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    Compounds containing tertiary amino groups, a process for their production and their use as catalysts
    1.
    发明授权
    Compounds containing tertiary amino groups, a process for their production and their use as catalysts 失效
    含有叔氨基的化合物，其制备方法及其用作催化剂

    公开(公告)号：US5482979A

    公开(公告)日：1996-01-09

    申请号：US255524

    申请日：1994-06-08

    申请人： Josef Sanders ,  Ulrich Liman ,  Klaus Konig

    发明人： Josef Sanders ,  Ulrich Liman ,  Klaus Konig

    IPC分类号： C07C229/30 ,  C08G18/18 ,  C08G18/67 ,  C07C229/02

    CPC分类号： C07C229/30 ,  C08G18/1825 ,  C08G18/1866 ,  C08G18/6795 ,  C08G2101/00

    摘要： Compounds containing ester groups and tertiary amino groups and optionally hydroxyl groups are made by reacting optionally hydroxyfunctional acetoacetic acid esters of monofunctional or polyfunctional alcohols (particularly polyfunctional polyether polyols) with primary/tertiary polyamines (particularly diamines). These compounds are useful as optionally incorporable catalysts for the isocyanate addition reaction in the production of polyurethane foams by the isocyanate polyaddition process.

    摘要翻译： 含有酯基和叔氨基和任选的羟基的化合物是通过使任意的单功能或多官能醇（特别是多官能聚醚多元醇）的羟基官能的乙酰乙酸酯与伯/叔多胺（特别是二胺）反应制得的。 这些化合物可用作用于通过异氰酸酯加聚方法生产聚氨酯泡沫体中的异氰酸酯加成反应的任选的可加入的催化剂。

    Tertiary amines having carbonate and urethane groups
    3.
    发明授权
    Tertiary amines having carbonate and urethane groups 失效
    具有碳酸酯和氨基甲酸酯基团的叔胺

    公开(公告)号：US5705672A

    公开(公告)日：1998-01-06

    申请号：US510830

    申请日：1995-08-03

    申请人： Klaus Konig ,  Ulrich Liman ,  Josef Sanders

    发明人： Klaus Konig ,  Ulrich Liman ,  Josef Sanders

    IPC分类号： C07C271/20 ,  C08G18/18 ,  C08G71/02 ,  C07C271/00

    CPC分类号： C08G18/1841 ,  C07C271/20 ,  C08G2101/00

    摘要： Tertiary amines having carbonate and urethane groups and optionally hydroxyl groups are produced by reacting a) a polyhydric alcohol and b) a primary-tertiary diamine with c) a carbonic acid derivative selected from the group consisting of optionally cyclic carbonates, urea, phosgene and bis-chlorocarbonates of alcohols of the same type as those used as component a). This reaction may be carried out in one or two steps. The tertiary amines produced by this process are useful as catalysts, which may optionally be incorporated into an isocyanate-reactive material, in the isocyanate addition reaction for the production of polyurethane plastics. These tertiary amines are particularly useful for the production of foam backed plastic films.

    摘要翻译： 具有碳酸酯和氨基甲酸酯基团和任选的羟基的叔胺通过使a）多元醇和b）伯 - 叔二胺与c）选自任选环状碳酸酯，脲，光气和双 与用作组分a）相同类型的醇的氯代碳酸酯。 该反应可以在一个或两个步骤中进行。 通过该方法生产的叔胺可用作用于生产聚氨酯塑料的异氰酸酯加成反应中的催化剂，其可任选地并入异氰酸酯反应性材料中。 这些叔胺特别可用于生产泡沫塑料膜。

    Process for the preparation of ethercarboxylic acids
    4.
    发明授权
    Process for the preparation of ethercarboxylic acids 失效
    制备醚羧酸的方法

    公开(公告)号：US5523479A

    公开(公告)日：1996-06-04

    申请号：US230282

    申请日：1994-04-20

    申请人： Josef Sanders ,  Klaus Konig

    发明人： Josef Sanders ,  Klaus Konig

    IPC分类号： C07C51/367 ,  C07C67/31 ,  C07C59/10 ,  C07C59/125 ,  C07C59/245

    CPC分类号： C07C67/31 ,  C07C51/367

    摘要： A process for the preparation of carboxylic acids which contain ether groups by the catalytically accelerated addition of alcoholic hydroxyl groups from mono- or polyhydric alcohols to tertiary-alkyl esters of .alpha.,.beta.-unsaturated carboxylic acids, and followed with acid hydrolysis of the tertiary-alkyl .beta.-ethercarboxylate obtained as intermediates in this way.

    摘要翻译： 通过催化加速将醇羟基从一元醇或多元醇加成加成α，β-不饱和羧酸的叔烷基酯，然后酸性水解叔丁醇，制备含有醚基团的羧酸的方法， 以此方式获得的作为中间体的β-羧酸叔丁酯。

    Continuous process for the preparation of highly stable, finely divided, low viscosity polymer polyols of small average particle size
    8.
    发明授权
    Continuous process for the preparation of highly stable, finely divided, low viscosity polymer polyols of small average particle size 失效
    用于制备平均粒度小的高度稳定，细分，低粘度的聚合物多元醇的连续方法

    公开(公告)号：US5814699A

    公开(公告)日：1998-09-29

    申请号：US723659

    申请日：1996-10-03

    申请人： Mark R. Kratz ,  Manfred Dietrich ,  Torsten Heinemann ,  Gundolf Jacobs ,  Josef Sanders ,  Helmut Woynar

    发明人： Mark R. Kratz ,  Manfred Dietrich ,  Torsten Heinemann ,  Gundolf Jacobs ,  Josef Sanders ,  Helmut Woynar

    IPC分类号： C08F212/10 ,  C08F220/42 ,  C08F220/44 ,  C08F283/06 ,  C08F285/00 ,  C08F290/02 ,  C08G18/63 ,  C08F283/02

    CPC分类号： C08G18/635 ,  C08F290/02 ,  C08G2101/0008 ,  C08G2101/0016

    摘要： A continuous process for the preparation of highly stable, finely divided, low viscosity polymer polyols of small average particle size wherein in the first step an intermediate is prepared by reacting (1) a mixture of at least two ethylenically unsaturated monomers, preferably styrene and acrylonitrile, in a mixture comprising (2) a base polyol and (3) a macromer in the presence of (4) a free radical initiator, (5) a solvent having moderate chain transfer activity, and, optionally, (6) a reaction moderator at a temperature of at least 100.degree. C., such that the intermediate contains at least about 12% by weight of macromer, based on the weight of the base polyol and macromer, and a solids content of at least about 15% by weight and less than about 30% by weight, based on the weight of the base polyol, macromer and ethylenically unsaturated monomers. The intermediate, which functions as a seed for further polymerization, is then further reacted, in one or more stirred-tank reactors in series, in a mixture of at least two ethylenically unsaturated monomers, preferably styrene and acrylonitrile, in a base polyol and, optionally, a macromer, in the presence of solvent, initiator and a reaction moderator which are distributed among the remaining reactors.

    摘要翻译： 一种用于制备平均粒度小的高度稳定，细分，低粘度的聚合物多元醇的连续方法，其中在第一步中，通过使（1）至少两种烯属不饱和单体，优选苯乙烯和丙烯腈的混合物 在（4）自由基引发剂，（5）具有中等链转移活性的溶剂的存在下，（2）基础多元醇和（3）大分子单体的混合物中，和（6）反应调节剂 在至少100℃的温度下，使得中间体含有至少约12重量％的大分子单体，基于基础多元醇和大分子单体的重量，固体含量至少约15重量％，和 小于约30重量％，基于基础多元醇，大分子单体和烯属不饱和单体的重量。 作为进一步聚合的种子的中间体在一个或多个串联的搅拌釜反应器中在基础多元醇中进一步在至少两种烯属不饱和单体，优选苯乙烯和丙烯腈的混合物中反应， 任选地，大分子单体在溶剂，引发剂和反应缓和剂的存在下分布在剩余的反应器中。

    Process for the production of diisocyanates, selected diisocyanates produced thereby and the production of polyurethane plastics therefrom
    10.
    发明授权
    Process for the production of diisocyanates, selected diisocyanates produced thereby and the production of polyurethane plastics therefrom 失效
    用于生产二异氰酸酯的方法，由此生产的所选择的二异氰酸酯和由其生产聚氨酯塑料

    公开(公告)号：US4820866A

    公开(公告)日：1989-04-11

    申请号：US84547

    申请日：1987-08-12

    申请人： Josef Sanders

    发明人： Josef Sanders

    IPC分类号： C08G18/76 ,  C07C67/00 ,  C07C69/00 ,  C07C201/00 ,  C07C205/37 ,  C07C213/00 ,  C07C241/00 ,  C07C263/10 ,  C07C265/12 ,  C08G18/77 ,  C08G18/78 ,  C08L75/04

    CPC分类号： C07C265/12 ,  C08G18/771

    摘要： Diisocyanates corresponding to a specified formula are produced by reacting an alcohol corresponding to a specified formula with a nitrochlorobenzene in the presence of NaOH and/or KOH in powder form and a strongly polar, aprotic solvent to produce a dinitro compound corresponding to a specified formula. This dinitro compound is hydrogenated to form the corresponding diamine which diamine is phosgenated to produce the corresponding diisocyanate. The resultant diisocyanates may then be used as starting materials in polyisocyanate addition processes.

    摘要翻译： 对应于规定的配方的二异氰酸酯是通过使在粉末形式的NaOH和/或KOH的存在下与对应于特定式的醇与硝基氯苯反应制得的，以产生对应于特定式的二硝基化合物。 将该二硝基化合物氢化以形成相应的二胺，其中二胺被光气化以产生相应的二异氰酸酯。 然后可以将得到的二异氰酸酯用作多异氰酸酯加成方法中的起始原料。