having a molecular weight of at least about 800 and comprising diol, polyol, diamine, polyamine or a combination thereof, conductive modifier, antioxidant, and hydrolytic stabilizer. Methods of forming such rolls include casting the polyurethane mixture, followed by curing, then demolding, grinding to desired dimensions and baking such that the outer layer of the cured roll is oxidized.

    摘要翻译： 具有由聚氨酯混合物形成的聚氨酯弹性体的辊，其中所述聚氨酯混合物包含聚二烯，三官能多元醇固化剂，分子量为至少约800的另外的接枝聚合物固化剂，并且包含二醇，多元醇，二胺，多胺或组合 导电改性剂，抗氧化剂和水解稳定剂。 形成这种辊的方法包括浇铸聚氨酯混合物，然后固化，然后脱模，研磨至所需尺寸并烘烤，使得固化的辊的外层被氧化。

    Polyurethane elastomers with combination of curatives
    8.
    发明授权
    Polyurethane elastomers with combination of curatives 有权
    聚氨酯弹性体与固化剂组合

    公开(公告)号：US07034097B2

    公开(公告)日：2006-04-25

    申请号：US10756009

    申请日：2004-01-13

    申请人： Bradley L. Beach ,  Bhaskar Gopalanarayanan ,  Kelly A. Killeen ,  Johnny D. Massie, II ,  Ronald L. Roe

    发明人： Bradley L. Beach ,  Bhaskar Gopalanarayanan ,  Kelly A. Killeen ,  Johnny D. Massie, II ,  Ronald L. Roe

    IPC分类号： C08G18/62

    CPC分类号： C08G18/4277 ,  C08G18/10 ,  Y10S428/906 ,  Y10T428/139 ,  C08G18/48 ,  C08G18/61 ,  C08G18/69

    摘要： Polyurethane elastomers are formed from first and second graft curatives, each graft curative having a molecular weight of at least about 800, wherein the first and second graft curatives are substantially immiscible with one another, and wherein the polyurethane elastomer exhibits a hardness of less than about 40 Shore A according to ASTM D2240-86 and a compression set of less than about 8% according to ASTM D395-89, method B, at a temperature of about 70° C. for about 22 hours. Rolls are manufactured using such polyurethane elastomers, particularly rolls that are suitable for use in image forming devices, such as electrophotographic print applications.

    摘要翻译： 聚氨酯弹性体由第一和第二接枝固化剂形成，每个接枝固化剂具有至少约800的分子量，其中第一和第二接枝固化剂基本上彼此不混溶，并且其中聚氨酯弹性体显示出小于约 40肖氏A，按照ASTM D395-89，方法B，在约70℃的温度下约22小时，压缩永久变形小于约8％。 使用这种聚氨酯弹性体制造卷筒，特别是适用于图像形成装置的卷，例如电子照相印刷应用。

    Having a core and at least one coaxial layer of filaments twisted in the same direction at the same pitch
    9.
    发明授权
    Having a core and at least one coaxial layer of filaments twisted in the same direction at the same pitch 失效
    具有芯和至少一个同轴的同轴层，以相同的间距在同一方向上扭转

    公开(公告)号：US5473878A

    公开(公告)日：1995-12-12

    申请号：US36951

    申请日：1993-03-25

    申请人： Charles E. Hamiel ,  Kenneth M. Kot ,  Johnny D. Massie, II ,  Kenneth J. Palmer ,  Italo M. Sinopoli

    发明人： Charles E. Hamiel ,  Kenneth M. Kot ,  Johnny D. Massie, II ,  Kenneth J. Palmer ,  Italo M. Sinopoli

    IPC分类号： D07B1/06

    CPC分类号： D07B1/0626 ,  D07B2201/2006 ,  D07B2201/2023 ,  D07B2201/2025 ,  D07B2201/2028 ,  D07B2201/2029 ,  D07B2201/204 ,  D07B2201/2061 ,  D07B2201/2097 ,  D07B2401/208 ,  D07B2501/2046 ,  Y10S57/902

    摘要： The invention is directed to several embodiments of metallic cord for the reinforcement of tires wherein one or more coaxial layers of metallic filaments are arranged around the metallic core filaments and twisted in the same direction at the same pitch. In one embodiment, the ratio of the diameter of the core filaments to the layer filaments is at least 1.28. In another embodiment, two of the core filaments have a first diameter and the third core filament has a second diameter smaller than the first diameter daimeter. In still another embodiment, two of the core filaments have a first diameter and a third of the core filaments has a second diameter smaller than the first diameter while the coaxial layer filaments have a third diameter equal to the second diameter. In another embodiment, the core has three core filaments twisted about each other and a coaxial layer of eight layer filaments arranged around the core filaments. In yet another embodiment, the core filaments have a first diameter and the layer filaments have a second diameter which is larger than the first diameter.

    摘要翻译： 本发明涉及用于加强轮胎的金属帘线的几个实施例，其中金属细丝的一个或多个同轴层布置在金属芯丝周围并且以相同的间距在相同方向上扭转。 在一个实施例中，芯丝的直径与层丝的比例至少为1.28。 在另一个实施例中，两个芯丝具有第一直径，并且第三芯丝具有小于第一直径daimeter的第二直径。 在另一个实施例中，两个芯丝具有第一直径，并且三根芯丝具有小于第一直径的第二直径，而同轴层丝具有等于第二直径的第三直径。 在另一个实施例中，芯具有三个彼此相互扭转的芯丝和围绕芯丝布置的八层丝的同轴层。 在另一个实施例中，芯丝具有第一直径，并且层丝具有大于第一直径的第二直径。